The influence of raw powder particle size on the properties and microstructures of Ti (C, N)-based cermets has been studied. The conclusions are as follows: The microstructures of cermets were composed of two kinds of...The influence of raw powder particle size on the properties and microstructures of Ti (C, N)-based cermets has been studied. The conclusions are as follows: The microstructures of cermets were composed of two kinds of grains, the one with black cores surrounded by obvious rim structures, and the other whose cores were white with unconspicuous rim structures and adhesive phase. In the cermet made from fine powders, the amount of grains with white cores was much more than that in cermet made from coarse powders. In addition, their properties were also much better.展开更多
An intensive study of the particle size distribution of four commercial ultrafine alumina powders to obtain information about the powder agglomeration and relate them to the compactibility and the sinterability has be...An intensive study of the particle size distribution of four commercial ultrafine alumina powders to obtain information about the powder agglomeration and relate them to the compactibility and the sinterability has been made.展开更多
Effects of particle size (A:d50 = 336. 9 μm, B:d50 =123.5μm, C: d50=19.5 μm, D: dso=2.21μm) and content (1 wt% , 3 wt% , 5 wt% , 7 wt% ) of silicon powder on cold crushing strength (CCS) , pore size dis...Effects of particle size (A:d50 = 336. 9 μm, B:d50 =123.5μm, C: d50=19.5 μm, D: dso=2.21μm) and content (1 wt% , 3 wt% , 5 wt% , 7 wt% ) of silicon powder on cold crushing strength (CCS) , pore size distribution and microstructure of Al2O3 - ZrO2 - C refractories coked at high temperature had been investigated by means of mercury porosimeter, SEM, EDS, tic. The results indicated that particle size and content of silicon powder affected the cold crushing strength of coked specimens. It increased with the addition of silicon powder and its finer particle size. However, it decreased greatly when using too fine silicon powder. The particle size and content of silicon powder also impacted the phase evolution and microstructure of coked specimens, much more β-SiC whiskers constituted network structure and well distributed in specimens with reduction of their slenderness ratios when finer silicon powder was added, corresponding to that, the specimens' pore size distribution range became narrower with smaller pore diameter, but β-SiC whiskers were distributed sparsely and the specific pore volume of small pores increased when much finer powder was added. It was worthly mentioned that some nitride could form in specimens with addition of appropriate particle size and content of silicon powder.展开更多
Particle size fractionation by sieving is used to optimize antioxydant potential of natural substances. The aim of the present study was to evaluate particle size effects on antioxidant and hepatoprotective potential ...Particle size fractionation by sieving is used to optimize antioxydant potential of natural substances. The aim of the present study was to evaluate particle size effects on antioxidant and hepatoprotective potential of Eucalyptus camaldulensis essential oils (EO) on CCl<sub>4</sub>-induced hepatic damage in Wistar rats. Animals were daily orally treated with the EOs extracted by hydrodistillation from powder sieved at four particle sizes (≥355, 200 - 355, 100 - 200, ≤100 μm) and those of the unsieved powder at dose of 50 mg/Kg for 7 days. Compounds that are evaluated for these activities are hydrocarbons and oxygenated terpenes that were identified and quantified by GC/MS. Activities of enzymes markers of hepatocellular damage in serum and antioxidant enzymes in the liver homogenates were measured. In this research, EOs significantly prevented the increase in serum ALT and AST (p < 0.05), total cholesterol, triglyceride and LDL-cholesterol level in acute liver damage induced by CCl<sub>4</sub> and significant increase level of plasma HDL-cholesterol. Also, significantly (p < 0.05) decreased the extent of malondialdehyde (MDA) formation and elevated the activities of superoxide dismutase (SOD) and catalase (CAT) liver in comparison to negative control group. The best antioxidant and hepatoprotective activities were those of EOs from two fine powder fractions (≤100 μm and 100 - 200 μm) was correlated to their high concentration in oxygenated terpenes (70.9% and 46.4%, respectively), when compared to the large particles (200 - 355 μm and ≥355 μm, with 33.3% and 41.8%, respectively) and unsieved powder (37.4%).展开更多
基金the National Natural Science Foundation of China, the Doctoral EducationFoundation of China, the State Key Laboratory of Powde
文摘The influence of raw powder particle size on the properties and microstructures of Ti (C, N)-based cermets has been studied. The conclusions are as follows: The microstructures of cermets were composed of two kinds of grains, the one with black cores surrounded by obvious rim structures, and the other whose cores were white with unconspicuous rim structures and adhesive phase. In the cermet made from fine powders, the amount of grains with white cores was much more than that in cermet made from coarse powders. In addition, their properties were also much better.
文摘An intensive study of the particle size distribution of four commercial ultrafine alumina powders to obtain information about the powder agglomeration and relate them to the compactibility and the sinterability has been made.
文摘Effects of particle size (A:d50 = 336. 9 μm, B:d50 =123.5μm, C: d50=19.5 μm, D: dso=2.21μm) and content (1 wt% , 3 wt% , 5 wt% , 7 wt% ) of silicon powder on cold crushing strength (CCS) , pore size distribution and microstructure of Al2O3 - ZrO2 - C refractories coked at high temperature had been investigated by means of mercury porosimeter, SEM, EDS, tic. The results indicated that particle size and content of silicon powder affected the cold crushing strength of coked specimens. It increased with the addition of silicon powder and its finer particle size. However, it decreased greatly when using too fine silicon powder. The particle size and content of silicon powder also impacted the phase evolution and microstructure of coked specimens, much more β-SiC whiskers constituted network structure and well distributed in specimens with reduction of their slenderness ratios when finer silicon powder was added, corresponding to that, the specimens' pore size distribution range became narrower with smaller pore diameter, but β-SiC whiskers were distributed sparsely and the specific pore volume of small pores increased when much finer powder was added. It was worthly mentioned that some nitride could form in specimens with addition of appropriate particle size and content of silicon powder.
文摘Particle size fractionation by sieving is used to optimize antioxydant potential of natural substances. The aim of the present study was to evaluate particle size effects on antioxidant and hepatoprotective potential of Eucalyptus camaldulensis essential oils (EO) on CCl<sub>4</sub>-induced hepatic damage in Wistar rats. Animals were daily orally treated with the EOs extracted by hydrodistillation from powder sieved at four particle sizes (≥355, 200 - 355, 100 - 200, ≤100 μm) and those of the unsieved powder at dose of 50 mg/Kg for 7 days. Compounds that are evaluated for these activities are hydrocarbons and oxygenated terpenes that were identified and quantified by GC/MS. Activities of enzymes markers of hepatocellular damage in serum and antioxidant enzymes in the liver homogenates were measured. In this research, EOs significantly prevented the increase in serum ALT and AST (p < 0.05), total cholesterol, triglyceride and LDL-cholesterol level in acute liver damage induced by CCl<sub>4</sub> and significant increase level of plasma HDL-cholesterol. Also, significantly (p < 0.05) decreased the extent of malondialdehyde (MDA) formation and elevated the activities of superoxide dismutase (SOD) and catalase (CAT) liver in comparison to negative control group. The best antioxidant and hepatoprotective activities were those of EOs from two fine powder fractions (≤100 μm and 100 - 200 μm) was correlated to their high concentration in oxygenated terpenes (70.9% and 46.4%, respectively), when compared to the large particles (200 - 355 μm and ≥355 μm, with 33.3% and 41.8%, respectively) and unsieved powder (37.4%).