An in situ reduction method has been developed to fabricate metallic Ag nanoparticles inside the channels of mesoporous carbon CMK-3. This approach combines function of the CMK-3 surface by oxidation using HNO3 with t...An in situ reduction method has been developed to fabricate metallic Ag nanoparticles inside the channels of mesoporous carbon CMK-3. This approach combines function of the CMK-3 surface by oxidation using HNO3 with the subsequent absorption of Ag^+ The resultant nanocomposite materials were characterized by nitrogen adsorption, X-ray diffraction, Auger electron spectroscopy and transmission electron microscopy. Compared with the conventional impregnation method, our approach shows that Ag nanonarticles of 2-4 nm can be uniformlv incorporated into CMK-3.展开更多
基金the financial support of the National Natural Science Foundation of China(No.20573106)the Ministry of Science and Technology of China through the National Key Project of Fundamental Research.
文摘An in situ reduction method has been developed to fabricate metallic Ag nanoparticles inside the channels of mesoporous carbon CMK-3. This approach combines function of the CMK-3 surface by oxidation using HNO3 with the subsequent absorption of Ag^+ The resultant nanocomposite materials were characterized by nitrogen adsorption, X-ray diffraction, Auger electron spectroscopy and transmission electron microscopy. Compared with the conventional impregnation method, our approach shows that Ag nanonarticles of 2-4 nm can be uniformlv incorporated into CMK-3.