MnO2/MnO cathode material with superior Zn^2+storage performance is prepared through a simple physical mixing method.The MnO2/MnO nanocomposite with a mixed mass ratio of 12:1 exhibits the highest specific capacity(36...MnO2/MnO cathode material with superior Zn^2+storage performance is prepared through a simple physical mixing method.The MnO2/MnO nanocomposite with a mixed mass ratio of 12:1 exhibits the highest specific capacity(364.2 mA·h/g at 0.2C),good cycle performance(170.4 mA·h/g after 100 cycles)and excellent rate performance(205.7 mA·h/g at 2C).Analysis of cyclic voltammetry(CV)data at various scan rates shows that both diffusioncontrolled insertion behavior and surface capacitive behavior contribute to the Zn2+storage performance of MnO2/MnO cathodes.And the capacitive behavior contributes more at high discharge rates,due to the short paths of ion diffusion and the rapid transfer of electrons.展开更多
In this paper, the effectiveness, applicability and validity of chemicalephysical combined methods(CPCMs) for treatment of marine clay (MC) slurries were evaluated. The method CPCM1 combineschemical stabilization ...In this paper, the effectiveness, applicability and validity of chemicalephysical combined methods(CPCMs) for treatment of marine clay (MC) slurries were evaluated. The method CPCM1 combineschemical stabilization and vacuum preloading (VP), while CPCM2 is similar to CPCM1 but includes boththe application of surcharge and use of geo-bags to provide confinement during surcharge preloading.The key advantage of CPCM2 using geo-bags is that the surcharge can be immediately applied on thechemically stabilized slurries. Two types of geo-bags were investigated under simulated land filling anddyke conditions, respectively. The test results show that the shear strength (cu) of treated slurry byCPCM2 is generally much higher than that by CPCM1. Besides, the use of CPCM2 can significantly reducethe treatment time due to the short drainage paths created by geo-bags. Overall, CPCM2 allows fasterconsolidation and higher preloading that help to achieve higher mechanical properties of the stabilizedslurry. There are consistent relationships between cU and water content of slurries treated by CPCM2.Several important observations were also made based on comparisons of experimental data. 2015 Institute of Rock and Soil Mechanics, Chinese Academy of Sciences. Production and hosting byElsevier B.V. All rights reserved.展开更多
Physical parameters are very important for vehicle dynamic modeling and analysis.However,most of physical parameter identification methods are assuming some physical parameters of vehicle are known,and the other unkno...Physical parameters are very important for vehicle dynamic modeling and analysis.However,most of physical parameter identification methods are assuming some physical parameters of vehicle are known,and the other unknown parameters can be identified.In order to identify physical parameters of vehicle in the case that all physical parameters are unknown,a methodology based on the State Variable Method(SVM) for physical parameter identification of two-axis on-road vehicle is presented.The modal parameters of the vehicle are identified by the SVM,furthermore,the physical parameters of the vehicle are estimated by least squares method.In numerical simulations,physical parameters of Ford Granada are chosen as parameters of vehicle model,and half-sine bump function is chosen to simulate tire stimulated by impulse excitation.The first numerical simulation shows that the present method can identify all of the physical parameters and the largest absolute value of percentage error of the identified physical parameter is 0.205%;and the effect of the errors of additional mass,structural parameter and measurement noise are discussed in the following simulations,the results shows that when signal contains 30 d B noise,the largest absolute value of percentage error of the identification is 3.78%.These simulations verify that the presented method is effective and accurate for physical parameter identification of two-axis on-road vehicles.The proposed methodology can identify all physical parameters of 7-DOF vehicle model by using free-decay responses of vehicle without need to assume some physical parameters are known.展开更多
To analyze the effect of different lowland rice varieties and different cooking methods on physical and chemical characteristics of cooked rice. A factorial randomized block design with two factors was used and each c...To analyze the effect of different lowland rice varieties and different cooking methods on physical and chemical characteristics of cooked rice. A factorial randomized block design with two factors was used and each combination of the factors was repeated three times. The first factor was rice variety(Ciherang and Ciliwung) and the second factor was the cooking method(stovetop, boiling and steaming, and rice cooker). Results showed that Ciherang and Ciliwung varieties were classified into slender grain rice type with yellowred color. The amylose content of Ciherang was classified as moderate, while the amylose content of Ciliwung classified as low. The most abundant amino acid contained in Ciherang and Ciliwung varieties was glutamic acid. Statistical analysis showed that cooking method had significant effects on texture, lightness, chroma, hue and moisture content of cooked rice. Rice cooked with liwet method had the lowest texture value, lowest lightness value, highest chroma value, and highest moisture content.展开更多
Method of VSC (Voltage Shorted Compaction)can be used to determine the intrinsic temperature dependence ofconductivity ofpolycrystalline compaction. The experimental conditions and technical key for preparation of VSC...Method of VSC (Voltage Shorted Compaction)can be used to determine the intrinsic temperature dependence ofconductivity ofpolycrystalline compaction. The experimental conditions and technical key for preparation of VSC device and its physical model as well as its applications in conducting polymers are discussed in detail.展开更多
The titanium oxide (TiO2) nanotubes have attracted attention for their use in dye-sensitized solar cells as photoanode. In this study semiconducting cadmium sulfide (CdS) nanoparticles arc grown on top opened TiO2...The titanium oxide (TiO2) nanotubes have attracted attention for their use in dye-sensitized solar cells as photoanode. In this study semiconducting cadmium sulfide (CdS) nanoparticles arc grown on top opened TiO2 nanotubes arrays by radio-frequency magnetron sputtering. X-ray diffraction, scanning electron mieroscopy, transmission electron microscopy and diffuse reflection spectra are used to study structural, morphological and optical properties of the CdS/TiO2 bilayer.展开更多
Nanometer-sized metal clusters were prepared inside single crystalline MgO films by vacuum co-deposition of metals and MgO. The atomic structure was studied by high-resolution electron microscopy (HREM) and nm-area el...Nanometer-sized metal clusters were prepared inside single crystalline MgO films by vacuum co-deposition of metals and MgO. The atomic structure was studied by high-resolution electron microscopy (HREM) and nm-area electron diffraction. The size of the clusters is ranging from 1 nm to 3 nm without those larger than 5 nm, and most of them have definite epitaxial orientations with the MgO matrix films. The character of the composite films is very much useful for the studies of various kinds of physical properties with anisotroPy. The physical properties such as electric transport, magnetic, optical absorption, sintering and catalytic ones were thus measured on the same samples analyzed by HREM by using high sensitivity apparatus with interest of clarifying the retationship between the atomic structure and physical properties展开更多
Three directions of development of kinetic indentation methods.Physical-energetic analysis of the indentation force diagram according to ISO 14577.Physical theory and universal criterion for the macrohardness of a mat...Three directions of development of kinetic indentation methods.Physical-energetic analysis of the indentation force diagram according to ISO 14577.Physical theory and universal criterion for the macrohardness of a material.Model of the physical process,thermomechanical potential,function of the state of the kinetic macroindentation process.Method for determining the physical function and unit of measurement of the kinetic macrohardness of a material.The ratio of the values of the empirical(standard)and physical macrohardness of the material.Physical reason for the appearance of the size effect in empirical indentation methods.The principle of determining the standard value of physical macrohardness.展开更多
Results of analytical studies of the physical properties of the function and number of empirical macrohardness based on the standard experimental force diagram of kinetic macroindentation by a sphere.An analytical com...Results of analytical studies of the physical properties of the function and number of empirical macrohardness based on the standard experimental force diagram of kinetic macroindentation by a sphere.An analytical comparison method and a criterion for the similarity of the physical and empirical macrohardness of a material are proposed.The physical properties of the hardness measurement process using the Calvert-Johnson method are shown.The physical reasons for the size effect when measuring macrohardness are considered.The universal physical unit and standard of macrohardness of kinetic macroindentation by a sphere is substantiated.展开更多
Different questions may be raised during the course of analysis concerning in particular the characterization of materials used, their preparation and application techniques. The different methods used to identify the...Different questions may be raised during the course of analysis concerning in particular the characterization of materials used, their preparation and application techniques. The different methods used to identify the materials of mud brick, limestone, plaster, mortar and pigments, collected from different sites and periods from Egypt, in order to identify and characterize the materials, their structure, composition and their mineralogical compounds were: (Op) optical microscopy, which was used to examine and to identify the materials structures. Methods used in initial examination were: (1) (MCA): Micro-chemical analysis, to identify the nature of the materials and for water-soluble salts, to identify sulphates, chlorides, carbonates, nitrites and nitrates; (2) (SM): Standard methods of wet chemical analysis were used to identify the quantitative and qualitative nature of the, mud building, mortars and their mixtures; (3) (SEM & EDS): Analytical scanning electron microscope with energy dispersive X-ray analysis system was used to examine the micro-morphology and determine the chemical composition of the different materials; (4) (XRD & XRPD): X-ray diffraction to identify the mineralogical compound of the plaster, limestone, mortars and pigments used. From all the results obtained, it was possible to establish the nature of the mortars and their binders as well as some other inclusion. In addition to the identification of the stratigraphy of the layers applied in some samples, the examination and analysis gave details of the materials and the approximate ratio of the amount of additives used. Furthermore, the mineralogical analysis provided information on the main mineralogical phases present in the materials analyzed from the different periods.展开更多
The identification of binding media presents a major difficulty in the investigation of painting techniques. The materials used in ancient times as a media for the pigments were varied, such as glues, gums and egg whi...The identification of binding media presents a major difficulty in the investigation of painting techniques. The materials used in ancient times as a media for the pigments were varied, such as glues, gums and egg white. These adhesives were mixed with the pigments to adhere to the surface or to prepare the ground. This medium serves to protect the pigments more or less perfectly, from chemical and mechanical injury. Binding media determines the technique of painting. Artists' techniques used through the centuries differ more in the binding media than in the pigments used. They are all organic substances containing the same common elements, and in the small samples which can be removed from paintings, occur only in micro quantities, moreover, binding media undergo considerable degradation over long periods of time. In the examination of works of art, only very small specimens can be taken and, the proportion of binding medium to pigment being small, sensitive methods of analysis have to be adopted in an attempt to detect and identify the medium that may have been used. On the other hand, the use of such methods possesses the disadvantage that impurities present in the painting materials may also be detected and may lead to erroneous conclusions. There is no general microanalysis technique existed in the identification of binding media, and the materials commonly used as media are highly complex compared with the simple inorganic compounds employed as pigments. However, several methods can be used in the identification of binding media such as micro-chemical, chemical and physical methods.展开更多
Due to local uneven heating during the welding process,the residual stress of the structure after welding affects the reliability of it.In order to ensure the reliability,it is of great significance to test the residu...Due to local uneven heating during the welding process,the residual stress of the structure after welding affects the reliability of it.In order to ensure the reliability,it is of great significance to test the residual stress distribution of the welded joint.It has always been the focus to find a simple and feasible method for residual stress testing to quickly and accurately obtain the residual stress distribution of welded joints.The mechanical measurement method has high measurement accuracy,convenient and easy operation,but it will cause certain damage to the components.Physical measurement method can avoid damage to components,but its test cost is usually high,and its measurement accuracy can also be affected by the material microstructure characteristics of welded components.Based on the advantages and disadvantages of these two residual stress test methods,a modal test method is proposed.This method is a non-destructive measurement method.Based on the mathematical relationship between the residual stress of the welded structure and the natural frequency(mathematical model),the natural frequency is measured through the modal test to calculate the residual stress quickly.However,it is difficult to establish a mathematical model with this method,and it is not suitable for realization.展开更多
A physical value mapping (PVM) algorithm based on finite element mesh from the stamped part in stamping process to the product is presented, In order to improve the efficiency of the PVM algorithm, a search way from...A physical value mapping (PVM) algorithm based on finite element mesh from the stamped part in stamping process to the product is presented, In order to improve the efficiency of the PVM algorithm, a search way from the mesh of the product to the mesh of the stamped part will be adopted. At the same time, the search process is divided into two steps: entire search (ES) and local search (LS), which improve the searching efficiency. The searching area is enlarged to avoid missing projection elements in ES process. An arc-length method is introduced in LS process. The validity is confirmed by the results of the complex industry-forming product.展开更多
The paper deals with some questions of important aspects of food safety and application of principles of food physics in the food sector. Food production and processing of quality food and safe food are today of prima...The paper deals with some questions of important aspects of food safety and application of principles of food physics in the food sector. Food production and processing of quality food and safe food are today of primary importance. Food production is based on the principles of Good Agricultural Practice (GAP), Good Manufactoring Practice (GMP) and Good Hygiene Practice (GHP). Recently, the industrial food processing is focused dominantly on the quality, and one of the basic requirements of the quality is the safety. There are different methods and techniques to produce safe food. The up-to-date food technologies and quality measurements (quality control and quality assurance) involve the application of different physical methods, e.g., high pressure, pulsing electrical field, nondestructive techniques, e.g., nuclear magnetic resonance (NMR), near infrared reflectance, near infrared transmittance (NIR-NIT), photo acoustic spectroscopy (PAS) and instrumental neutron activation analysis (INAA) for chemical composition determination, radiation techniques, nanofiltration and reverse osmosis (RO) as well. Using ionizing radiation (nuclear methods) and non-ionizing radiation technologies, it is possible to fulfill a lot of expectations: decrease of microbial contamination, improve of sensory properties, increase of storability, etc..展开更多
Solar forecasting is of great importance for ensuring safe and stable operations of the power system with increased solar power integration,thus numerous models have been presented and reviewed to predict solar irradi...Solar forecasting is of great importance for ensuring safe and stable operations of the power system with increased solar power integration,thus numerous models have been presented and reviewed to predict solar irradiance and power forecasting in the past decade.Nevertheless,few studies take into account the temporal and spatial resolutions along with specific characteristics of the models.Therefore,this paper aims to demonstrate a comprehensive and systematic review to further solve these problems.First,five classifications and seven pre-processing methods of solar forecasting data are systematically reviewed,which are significant in improving forecasting accuracy.Then,various methods utilized in solar irradiance and power forecasting are thoroughly summarized and discussed,in which 128 algorithms are elaborated in tables in the light of input variables,temporal resolution,spatial resolution,forecast variables,metrics,and characteristics for a more fair and comprehensive comparison.Moreover,they are categorized into four groups,namely,statistical,physical,hybrid,and others with relevant application conditions and features.Meanwhile,six categories,along with 30 evaluation criteria,are summarized to clarify the major purposes/applicability of the different methods.The prominent merit of this study is that a total of seven perspectives and trends for further research in solar forecasting are identified,which aim to help readers more effectively utilize these approaches for future in-depth research.展开更多
Silicon carbide (SiC) single crystal,which hasn’t melting point at normal pressu r e and sublimates at temperature above 2000℃,is a wide bandgap semiconductor.Si lic on carbide has more than 200 kinds of polytype.Am...Silicon carbide (SiC) single crystal,which hasn’t melting point at normal pressu r e and sublimates at temperature above 2000℃,is a wide bandgap semiconductor.Si lic on carbide has more than 200 kinds of polytype.Among these polytypes,3C SiC、6H SiC and 4H SiC are the most common ones,the band width of them are 2.4eV,3.0eV , an d 3.4eV,restpectively.For its high temperature tolerance and radiation resistanc e,silicon carbide semiconductor can be extensively used to fabricate the power d evi ces and electroluminescence devices operating at high power,high frequency and high radiation environments. The aim of this paper is to introduce our research results of the growth of larg e SiC single crystals by physical vapor transport method.The seed is SiC single crystal wafer with perfect (0001)Si face,which is chosen from the furnace growi ng the green abrasive material of SiC in industry.The source is green powder of SiC .The seed and the source are placed into the graphite crucible of a graphite res i stively heated vacuum furnace.The growth chamber is filled with the atmosphere o f pure araon.When the temperature of source rises to 2300℃,the crystal growth p ro ceeds.The rate of crystal growth is dependent on the growth temperature,the pres sure in furnace and the temperature gradient and distance between the seed and t h e source.Under the controlled growth conditions,the bulk SiC crystal with a diam eter of 40mm and a thickness of 15mm is obtained.The crystal appears to be n type electrical conductivity,the results of X ray Laue photography analysis indicat e that it is 6H SiC polytype.The defects of the crystal are also studied by many kinds of method.展开更多
The studies for raising potash feldspar utilization ratio by physical, biological and chemical methods are carried out in laboratory and the results are presented. It is shown that calcinatory and biological methods h...The studies for raising potash feldspar utilization ratio by physical, biological and chemical methods are carried out in laboratory and the results are presented. It is shown that calcinatory and biological methods have positive effects on conversion of K in potash feldspar into water-soluble form, but the conversion is low; chemical method can change most of insoluble potassium into available form, and might be significant in industry to some extent.展开更多
In order to improve the survivability of the aircraft,conceptual design and radar cross section(RCS) performance research are done. The CATIA software is used to design the 3D digital model of the shipborne early wa...In order to improve the survivability of the aircraft,conceptual design and radar cross section(RCS) performance research are done. The CATIA software is used to design the 3D digital model of the shipborne early warning aircraft, and some measures are taken to reduce the RCS characteristics of the early warning aircraft at the same time. Based on the physical optics method and the equivalent electromagnetic flow method,the aircraft's RCS characteristics and strength distribution characteristics are simulated numerically, and compared with the foreign advanced shipborne early warning aircraft. The simulation results show that under the X radar band, when the incident wave pitching angle is 0?, compared with the foreign advanced shipborne early warning aircraft, the forward RCS average value of the conceptual shipborne early warning aircraft is reduced to 24.49%, the lateral RCS average value is reduced to 5.04%, and the backward RCS average value is reduced to 39.26%. The research results of this paper are expected to provide theoretical basis and technical support for the conceptual design and the stealth design of the shipborne early warning aircraft.展开更多
Short-term climate reconstruction,i.e.,the reproduction of short-term(several decades)historical climatic time series based on the relationship between observed data and available longer-term reference data in a certa...Short-term climate reconstruction,i.e.,the reproduction of short-term(several decades)historical climatic time series based on the relationship between observed data and available longer-term reference data in a certain area,can extend the length of climatic time series and offset the shortage of observations.This can be used to assess regional climate change over a much longer time scale.Based on monthly grid climate data from a Coupled Model Inter-comparison Project phase 5(CMIP5)dataset for the period of 1850–2000,the Climatic Research Unit(CRU)dataset for the period of 1901–2000 and the observed data from 53 meteorological stations located in the Tianshan Mountains region(TMR)of China during the period of 1961–2011,we calibrated and validated monthly average temperature(MAT)and monthly accumulated precipitation(MAP)in the TMR using the delta,physical scaling(SP)and artificial neural network(ANN)methods.Performance and uncertainty during the calibration(1971–1999)and verification(1961–1970)periods were assessed and compared using traditional performance indices and a revised set pair analysis(RSPA)method.The calibration and verification processes were subjected to various sources of uncertainty due to the influence of different reconstructed variables,different data sources,and/or different methods used.According to traditional performance indices,both the CRU and CMIP5 datasets resulted in satisfactory calibrated and verified MAT time series at 53 meteorological stations and MAP time series at 20 meteorological stations using the delta and SP methods for the period of 1961–1999.However,the results differed from those obtained by the RSPA method.This showed that the CRU dataset produced a low degree of uncertainty(positive connection degree)during the calibration and verification of MAT using the delta and SP methods compared to the CMIP5 dataset.Overall,the calibrated and verified MAP had a high degree of uncertainty(negative connection degree)regardless of the dataset or reconstruction method used.Therefore,the reconstructed time series of MAT for the period of 1850(or 1901)–1960 based on the CRU and CMIP5 datasets using the delta and SP methods could be used for further study.The results of this study will be useful for short-term(several decades)regional climate reconstruction and longer-term(100 a or more)assessments of regional climate change.展开更多
基金Project(21905304)supported by the National Natural Science Foundation of ChinaProject(ZR2019BEM031)supported by the Natural Science Foundation of Shandong Province,ChinaProjects(18CX02158A,19CX05001A)supported by the Fundamental Research Funds for the Central Universities,China。
文摘MnO2/MnO cathode material with superior Zn^2+storage performance is prepared through a simple physical mixing method.The MnO2/MnO nanocomposite with a mixed mass ratio of 12:1 exhibits the highest specific capacity(364.2 mA·h/g at 0.2C),good cycle performance(170.4 mA·h/g after 100 cycles)and excellent rate performance(205.7 mA·h/g at 2C).Analysis of cyclic voltammetry(CV)data at various scan rates shows that both diffusioncontrolled insertion behavior and surface capacitive behavior contribute to the Zn2+storage performance of MnO2/MnO cathodes.And the capacitive behavior contributes more at high discharge rates,due to the short paths of ion diffusion and the rapid transfer of electrons.
基金the R&D project, titled " Creating a Marine Clay Matrix with Incineration Bottom Ash (IBA) for Land Reclamation " (Wu et al., 2014), under the Innovation for Environmental Sustainability (IES) Fund from National Environment Agency (NEA) of Singapore (ETO/CF/3/1)
文摘In this paper, the effectiveness, applicability and validity of chemicalephysical combined methods(CPCMs) for treatment of marine clay (MC) slurries were evaluated. The method CPCM1 combineschemical stabilization and vacuum preloading (VP), while CPCM2 is similar to CPCM1 but includes boththe application of surcharge and use of geo-bags to provide confinement during surcharge preloading.The key advantage of CPCM2 using geo-bags is that the surcharge can be immediately applied on thechemically stabilized slurries. Two types of geo-bags were investigated under simulated land filling anddyke conditions, respectively. The test results show that the shear strength (cu) of treated slurry byCPCM2 is generally much higher than that by CPCM1. Besides, the use of CPCM2 can significantly reducethe treatment time due to the short drainage paths created by geo-bags. Overall, CPCM2 allows fasterconsolidation and higher preloading that help to achieve higher mechanical properties of the stabilizedslurry. There are consistent relationships between cU and water content of slurries treated by CPCM2.Several important observations were also made based on comparisons of experimental data. 2015 Institute of Rock and Soil Mechanics, Chinese Academy of Sciences. Production and hosting byElsevier B.V. All rights reserved.
基金Supported by National Natural Science Foundation of China(Grant Nos.51175157,U124208)
文摘Physical parameters are very important for vehicle dynamic modeling and analysis.However,most of physical parameter identification methods are assuming some physical parameters of vehicle are known,and the other unknown parameters can be identified.In order to identify physical parameters of vehicle in the case that all physical parameters are unknown,a methodology based on the State Variable Method(SVM) for physical parameter identification of two-axis on-road vehicle is presented.The modal parameters of the vehicle are identified by the SVM,furthermore,the physical parameters of the vehicle are estimated by least squares method.In numerical simulations,physical parameters of Ford Granada are chosen as parameters of vehicle model,and half-sine bump function is chosen to simulate tire stimulated by impulse excitation.The first numerical simulation shows that the present method can identify all of the physical parameters and the largest absolute value of percentage error of the identified physical parameter is 0.205%;and the effect of the errors of additional mass,structural parameter and measurement noise are discussed in the following simulations,the results shows that when signal contains 30 d B noise,the largest absolute value of percentage error of the identification is 3.78%.These simulations verify that the presented method is effective and accurate for physical parameter identification of two-axis on-road vehicles.The proposed methodology can identify all physical parameters of 7-DOF vehicle model by using free-decay responses of vehicle without need to assume some physical parameters are known.
基金supported by International Rice Research Institute (IRRI)Research Center of Sub-Optimal Land (PUR-PLSO) Universitas Sriwijaya
文摘To analyze the effect of different lowland rice varieties and different cooking methods on physical and chemical characteristics of cooked rice. A factorial randomized block design with two factors was used and each combination of the factors was repeated three times. The first factor was rice variety(Ciherang and Ciliwung) and the second factor was the cooking method(stovetop, boiling and steaming, and rice cooker). Results showed that Ciherang and Ciliwung varieties were classified into slender grain rice type with yellowred color. The amylose content of Ciherang was classified as moderate, while the amylose content of Ciliwung classified as low. The most abundant amino acid contained in Ciherang and Ciliwung varieties was glutamic acid. Statistical analysis showed that cooking method had significant effects on texture, lightness, chroma, hue and moisture content of cooked rice. Rice cooked with liwet method had the lowest texture value, lowest lightness value, highest chroma value, and highest moisture content.
文摘Method of VSC (Voltage Shorted Compaction)can be used to determine the intrinsic temperature dependence ofconductivity ofpolycrystalline compaction. The experimental conditions and technical key for preparation of VSC device and its physical model as well as its applications in conducting polymers are discussed in detail.
文摘The titanium oxide (TiO2) nanotubes have attracted attention for their use in dye-sensitized solar cells as photoanode. In this study semiconducting cadmium sulfide (CdS) nanoparticles arc grown on top opened TiO2 nanotubes arrays by radio-frequency magnetron sputtering. X-ray diffraction, scanning electron mieroscopy, transmission electron microscopy and diffuse reflection spectra are used to study structural, morphological and optical properties of the CdS/TiO2 bilayer.
文摘Nanometer-sized metal clusters were prepared inside single crystalline MgO films by vacuum co-deposition of metals and MgO. The atomic structure was studied by high-resolution electron microscopy (HREM) and nm-area electron diffraction. The size of the clusters is ranging from 1 nm to 3 nm without those larger than 5 nm, and most of them have definite epitaxial orientations with the MgO matrix films. The character of the composite films is very much useful for the studies of various kinds of physical properties with anisotroPy. The physical properties such as electric transport, magnetic, optical absorption, sintering and catalytic ones were thus measured on the same samples analyzed by HREM by using high sensitivity apparatus with interest of clarifying the retationship between the atomic structure and physical properties
文摘Three directions of development of kinetic indentation methods.Physical-energetic analysis of the indentation force diagram according to ISO 14577.Physical theory and universal criterion for the macrohardness of a material.Model of the physical process,thermomechanical potential,function of the state of the kinetic macroindentation process.Method for determining the physical function and unit of measurement of the kinetic macrohardness of a material.The ratio of the values of the empirical(standard)and physical macrohardness of the material.Physical reason for the appearance of the size effect in empirical indentation methods.The principle of determining the standard value of physical macrohardness.
文摘Results of analytical studies of the physical properties of the function and number of empirical macrohardness based on the standard experimental force diagram of kinetic macroindentation by a sphere.An analytical comparison method and a criterion for the similarity of the physical and empirical macrohardness of a material are proposed.The physical properties of the hardness measurement process using the Calvert-Johnson method are shown.The physical reasons for the size effect when measuring macrohardness are considered.The universal physical unit and standard of macrohardness of kinetic macroindentation by a sphere is substantiated.
文摘Different questions may be raised during the course of analysis concerning in particular the characterization of materials used, their preparation and application techniques. The different methods used to identify the materials of mud brick, limestone, plaster, mortar and pigments, collected from different sites and periods from Egypt, in order to identify and characterize the materials, their structure, composition and their mineralogical compounds were: (Op) optical microscopy, which was used to examine and to identify the materials structures. Methods used in initial examination were: (1) (MCA): Micro-chemical analysis, to identify the nature of the materials and for water-soluble salts, to identify sulphates, chlorides, carbonates, nitrites and nitrates; (2) (SM): Standard methods of wet chemical analysis were used to identify the quantitative and qualitative nature of the, mud building, mortars and their mixtures; (3) (SEM & EDS): Analytical scanning electron microscope with energy dispersive X-ray analysis system was used to examine the micro-morphology and determine the chemical composition of the different materials; (4) (XRD & XRPD): X-ray diffraction to identify the mineralogical compound of the plaster, limestone, mortars and pigments used. From all the results obtained, it was possible to establish the nature of the mortars and their binders as well as some other inclusion. In addition to the identification of the stratigraphy of the layers applied in some samples, the examination and analysis gave details of the materials and the approximate ratio of the amount of additives used. Furthermore, the mineralogical analysis provided information on the main mineralogical phases present in the materials analyzed from the different periods.
文摘The identification of binding media presents a major difficulty in the investigation of painting techniques. The materials used in ancient times as a media for the pigments were varied, such as glues, gums and egg white. These adhesives were mixed with the pigments to adhere to the surface or to prepare the ground. This medium serves to protect the pigments more or less perfectly, from chemical and mechanical injury. Binding media determines the technique of painting. Artists' techniques used through the centuries differ more in the binding media than in the pigments used. They are all organic substances containing the same common elements, and in the small samples which can be removed from paintings, occur only in micro quantities, moreover, binding media undergo considerable degradation over long periods of time. In the examination of works of art, only very small specimens can be taken and, the proportion of binding medium to pigment being small, sensitive methods of analysis have to be adopted in an attempt to detect and identify the medium that may have been used. On the other hand, the use of such methods possesses the disadvantage that impurities present in the painting materials may also be detected and may lead to erroneous conclusions. There is no general microanalysis technique existed in the identification of binding media, and the materials commonly used as media are highly complex compared with the simple inorganic compounds employed as pigments. However, several methods can be used in the identification of binding media such as micro-chemical, chemical and physical methods.
基金Project was supported by the National Natural Science Foundation of China(Grant No.52165034)Science and Technology Programs of Inner Mongolia(Grant No.2020GG0301)+1 种基金Natural Science Foundation of Inner Mongolia Autonomous Region(Grant No.2019MS05061)Scientific Research Projects of Higher Education of Inner Mongolia Autonomous Region Institutions(Grant No.NJZY20066).
文摘Due to local uneven heating during the welding process,the residual stress of the structure after welding affects the reliability of it.In order to ensure the reliability,it is of great significance to test the residual stress distribution of the welded joint.It has always been the focus to find a simple and feasible method for residual stress testing to quickly and accurately obtain the residual stress distribution of welded joints.The mechanical measurement method has high measurement accuracy,convenient and easy operation,but it will cause certain damage to the components.Physical measurement method can avoid damage to components,but its test cost is usually high,and its measurement accuracy can also be affected by the material microstructure characteristics of welded components.Based on the advantages and disadvantages of these two residual stress test methods,a modal test method is proposed.This method is a non-destructive measurement method.Based on the mathematical relationship between the residual stress of the welded structure and the natural frequency(mathematical model),the natural frequency is measured through the modal test to calculate the residual stress quickly.However,it is difficult to establish a mathematical model with this method,and it is not suitable for realization.
基金This project is supported by National Natural Science Foundation ofChina(No.l9832020) and National Outstanding Youth Science Foundation ofChina(No.10125208).
文摘A physical value mapping (PVM) algorithm based on finite element mesh from the stamped part in stamping process to the product is presented, In order to improve the efficiency of the PVM algorithm, a search way from the mesh of the product to the mesh of the stamped part will be adopted. At the same time, the search process is divided into two steps: entire search (ES) and local search (LS), which improve the searching efficiency. The searching area is enlarged to avoid missing projection elements in ES process. An arc-length method is introduced in LS process. The validity is confirmed by the results of the complex industry-forming product.
文摘The paper deals with some questions of important aspects of food safety and application of principles of food physics in the food sector. Food production and processing of quality food and safe food are today of primary importance. Food production is based on the principles of Good Agricultural Practice (GAP), Good Manufactoring Practice (GMP) and Good Hygiene Practice (GHP). Recently, the industrial food processing is focused dominantly on the quality, and one of the basic requirements of the quality is the safety. There are different methods and techniques to produce safe food. The up-to-date food technologies and quality measurements (quality control and quality assurance) involve the application of different physical methods, e.g., high pressure, pulsing electrical field, nondestructive techniques, e.g., nuclear magnetic resonance (NMR), near infrared reflectance, near infrared transmittance (NIR-NIT), photo acoustic spectroscopy (PAS) and instrumental neutron activation analysis (INAA) for chemical composition determination, radiation techniques, nanofiltration and reverse osmosis (RO) as well. Using ionizing radiation (nuclear methods) and non-ionizing radiation technologies, it is possible to fulfill a lot of expectations: decrease of microbial contamination, improve of sensory properties, increase of storability, etc..
基金supported by National Natural Science Foundation of China(61963020,52037003)Key Science and Technology Project of Yunnan Province(202002AF080001)Science and Technology Project of State Grid Corporation of China(Research on Demand Strategies of Multi-source Interconnected Distribution Network and Diversified Power Consumption in Energy Internet).
文摘Solar forecasting is of great importance for ensuring safe and stable operations of the power system with increased solar power integration,thus numerous models have been presented and reviewed to predict solar irradiance and power forecasting in the past decade.Nevertheless,few studies take into account the temporal and spatial resolutions along with specific characteristics of the models.Therefore,this paper aims to demonstrate a comprehensive and systematic review to further solve these problems.First,five classifications and seven pre-processing methods of solar forecasting data are systematically reviewed,which are significant in improving forecasting accuracy.Then,various methods utilized in solar irradiance and power forecasting are thoroughly summarized and discussed,in which 128 algorithms are elaborated in tables in the light of input variables,temporal resolution,spatial resolution,forecast variables,metrics,and characteristics for a more fair and comprehensive comparison.Moreover,they are categorized into four groups,namely,statistical,physical,hybrid,and others with relevant application conditions and features.Meanwhile,six categories,along with 30 evaluation criteria,are summarized to clarify the major purposes/applicability of the different methods.The prominent merit of this study is that a total of seven perspectives and trends for further research in solar forecasting are identified,which aim to help readers more effectively utilize these approaches for future in-depth research.
文摘Silicon carbide (SiC) single crystal,which hasn’t melting point at normal pressu r e and sublimates at temperature above 2000℃,is a wide bandgap semiconductor.Si lic on carbide has more than 200 kinds of polytype.Among these polytypes,3C SiC、6H SiC and 4H SiC are the most common ones,the band width of them are 2.4eV,3.0eV , an d 3.4eV,restpectively.For its high temperature tolerance and radiation resistanc e,silicon carbide semiconductor can be extensively used to fabricate the power d evi ces and electroluminescence devices operating at high power,high frequency and high radiation environments. The aim of this paper is to introduce our research results of the growth of larg e SiC single crystals by physical vapor transport method.The seed is SiC single crystal wafer with perfect (0001)Si face,which is chosen from the furnace growi ng the green abrasive material of SiC in industry.The source is green powder of SiC .The seed and the source are placed into the graphite crucible of a graphite res i stively heated vacuum furnace.The growth chamber is filled with the atmosphere o f pure araon.When the temperature of source rises to 2300℃,the crystal growth p ro ceeds.The rate of crystal growth is dependent on the growth temperature,the pres sure in furnace and the temperature gradient and distance between the seed and t h e source.Under the controlled growth conditions,the bulk SiC crystal with a diam eter of 40mm and a thickness of 15mm is obtained.The crystal appears to be n type electrical conductivity,the results of X ray Laue photography analysis indicat e that it is 6H SiC polytype.The defects of the crystal are also studied by many kinds of method.
文摘The studies for raising potash feldspar utilization ratio by physical, biological and chemical methods are carried out in laboratory and the results are presented. It is shown that calcinatory and biological methods have positive effects on conversion of K in potash feldspar into water-soluble form, but the conversion is low; chemical method can change most of insoluble potassium into available form, and might be significant in industry to some extent.
基金supported by the National Natural Science Foundation of China(51375490)
文摘In order to improve the survivability of the aircraft,conceptual design and radar cross section(RCS) performance research are done. The CATIA software is used to design the 3D digital model of the shipborne early warning aircraft, and some measures are taken to reduce the RCS characteristics of the early warning aircraft at the same time. Based on the physical optics method and the equivalent electromagnetic flow method,the aircraft's RCS characteristics and strength distribution characteristics are simulated numerically, and compared with the foreign advanced shipborne early warning aircraft. The simulation results show that under the X radar band, when the incident wave pitching angle is 0?, compared with the foreign advanced shipborne early warning aircraft, the forward RCS average value of the conceptual shipborne early warning aircraft is reduced to 24.49%, the lateral RCS average value is reduced to 5.04%, and the backward RCS average value is reduced to 39.26%. The research results of this paper are expected to provide theoretical basis and technical support for the conceptual design and the stealth design of the shipborne early warning aircraft.
基金financially supported by the National Natural Science Foundation of China (41401050, 41761014)the Foundation of A Hundred Youth Talents Training Program of Lanzhou Jiaotong Universitythe Discovery Grant of Natural Sciences and Research Council of Canada
文摘Short-term climate reconstruction,i.e.,the reproduction of short-term(several decades)historical climatic time series based on the relationship between observed data and available longer-term reference data in a certain area,can extend the length of climatic time series and offset the shortage of observations.This can be used to assess regional climate change over a much longer time scale.Based on monthly grid climate data from a Coupled Model Inter-comparison Project phase 5(CMIP5)dataset for the period of 1850–2000,the Climatic Research Unit(CRU)dataset for the period of 1901–2000 and the observed data from 53 meteorological stations located in the Tianshan Mountains region(TMR)of China during the period of 1961–2011,we calibrated and validated monthly average temperature(MAT)and monthly accumulated precipitation(MAP)in the TMR using the delta,physical scaling(SP)and artificial neural network(ANN)methods.Performance and uncertainty during the calibration(1971–1999)and verification(1961–1970)periods were assessed and compared using traditional performance indices and a revised set pair analysis(RSPA)method.The calibration and verification processes were subjected to various sources of uncertainty due to the influence of different reconstructed variables,different data sources,and/or different methods used.According to traditional performance indices,both the CRU and CMIP5 datasets resulted in satisfactory calibrated and verified MAT time series at 53 meteorological stations and MAP time series at 20 meteorological stations using the delta and SP methods for the period of 1961–1999.However,the results differed from those obtained by the RSPA method.This showed that the CRU dataset produced a low degree of uncertainty(positive connection degree)during the calibration and verification of MAT using the delta and SP methods compared to the CMIP5 dataset.Overall,the calibrated and verified MAP had a high degree of uncertainty(negative connection degree)regardless of the dataset or reconstruction method used.Therefore,the reconstructed time series of MAT for the period of 1850(or 1901)–1960 based on the CRU and CMIP5 datasets using the delta and SP methods could be used for further study.The results of this study will be useful for short-term(several decades)regional climate reconstruction and longer-term(100 a or more)assessments of regional climate change.