Blends of PC and PPSQ (A) with high M-w and good ladderlike regularity or PPSQ(B) with low M-w and more defective Si-atoms in its structure have been prepared by solution casting. The dispersed spheres (PPSQ(A)-rich) ...Blends of PC and PPSQ (A) with high M-w and good ladderlike regularity or PPSQ(B) with low M-w and more defective Si-atoms in its structure have been prepared by solution casting. The dispersed spheres (PPSQ(A)-rich) are unevenly dispersed in the continuous PC-rich phase and there is no phase-inversion as PPSQ(A) content increases when the percentage of PPSQ(A) is not more than 70%. PPSQ(B)-rich spheres are evenly dispersed in the continuous phase (PC-rich) and phase-inversion occurs when PPSQ(B) percentage is up to 70%. T-g of PPSQ(A)/PC or PPSQ(B)/PC at some compositions are lower than that of pure PC due to the enlarged free-volume of PC-rich phase because some spheres of rigid PPSQ chains are included in the PC-rich phase. PC and PPSQ(A) or PPSQ(B) are partially compatible. The compatibility of PC and PPSQ(B) is better than that of PC and PPSQ(A) with high M-w and good ladderlike regularity. Heat history has some influence on the T(g)s and compatibility of PPSQ(A)/PC and PPSQ(B)/PC blends.展开更多
A set of device is designed based on PC to realize the functions of traditional potentiostats in the phase ana1ysis of galvanochemistry. In the device, A/D and D/A conversion is used to measure the electrode potential...A set of device is designed based on PC to realize the functions of traditional potentiostats in the phase ana1ysis of galvanochemistry. In the device, A/D and D/A conversion is used to measure the electrode potential and convert the voltage for outPut; specific program runs in the PC to regulate and control the system. The effect of the proportion factor Kp on the control variation is researched through certain experiment. Two experiments, the control of electrolysis in constant poteniial and the determination of polarization curves, are designed to test and evaluate the effectiveness of the device. The experimemel results show that the variation between the actualanode potential and the target potential could be controlled to below 1 mV if Kp is set to an appropriate value.展开更多
In this paper, a new approach of muhi-modality image registration is represented with not only image intensity, but also features describing image structure. There are two novelties in the proposed method. Firstly, in...In this paper, a new approach of muhi-modality image registration is represented with not only image intensity, but also features describing image structure. There are two novelties in the proposed method. Firstly, instead of standard mutual information ( MI ) based on joint intensity histogram, regional mutual information ( RMI ) is employed, which allows neighborhood information to be taken into account. Secondly, a new feature images obtained by means of phase congruency are invariants to brightness or contrast changes. By incorporating these features and intensity into RMI, we can combine the aspects of both structural and neighborhood information together, which offers a more robust and a high level of registration accuracy.展开更多
基金This work was supported by Fund of Head of College of Chemistry,Shandong University.
文摘Blends of PC and PPSQ (A) with high M-w and good ladderlike regularity or PPSQ(B) with low M-w and more defective Si-atoms in its structure have been prepared by solution casting. The dispersed spheres (PPSQ(A)-rich) are unevenly dispersed in the continuous PC-rich phase and there is no phase-inversion as PPSQ(A) content increases when the percentage of PPSQ(A) is not more than 70%. PPSQ(B)-rich spheres are evenly dispersed in the continuous phase (PC-rich) and phase-inversion occurs when PPSQ(B) percentage is up to 70%. T-g of PPSQ(A)/PC or PPSQ(B)/PC at some compositions are lower than that of pure PC due to the enlarged free-volume of PC-rich phase because some spheres of rigid PPSQ chains are included in the PC-rich phase. PC and PPSQ(A) or PPSQ(B) are partially compatible. The compatibility of PC and PPSQ(B) is better than that of PC and PPSQ(A) with high M-w and good ladderlike regularity. Heat history has some influence on the T(g)s and compatibility of PPSQ(A)/PC and PPSQ(B)/PC blends.
文摘A set of device is designed based on PC to realize the functions of traditional potentiostats in the phase ana1ysis of galvanochemistry. In the device, A/D and D/A conversion is used to measure the electrode potential and convert the voltage for outPut; specific program runs in the PC to regulate and control the system. The effect of the proportion factor Kp on the control variation is researched through certain experiment. Two experiments, the control of electrolysis in constant poteniial and the determination of polarization curves, are designed to test and evaluate the effectiveness of the device. The experimemel results show that the variation between the actualanode potential and the target potential could be controlled to below 1 mV if Kp is set to an appropriate value.
文摘In this paper, a new approach of muhi-modality image registration is represented with not only image intensity, but also features describing image structure. There are two novelties in the proposed method. Firstly, instead of standard mutual information ( MI ) based on joint intensity histogram, regional mutual information ( RMI ) is employed, which allows neighborhood information to be taken into account. Secondly, a new feature images obtained by means of phase congruency are invariants to brightness or contrast changes. By incorporating these features and intensity into RMI, we can combine the aspects of both structural and neighborhood information together, which offers a more robust and a high level of registration accuracy.