[Objectives]This study was conducted to establish a method for the simultaneous determination of caffeic acid, rutin, ononin, luteolin, and apigenin in Operculina turpethum(L.) S. Manso. [Methods]With ononin from O. t...[Objectives]This study was conducted to establish a method for the simultaneous determination of caffeic acid, rutin, ononin, luteolin, and apigenin in Operculina turpethum(L.) S. Manso. [Methods]With ononin from O. turpethum as the internal reference, the five components were separated by HPLC, and the contents of various components were calculated according to the relative correction factors of ononin with caffeic acid, rutin, luteolin, and apigenin. Meanwhile, the calculated results of quantitative analysis of multi-components by single marker(QAMS) were compared with the determined values of the external standard method. [Results] The linear relationship of the five components in their respective ranges was good(r=0.999 9). The average recovery was in the range of 97.48%-101.05%, and the RSD values were in the range of 1.04%-2.71%. The results obtained by QAMS were close to those obtained by the external standard method. [Conclusions] The method is accurate, stable and adaptable, and can be used for the determination of five flavonoids in O. turpethum.展开更多
In the SU(3) simple group model, the new neutral gauge boson Z' couples to pairs of SM fermions with couplings fixed in terms of the SM gauge couplings and depending only on the choice of the fermion embedding. In ...In the SU(3) simple group model, the new neutral gauge boson Z' couples to pairs of SM fermions with couplings fixed in terms of the SM gauge couplings and depending only on the choice of the fermion embedding. In this paper, we calculate the contributions of this new particle to the processes e^+e^-→l^+l^-, bb^-, and cc^- and study the possibility of detecting this new particle via these processes in the future high-energy linear e^+e^- collider(LC) experiments with √s= 500 GeV and £int= 340 fb^-1. We find that the new gauge boson Z' is most sensitive to the process e^+e^-→b^+b^-. As long as Mz,≤2 TeV , the absolute values of the relative correction parameter are larger than 5%. We calculate the forward-backward asymmetries and left-right asymmetries for the process e^+e^-→c^+c^-, with both the universal and anomaly-free fermion embeddings. Bounds on Z' masses are also estimated within 95% confidence level.展开更多
At the CERN large hadron collider (LHC), production of the Higgs boson in association with Z or W bosons provides a dramatic experimental signal for detecting the standard model (SM) Higgs boson. In this paper, we...At the CERN large hadron collider (LHC), production of the Higgs boson in association with Z or W bosons provides a dramatic experimental signal for detecting the standard model (SM) Higgs boson. In this paper, we consider the contributions of the left-right twin Higgs (LRTH) model to the processes qq' --~ Z(W)H. Our numerical results show that, in the favorable parameter spaces, the cross sections deviate distinctly from the predictions of the SM. The possible signals of the LRTH model can be detected via these processes at the LHC experiments.展开更多
As an advanced generation instrument of earth observation,small footprint full waveform light detection and ranging(LiDAR) technology has been widely used in the past few years.Decomposition and radiative correction i...As an advanced generation instrument of earth observation,small footprint full waveform light detection and ranging(LiDAR) technology has been widely used in the past few years.Decomposition and radiative correction is an important step in waveform data processing,it influences the accuracy of both information extraction and further applications.Based on a stepwise strategy,this study adopts Gaussian mixture model to approximate the LiDAR waveform.In addition to waveform decomposition,a relative correction model is proposed in this paper,the model considers the transmit pulses as well as the different of the travel path for implementing LiDAR waveform relative correction.Validation of the stepwise decomposition and relative correction model are carried out on LiDAR waveform acquired over Zhangye,China.The results indicate that stepwise decomposition identified the number of peaks in LiDAR waveforms,center position and width of each peak well.The relative radiometric correction also improves the similarity of waveforms which acquired at the same target.展开更多
Objective To develop a quantitative method for simultaneously determining multi-components in Rhei Radix et Rhizoma using one chemical reference substance.Methods The contents of multi-components were calculated by th...Objective To develop a quantitative method for simultaneously determining multi-components in Rhei Radix et Rhizoma using one chemical reference substance.Methods The contents of multi-components were calculated by the UV relative correction factors(RCFs)of chrysophanol,physcion,and rhein to emodin.Results The values of RCFs at 274 nm for rhein,chrysophanol,and physcion to emodin were 0.712,0.674,and 1.051.The calibration curves were linear over the ranges of 0.02-4.08,0.02-4.12,0.07-12.92,and 0.02-3.68μg/mL for rhein,emodin, chrysophanol,and physcion,respectively.The contents of emodin in 18 samples were determined by the external standard method,and the contents of the other three anthraquinone aglycones were calculated according to their RCFs. Conclusion No significant difference is found in comparison with the classical method,indicating that the RCFs have high reliability within their linear ranges and could be used in quality control of Rhei Radix et Rhizoma.The quantitative analysis of multi-component with a single marker is especially suitable for herbal medicines containing unstable or hard to be purified components as quality control markers.展开更多
In the present study, a method for the quantitative analysis of multi-components by single marker(QAMS) has been developed and validated for the simultaneous determination of echinacoside(ECH), tubuloside A, acteoside...In the present study, a method for the quantitative analysis of multi-components by single marker(QAMS) has been developed and validated for the simultaneous determination of echinacoside(ECH), tubuloside A, acteoside, isoacteoside, and2’-acetylacteoside in Cistanches Herba. ECH was used as the internal standard(IS) to obtain the relative correction factors(RCFs) of the other four phenylethanoid glycosides(PhGs);meanwhile, various influencing factors on RCFs were investigated under different conditions. The content of each component was calculated with RCF. The results were compared with those obtained by the external standard method(ESM) to verify the feasibility and accuracy of the established QAMS method. No significant difference was found in the quantitative results of 10 batches of Cistanches Herba between QAMS and ESM. The proposed QAMS method for simultaneous determination of PhGs in Cistanches Herba is accurate and feasible, providing an efficient and economical approach for the quality control of Cistanches Herba.展开更多
基金Supported by Guangxi Natural Science Foundation (2018GXNSFAA281138,2022JJA140749)Open Project for the Construction of First-class Disciplines in Guangxi (2019XK134)Key Laboratory of Extraction,Purification and Quality Analysis of Traditional Chinese Medicine in Colleges and Universities of Guangxi(GJKY[2014]6)。
文摘[Objectives]This study was conducted to establish a method for the simultaneous determination of caffeic acid, rutin, ononin, luteolin, and apigenin in Operculina turpethum(L.) S. Manso. [Methods]With ononin from O. turpethum as the internal reference, the five components were separated by HPLC, and the contents of various components were calculated according to the relative correction factors of ononin with caffeic acid, rutin, luteolin, and apigenin. Meanwhile, the calculated results of quantitative analysis of multi-components by single marker(QAMS) were compared with the determined values of the external standard method. [Results] The linear relationship of the five components in their respective ranges was good(r=0.999 9). The average recovery was in the range of 97.48%-101.05%, and the RSD values were in the range of 1.04%-2.71%. The results obtained by QAMS were close to those obtained by the external standard method. [Conclusions] The method is accurate, stable and adaptable, and can be used for the determination of five flavonoids in O. turpethum.
基金supported in part by a grant from Henan Institute of Science and Technology under Grant No.06040
文摘In the SU(3) simple group model, the new neutral gauge boson Z' couples to pairs of SM fermions with couplings fixed in terms of the SM gauge couplings and depending only on the choice of the fermion embedding. In this paper, we calculate the contributions of this new particle to the processes e^+e^-→l^+l^-, bb^-, and cc^- and study the possibility of detecting this new particle via these processes in the future high-energy linear e^+e^- collider(LC) experiments with √s= 500 GeV and £int= 340 fb^-1. We find that the new gauge boson Z' is most sensitive to the process e^+e^-→b^+b^-. As long as Mz,≤2 TeV , the absolute values of the relative correction parameter are larger than 5%. We calculate the forward-backward asymmetries and left-right asymmetries for the process e^+e^-→c^+c^-, with both the universal and anomaly-free fermion embeddings. Bounds on Z' masses are also estimated within 95% confidence level.
基金Supported by the National Natural Science Foundation of China under Grant Nos. 10975047 and 10979008
文摘At the CERN large hadron collider (LHC), production of the Higgs boson in association with Z or W bosons provides a dramatic experimental signal for detecting the standard model (SM) Higgs boson. In this paper, we consider the contributions of the left-right twin Higgs (LRTH) model to the processes qq' --~ Z(W)H. Our numerical results show that, in the favorable parameter spaces, the cross sections deviate distinctly from the predictions of the SM. The possible signals of the LRTH model can be detected via these processes at the LHC experiments.
基金supported by Major State Basic Research Development Program of China(Grant No.2007CB714406)National Key Technology R&D Program of China(Grant No.2008BAC34B03)
文摘As an advanced generation instrument of earth observation,small footprint full waveform light detection and ranging(LiDAR) technology has been widely used in the past few years.Decomposition and radiative correction is an important step in waveform data processing,it influences the accuracy of both information extraction and further applications.Based on a stepwise strategy,this study adopts Gaussian mixture model to approximate the LiDAR waveform.In addition to waveform decomposition,a relative correction model is proposed in this paper,the model considers the transmit pulses as well as the different of the travel path for implementing LiDAR waveform relative correction.Validation of the stepwise decomposition and relative correction model are carried out on LiDAR waveform acquired over Zhangye,China.The results indicate that stepwise decomposition identified the number of peaks in LiDAR waveforms,center position and width of each peak well.The relative radiometric correction also improves the similarity of waveforms which acquired at the same target.
文摘Objective To develop a quantitative method for simultaneously determining multi-components in Rhei Radix et Rhizoma using one chemical reference substance.Methods The contents of multi-components were calculated by the UV relative correction factors(RCFs)of chrysophanol,physcion,and rhein to emodin.Results The values of RCFs at 274 nm for rhein,chrysophanol,and physcion to emodin were 0.712,0.674,and 1.051.The calibration curves were linear over the ranges of 0.02-4.08,0.02-4.12,0.07-12.92,and 0.02-3.68μg/mL for rhein,emodin, chrysophanol,and physcion,respectively.The contents of emodin in 18 samples were determined by the external standard method,and the contents of the other three anthraquinone aglycones were calculated according to their RCFs. Conclusion No significant difference is found in comparison with the classical method,indicating that the RCFs have high reliability within their linear ranges and could be used in quality control of Rhei Radix et Rhizoma.The quantitative analysis of multi-component with a single marker is especially suitable for herbal medicines containing unstable or hard to be purified components as quality control markers.
基金National Key R&D Program of China(Grant Nos.2017YFC1702400,2018YFC1707300 and 2018YFC1707904)
文摘In the present study, a method for the quantitative analysis of multi-components by single marker(QAMS) has been developed and validated for the simultaneous determination of echinacoside(ECH), tubuloside A, acteoside, isoacteoside, and2’-acetylacteoside in Cistanches Herba. ECH was used as the internal standard(IS) to obtain the relative correction factors(RCFs) of the other four phenylethanoid glycosides(PhGs);meanwhile, various influencing factors on RCFs were investigated under different conditions. The content of each component was calculated with RCF. The results were compared with those obtained by the external standard method(ESM) to verify the feasibility and accuracy of the established QAMS method. No significant difference was found in the quantitative results of 10 batches of Cistanches Herba between QAMS and ESM. The proposed QAMS method for simultaneous determination of PhGs in Cistanches Herba is accurate and feasible, providing an efficient and economical approach for the quality control of Cistanches Herba.