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Effect of Saliva Contamination on Shear Bond Strength of Orthodontic Brackets When Using a Self-Etch Primer 被引量:3
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作者 毛靖 齐娟 《Journal of Huazhong University of Science and Technology(Medical Sciences)》 SCIE CAS 2005年第1期111-112,共2页
The effect of saliva contamination on the shear bond strength of orthodontic brackets, at various stages of the bonding procedure using a new self-etch primer was studied. The samples were divided into 4 groups accord... The effect of saliva contamination on the shear bond strength of orthodontic brackets, at various stages of the bonding procedure using a new self-etch primer was studied. The samples were divided into 4 groups according to 4 different enamel surface conditions: Group A: dry; Group B: saliva contamination before priming; Group C: saliva contamination after priming, and Group D: saliva contamination before and after priming. Stainless steel brackets were bonded in each test group with a light-cured composite resin (TransbondXT 3M). The shear bond strength was determined in the first 30 min after bonding. The analysis of variance indicated that the shear bond strengths of the 4 groups were significantly different (F=11.89, P<0.05). Tukey HSD tests indicated that contamination both before and after the application of the acid-etch primer resulted in a significantly lower (=4.6±1.7 MPa) shear bond strength than either the control group (=8.8±1.9 MPa) or the groups where contamination occurred either before (=7.9±2.0 MPa) or after (=6.9±1.5 MPa) the application of the primer. It was concluded that the new acid-etch primer could maintain adequate shear bond strength if contamination occurred either before or after the application of the primer. On the other hand, contamination both before and after the application of the primer could significantly reduce the shear bond strength of orthodontic brackets. 展开更多
关键词 SELF-ETCH SALIVA CONTAMINATION shear bond strength
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Isotropic shear bond strength behavior of superficial bovine dentin: A pilot study 被引量:1
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作者 Camila Sabatini Sebastiano Andreana 《Open Journal of Stomatology》 2013年第1期1-7,共7页
The aim of this pilot study was to evaluate the shear bond strength of superficial bovine incisor dentin in different crown regions. Bonding was performed to the incisal, middle and cervical thirds of superficial bovi... The aim of this pilot study was to evaluate the shear bond strength of superficial bovine incisor dentin in different crown regions. Bonding was performed to the incisal, middle and cervical thirds of superficial bovine coronal dentin (n = 20) with a two-step etch-and-rinse adhesive (Optibond Solo Plus) and resin composite (Z100). Shear bond strength was evaluated at 24 h and failure modes of representative specimens wereobserved with FE-SEM. Non-parametric Kruskal-Wallis test with a significance level of 0.05 was used for data analysis. Mean shear bond strength values for the incisal, middle, and cervical thirds were 36.9 (3.1), 42.6 (2.6), and 37.1 (2.1) respectively with no significant differences evidenced between the crown thirds (p = 0.19). Observation of the failure mode of representative specimens demonstrated that specimens with high bond strength values exhibited predominantly mixed-type failures whereas low strength specimens exhibited adhesive failures between the dentin and adhesive. The absence of significant differences in shear bond strength between crown thirds indicate that, regardless of tubule orientation, any crown region can be used when superficial bovine incisor dentin is used for shear bond strength testing. 展开更多
关键词 Adhesion shear bond strength BOVINE DENTIN ISOTROPIC Properties Failure Mode
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Shear bond strengths between alumina-toughened zirconia cores and veneering ceramics and their susceptibility to aging
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作者 Yong-Qi Zhao Li Jiang +3 位作者 Jing-Chao Zhang Yun-Mao Liao Jun-Jun Lu Wei Li 《Asian Pacific Journal of Tropical Medicine》 SCIE CAS 2012年第5期402-405,共4页
Objective:To evaluate the shear bond strength(SBS) between alumina-toughened zirconia (ATZ) cores and veneering ceramics,investigate the effect of aging in artificial saliva on SBS and compare it with that of yttria-s... Objective:To evaluate the shear bond strength(SBS) between alumina-toughened zirconia (ATZ) cores and veneering ceramics,investigate the effect of aging in artificial saliva on SBS and compare it with that of yttria-stabilized tetragonal zirconia polycrystals(Y-TZP).Methods:Bars of ATZ and Y-TZP were layered with veneering ceramics in accordance to the recommendation of the manufacturer.Half of each group(n = 10) was aged at 134℃.(under 2 bar pressure) in an autoclave for 48 h.Subsequently,all specimens were subjected to shear force in a universal testing machine.The interface and fractured surface of the specimens were evaluated using scanning electron microscopy and X-ray energy dispersive spectroscopy.Results:The initial mean SBS values in MPa±SD were 28.9±8.0 for ATZ and 26.2±7.6 for Y-TZP.After aging,the mean SBS values for ATZ and Y-TZP were 22.9±4.9 MPa and 22.8±6.9 MPa,respectively.Neither the differences between the SBS values of the ATZ and Y-TZP groups nor the influence of aging on all groups were statistically significant.Conclusions:The SBS between the ATZ core and the veneering ceramics was not affected by aging.The SBS of ATZ to veneering ceramics was not significantly different compared with that of Y-TZP. 展开更多
关键词 shear bond strength ZIRCONIA ALUMINA Veneering CERAMICS AGING
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Comparison of Two Methods of Chlorhexidine Application of Shear Bond Strength Degradation between Composite Resin and Dentin
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作者 Endang Suprastiwi Itja Risanti Nila Kesuma Djauharie 《Open Journal of Stomatology》 2015年第8期211-216,共6页
Background: Chlorhexidine could have effect on shear bond strength of composite resin-dentin. Objective: The purpose of this study is to compare two methods of chlorhexidine application of shear bond strength degradat... Background: Chlorhexidine could have effect on shear bond strength of composite resin-dentin. Objective: The purpose of this study is to compare two methods of chlorhexidine application of shear bond strength degradation between composite resin and dentin. Methods: Thirty samples of dentin were taken from the crown of premolars and then divided into three groups (n = 10). Group 1 were applied bonding without chlorhexidine, group 2 were applied with liquid chlorhexidine and followed by bonding, group 3 were applied bonding which contains chlorhexidine. Each group was divided into two sub-groups (n = 5): the group with and without 10% NaOCl immersion for one hour. Then, 4 samples in each sub-group were used to measure shear bond strength using Universal Testing Machine, and 1 sample was examined with Scanning Electron Microscope (SEM). Data were analyzed using SPSS 17 by Mann-Whitney and Kruskal Wallis test. Results: The highest mean shear bond strength without 10% NaOCl immersion was in group 1, while the highest mean with 10% NaOCl immersion was in group 3. Significant differences occurred between the groups 1 and 2, groups 2 and 3. Conclusion: Method of using bonding contains chlorhexidine can increase and inhibit degradation shear bond strength between composite resin and dentin. 展开更多
关键词 CHLORHEXIDINE Composite RESIN DENTIN shear bond strength
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The Shear Bond Strengths of Composite Bonded to Dentine Following Treatment with Two Dentine Occluding Desensitizing Toothpastes
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作者 Shivaughn Marchan Daniel White +3 位作者 Jessica Pruszynski Tichard Manwah Vishala Bassaw William Smith 《Open Journal of Stomatology》 2014年第3期121-125,共5页
Aim: This study determined whether prior brushing with desensitizing toothpastes (Sensodyne Rapid Relief and Colgate Pro-Relief) affected the shear bond strengths of composite to dentine surfaces after appropriate use... Aim: This study determined whether prior brushing with desensitizing toothpastes (Sensodyne Rapid Relief and Colgate Pro-Relief) affected the shear bond strengths of composite to dentine surfaces after appropriate use of two different dentine bonding agents (SingleBond and PQ-1). Materials and Methods: Sixty caries free molar teeth were cleaned, disinfected and embedded in individual cylinders of polymethylmethracyrlate. The occulsal surfaces were flattened to expose dentine and finished down with 600 grit silicone carbide paper. The teeth were randomly divided into six groups of 10 teeth each. Two groups served as control where dentine surfaces were brushed with pumice slurry. Of the remaining 4 groups, 2 groups were brushed with Sensodyne Rapid Relief and 2 groups brushed with Colgate Pro-Relief. The dentine surfaces were brushed to simulate 2 weeks of twice-daily toothpaste use. The specimens in each of the control groups and experimental groups were subjected to dentine bonding procedures (Single Bond or PQ-1), and application of hybrid composite resin (Z-250) according to the manufacturer’s instructions. A universal material testing machine, with a cross head speed of 0.05 mm/min was used to determine shear bond strengths. Results: Mean shear bond strengths ranged from 5.71 MPa (Colgate pretreatment, composite bonded with Single Bond) to 9.07 MPa (Sensodyne pretreatment, composite bonded with Single Bond). Results showed neither of the main effects, of toothpaste type or bonding agent were significant (p > 0.05) but their interaction was (F = 4.25, p = 0.02). Post hoc analysis showed that teeth brushed with the Sensodyne group, treated with the unfilled dentine bonding agent had a significantly higher bond strength than those treated with the filled dentine bonding agent. Conclusion: The desensitizing toothpastes that use the mechanism of occlusion of open dentinal tubules in the preliminary management of tooth sensitivity should not have an adverse effect on future restorative treatment modalities. 展开更多
关键词 shear bond strengths Desensitizing Toothpastes
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Influence of holding time on microstructure and shear strength of Mg alloy/steel joint diffusion bonded with Zn-5Al interlayer 被引量:5
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作者 赵丽敏 于海 冉伟锋 《China Welding》 EI CAS 2017年第1期1-8,共8页
The diffusion bonding of AZ31B Mg alloy and Q235 steel was investigated with a Zn-5Al alloy as interlayer and under different holding time ranging from 3 to 1 200 s. The microstructure and phase compositions of bonded... The diffusion bonding of AZ31B Mg alloy and Q235 steel was investigated with a Zn-5Al alloy as interlayer and under different holding time ranging from 3 to 1 200 s. The microstructure and phase compositions of bonded joints were characterized by scanning electron microscopy( SEM),energy dispersive spectrometer( EDS) and X-ray diffraction( XRD)methods. The shear strength of Mg alloy/steel joints was measured by tensile tester. It was found that the microstructure of bonded joints evolved dramatically along with the prolongation of holding time. Under the holding time of 3 s,the main part of joint was composed of MgZn_2 phase and dispersed Al-rich solid solution particles. When increased the holding time more than 60 s,the excessive solution of AZ31B into the interfacial reaction area led to the formation of coarse phase and eutectic microstructure,and also the complex Fe-Al and Mg-Al-Zn IMCs at transition layer closed to Q235 steel side. According to the tensile testing characterizations,the joints obtained under holding time of 3 s exhibited the best shear strength of 84 MPa,and the fracture occurred at the intermediary part of joint where the flexible Al-rich solid solution particles could help to impede the microcrack propagations. With prolonging the holding time to 600 s,the shear strength of joints was deteriorated enormously and the fracture position was shifted to the transition layer part closed to Q235 steel. 展开更多
关键词 diffusion bondING MICROSTRUCTURE shear strength transition layer
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Impact of Dentinal Tubule Orientation on Dentin Bond Strength
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作者 Jing GUO Li-ping WANG +2 位作者 Jia ZHU Jian YANG Hong-shui ZHU 《Current Medical Science》 SCIE CAS 2018年第4期721-726,共6页
This study aimed to determine the impact of dentinal tubule orientation on dentin bond strength to provide a reference for clinical cavity preparation in resin-bonded restoration. Patients aged 13-16 years were select... This study aimed to determine the impact of dentinal tubule orientation on dentin bond strength to provide a reference for clinical cavity preparation in resin-bonded restoration. Patients aged 13-16 years were selected, including 18 males and 21 females. Forty-eight human maxillary first premolars from orthodontic extractions were chosen to prepare the test models with the dentinal tubule orientations perpendicular and parallel to the bonding substrate. The test models in the vertical and parallel groups were divided into three groups: total-etching with 20% phosphoric acid, total-etching with 35% phosphoric acid and self-etching, with the dentinal tubule surfaces bonded with composite resin blocks in each group. After the standard test models of dentinal tubule-composite resin blocks were placed in distilled water and stored at 37℃ for 24 h, shearing tests were performed using a universal material testing machine at a crosshead speed of 0.5 mm/min. The bond strength values in the vertical group were 19.33+1.59 MPa for the 20% phosphoric acid group, 21.39±2.34 MPa for the 35% phosphoric acid group, and 16.88±1.54 MPa for the self-etching group. The bond strength values in the parallel group were 24.53±1.99 MPa for the 20% phosphoric acid group, 25.16+2.88 MPa for the 35% phosphoric acid group, and 20.83±1.99 for the self-etching group. After using same total-etching adhesive, the shear bond strength of the parallel group was higher than that of the vertical group, and the difference was statistically significant (P〈0.05). Regardless of vertical group or parallel group, the difference in the bond strength value between the total-etching groups and the self-etching group was statistically significant (P〈0.05). It was concluded that the dentin bonding substrate which was parallel to the direction of the dentin tubule achieved an improved bond strength; the total-etching adhesives achieved higher bond strengths in dentin bond than the self-etching adhesives. 展开更多
关键词 dentinal tubule orientation bonding substrate shear bond strength
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Bond Strength of Orthodontic Bracket Cement Using a Bleaching Light for Curing
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作者 Yoav Shapinko Iro Eleftheriadi +4 位作者 Nir Shpack Moshe Davidovitch Elias Bitsanis Shlomo Matalon Tamar Brosh 《Open Journal of Stomatology》 2018年第3期81-89,共9页
Aim: To investigate the bond strengths achieved by using a Bleaching Curing Light (BCL) to polymerize orthodontic bonding cement. Material and Methods: 160 anterior bovine teeth were used to form 20 average sized huma... Aim: To investigate the bond strengths achieved by using a Bleaching Curing Light (BCL) to polymerize orthodontic bonding cement. Material and Methods: 160 anterior bovine teeth were used to form 20 average sized human dental arches, and distributed into 2 groups according to which light curing method used: Group 1: BCL for 40 seconds, or Group 2: LED for 10 seconds. After storage in a controlled environment, Shear Bond Strength (SBS) and Adhesive Remnant Index (ARI) were determined. Results: Group 1 showed significantly lower SBS in the most posterior (first molar) position of the dental arch, (Group 1: 0.7 ± 1.0 MPa, Group 2: 2.9 ± 1.7 MPa, p Conclusion: Simultaneous full-arch curing of orthodontic bracket cement using a BCL is clinically acceptable in all but the most posterior locations along the dental arch. 展开更多
关键词 BLEACHING Light-Cure ORTHODONTIC bondING shear bond strength
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Numerical Determination of Shear Strength of Steel Reinforced Concrete Column Strengthened by CFRP Sheets 被引量:1
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作者 王铁成 余流 王立军 《Transactions of Tianjin University》 EI CAS 2003年第1期58-62,共5页
The earthquake resistant property of reinforced concrete members depends on the interaction between reinforcing bars and surrounding concrete through bond to a large degree. In this paper a general system aimed at dea... The earthquake resistant property of reinforced concrete members depends on the interaction between reinforcing bars and surrounding concrete through bond to a large degree. In this paper a general system aimed at dealing with the failure analysis of reinforced concrete columns strengthened with carbon fiber reinforced plastic (CFRP) sheets including bond slip of the anchored reinforcing bars at the foot of the columns is presented. It is based on the yield design theory with a mixed modeling of the structure, according to which the concrete material is treated as a classical two dimensional continuum, whereas the longitudinal reinforcing bars are regarded as one dimensional rods including bond slip at the foot of the columns. In shear reinforced zones both the shear CFRP sheets and transverse reinforcing bars are incorporated in the analysis through a homogenization procedure and they are only in tension. The approach is then implemented numerically by means of the finite element formulation. The numerical procedure produces accurate estimates for the loading carrying capacity of the shear members taken as an illustrative application by correlation with the experimental results, so the proposed approach is valid. 展开更多
关键词 钢筋混凝土柱 碳纤维增强塑料板 玻璃钢板 剪切强度 数值计算 地震激励
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Full-scale pullout tests of rock anchors in a limestone quarry focusing on bond failure at the anchor-grout and grout-rock interfaces
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作者 Bjarte Grindheim Charlie CLi Are Håvard Høien 《Journal of Rock Mechanics and Geotechnical Engineering》 SCIE CSCD 2023年第9期2264-2279,共16页
Rock anchors are a common safety measure for stabilising large-scale infrastructure,such as bridge towers,retaining walls,rock slopes and windmills.There are four principal failure modes for rock anchors:(a)tensile fa... Rock anchors are a common safety measure for stabilising large-scale infrastructure,such as bridge towers,retaining walls,rock slopes and windmills.There are four principal failure modes for rock anchors:(a)tensile failure of the steel anchor,(b)anchor-grout interface failure,(c)grout-rock interface failure,and(d)rock mass uplift.Field tests were performed in a limestone quarry.These tests were designed to test failure modes B and C through pullout.In the tests of failure mode B,the shear stress on the anchor-grout interface is the largest at the top of the grout column and attenuates towards the distal end for small loads.The shear stress becomes uniformly distributed when the applied load is approximately 50%of the ultimate pullout load.The anchors designed to test failure mode C were installed with an endplate and had a higher toughness than the straight bar anchors.The shear stress on the grout-rock interface is the largest at the endplate and attenuates upward before slip starts along the interface.When the ultimate pullout load is reached,and the grout column starts to slip,the shear stress is approximately constant.The bond shear strength on the anchor-grout interface was approximately 20%of the uniaxial compressive strength of the grout,and the bond strength of the grout-rock interface was around 5%for that of the grout.The grout-rock interface is likely determined by whichever is weaker,the grout or the rock. 展开更多
关键词 Rock anchor Load transfer shear stress distribution bond shear strength Field test
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不同清洁方法对高透氧化锆粘接强度和表面润湿性的影响
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作者 焦纪兰 叶心仪 +4 位作者 邓璐 江辉 李霄夏 曾利伟 谭建国 《上海口腔医学》 CAS 2024年第1期36-39,共4页
目的:研究不同清洁方法对唾液污染的高透氧化锆与自粘接树脂水门汀间剪切粘接强度和表面润湿性的影响。方法:制备80个高透氧化锆试件,随机分为5组(n=16),即对照组(无污染处理)、75%乙醇组、喷砂组、清洁剂组和大气压冷等离子体处理组等... 目的:研究不同清洁方法对唾液污染的高透氧化锆与自粘接树脂水门汀间剪切粘接强度和表面润湿性的影响。方法:制备80个高透氧化锆试件,随机分为5组(n=16),即对照组(无污染处理)、75%乙醇组、喷砂组、清洁剂组和大气压冷等离子体处理组等。测量表面接触角,测试剪切粘接强度,观察断裂模式。采用SPSS 26.0软件包对数据进行统计学分析。结果:大气压冷等离子体组的接触角最小(P<0.05);喷砂组、清洁剂组及大气压冷等离子体组的剪切粘接强度与对照组相比,无统计学差异(P>0.05),但均显著大于75%乙醇组(P<0.05);大气压冷等离子体组混合断裂模式增多。结论:喷砂、清洁剂及大气压冷等离子体清洁唾液污染的高透氧化锆,可获得与未被唾液污染前相当的粘接强度;大气压冷等离子体可显著提高高透氧化锆的表面润湿性。 展开更多
关键词 氧化锆 唾液污染 大气压冷等离子体 表面润湿性 粘接强度
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两种复合树脂与牙本质剪切粘接强度的比较
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作者 潘悦萍 李婷婷 《口腔材料器械杂志》 2024年第2期107-110,共4页
目的在离体牙牙本质上涂布粘接剂后分别予以声波技术充填Sonicfill树脂及分层充填P60树脂,评估应用两种复合树脂与牙本质的剪切粘接强度。方法选择因牙周病拔除的磨牙40颗,制成40个牙本质试件,随机分为2组。A组为Sonicfill树脂组,B组为... 目的在离体牙牙本质上涂布粘接剂后分别予以声波技术充填Sonicfill树脂及分层充填P60树脂,评估应用两种复合树脂与牙本质的剪切粘接强度。方法选择因牙周病拔除的磨牙40颗,制成40个牙本质试件,随机分为2组。A组为Sonicfill树脂组,B组为P60树脂组。每组涂布粘接剂后,A组采用声波技术充填树脂,B组采用分层技术充填树脂。经过循环温度为5℃及55℃的冷热循环疲劳试验,每个循环为3 min,共循环500次后,测试2组的剪切粘接强度(Shear Bond Strength,SBS)。结果A组的SBS为(10.32±1.13)MPa,B组的SBS为(8.43±0.98)MPa,两者差别有统计学意义(P<0.05)。结论运用声波技术的Sonicfill树脂充填体相比采用分层充填的P60树脂拥有更高的剪切粘接强度。因此,在修复过程中使用声波充填技术不亚于传统分层充填树脂,且临床操作时间更短。 展开更多
关键词 剪切粘接强度 复合树脂 声波技术充填
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新旧混凝土结合面剪切强度参数分析和计算研究
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作者 张望喜 叶缘 +2 位作者 张晨 林泽宇 陈乐球 《湖南大学学报(自然科学版)》 EI CAS CSCD 北大核心 2024年第1期112-125,共14页
新旧混凝土结合面的抗剪强度是装配式混凝土结构和混凝土结构加固等领域重点关注的问题.基于搜集、整理的新旧混凝土结合面(以下简称结合面)的剪切试验数据库(含439个试件),对GB 50010―2010、ACI 318―19、Eurocode 2、PCI7th四个规范... 新旧混凝土结合面的抗剪强度是装配式混凝土结构和混凝土结构加固等领域重点关注的问题.基于搜集、整理的新旧混凝土结合面(以下简称结合面)的剪切试验数据库(含439个试件),对GB 50010―2010、ACI 318―19、Eurocode 2、PCI7th四个规范所给结合面抗剪建议计算式进行对比分析.结果表明:在各参数的影响下,ACI结果的保证率表现最好,而Eurocode 2计算强度的拟合效果最好;在结合面宽度达到300~400 mm时,GB 50010―2010的表现最好,但安全富余均较低,相对误差最大达到9倍.对数据库进行参数分析,发现结合面剪切强度τ_(exp)存在尺寸效应,与结合面的沿剪切方向尺寸关联较大;且τ_(exp)与夹紧力ρfy有较好的相关性.基于分析结果,根据叠加计算理论,对计算式提出建议和修正:分析引入尺寸效应系数β;同时修正了摩擦系数μ;应用了数据库拟合的销栓力分段函数,极大值为6.6 MPa.经对比验算证明,修正计算式在有无插筋及各种粗糙度情况下的误差最小,拟合效果最好,可为工程应用提供参考. 展开更多
关键词 新旧混凝土结合面 剪切强度 规范对比 参数分析 公式修正
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固位钉对All-Bond2粘结强度的影响 被引量:2
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作者 马琦 潘洁 +1 位作者 孙智辉 田立坤 《现代口腔医学杂志》 CAS CSCD 2001年第1期27-28,共2页
目的 探讨固位钉对All-Bond 2粘结强度的影响。方法 应用All-Bond 2为粘结剂 ,将 15个离体牙随机分为 3组 ,测试加金属固位钉前后光敏复合树脂粘结离体牙表面的剪切粘结力 ,分析固位钉的作用。结果 实验I组 (不加固位钉 )的剪切粘结... 目的 探讨固位钉对All-Bond 2粘结强度的影响。方法 应用All-Bond 2为粘结剂 ,将 15个离体牙随机分为 3组 ,测试加金属固位钉前后光敏复合树脂粘结离体牙表面的剪切粘结力 ,分析固位钉的作用。结果 实验I组 (不加固位钉 )的剪切粘结力为 2 5 .87+ 5 .10Kgf;实验II组和实验III组是将固位钉攻入牙本质内 ,深度分别为 2mm和 3mm ,其剪切粘结力分别为 :2 5 .77+ 3 .72Kgf及 2 6 .2 6 + 3.14Kgf。经统计学处理 ,三组间无显著性差异。结论 复合树脂与牙齿间的粘结强度与加或不加固位钉无相关性 ; 展开更多
关键词 粘结剂 固位钉 剪切粘结力 All-bond2 复合树脂 牙体修复
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5种流体树脂与牙釉质粘接性能的对比研究
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作者 郭欣欣 苗振云 +2 位作者 荆雪 马思雨 李涛 《口腔医学》 CAS 2024年第3期192-199,共8页
目的通过比较Beautifil Flow Plus F00、FiltekTM Z350 XT、SDR、Tetric®N-Flows、Constic 5种流体树脂与牙釉质的粘接性能,为流体树脂的临床选择提供参考。方法选择因正畸拔除的成人离体前磨牙50颗,将离体牙随机分为5组(n=10),分... 目的通过比较Beautifil Flow Plus F00、FiltekTM Z350 XT、SDR、Tetric®N-Flows、Constic 5种流体树脂与牙釉质的粘接性能,为流体树脂的临床选择提供参考。方法选择因正畸拔除的成人离体前磨牙50颗,将离体牙随机分为5组(n=10),分别为F00组、Z350组、SDR组、Tetric组、Constic组,每组之间互为平行对照组。每颗离体牙颊侧中1/3磨除厚度为0.5 mm牙釉质,以直径为3 mm的圆形形态作为粘接面,每种树脂制作直径和长度均为3 mm圆柱形树脂试件10个,与预备好的牙釉质面进行粘接,自凝树脂进行包埋。将试件进行3000次冷热循环交替实验和37℃恒温水浴24 h实验后,进行剪切强度测试,记录数据;切断的粘接界面在扫描电镜下观察。结果F00组的剪切强度为(18.39±2.93)MPa、Z350组的剪切强度(11.03±1.55)MPa、SDR组的剪切强度为(12.77±1.55)MPa、Tetric组的剪切强度为(15.25±1.88)MPa、Constic组的剪切强度为(12.79±2.78)MPa,对所得数据进行ANOVA检验和SNK检验后得出,F00组的剪切强度显著高于其他4组(Z350组、SDR组、Tetric组、Constic组)(P<0.05);Tetric组的剪切强度显著高于其余3组(Z350组、SDR组、Constic组)(P<0.05);Z350组、SDR组、Constic组3组之间的剪切强度没有显著性差异(P>0.05)。结论5种流体树脂中Beautifil Flow Plus F00流体树脂粘接性能最高,Tetric®N-Flow流体树脂次之,FiltekTM Z350 XT、SDR、Constic这3种流体树脂粘接性能较低。 展开更多
关键词 流体树脂 剪切强度 粘接性能
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工艺参数对5A90铝锂合金扩散连接质量的影响规律
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作者 康良炜 蒋少松 +4 位作者 侯晨睿 韩政 邢宇涵 赵文辉 孙甜 《塑性工程学报》 CAS CSCD 北大核心 2024年第5期55-63,共9页
采用金相显微镜、扫描电镜和真空热压烧结炉等设备探究了5A90铝锂合金的扩散连接工艺。结果表明,在扩散连接过程中,随着温度的升高和保温时间的延长,试样中白色强化相增多,空洞减少,焊合度明显提高。剪切强度随扩散连接温度的提高而降低... 采用金相显微镜、扫描电镜和真空热压烧结炉等设备探究了5A90铝锂合金的扩散连接工艺。结果表明,在扩散连接过程中,随着温度的升高和保温时间的延长,试样中白色强化相增多,空洞减少,焊合度明显提高。剪切强度随扩散连接温度的提高而降低,随保温时间的减少而降低,进而使连接强度降低;这主要是由于扩散温度及保温时间对原子扩散过程产生影响。试样界面15μm的粗糙度避免了氧化铝薄膜的过厚,并保证了扩散连接时接头处的局部接触,使氧化膜破裂,得到最佳接头质量。典型参数下的断裂发生在母材中,以穿晶断裂为主要断裂形式,证明了5A90铝锂合金扩散连接接头的可靠性。通过对比分析,得到扩散连接最佳工艺参数为:连接温度540℃、保温2.5 h、表面粗糙度15μm。 展开更多
关键词 5A90铝锂合金 扩散连接 剪切强度 力学性能
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超高性能混凝土-石材界面黏结性能试验研究
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作者 黄伟 黄雅莹 +3 位作者 陈雪莉 吴应雄 郑新颜 张恒春 《硅酸盐通报》 CAS 北大核心 2024年第2期397-406,417,共11页
超高性能混凝土(UHPC)加固修复既有石结构中,UHPC与石材之间优异的黏结性能是保证加固效果的关键。因此,为探究UHPC-石材界面的黏结性能,通过劈裂抗拉试验和双L型剪切试验,考察不同界面处理方式对UHPC-石材界面黏结性能的影响。结果表明... 超高性能混凝土(UHPC)加固修复既有石结构中,UHPC与石材之间优异的黏结性能是保证加固效果的关键。因此,为探究UHPC-石材界面的黏结性能,通过劈裂抗拉试验和双L型剪切试验,考察不同界面处理方式对UHPC-石材界面黏结性能的影响。结果表明,UHPC-石材界面破坏模式主要分为三种,其中发生模式C破坏(石材UHPC破坏)时界面黏结强度最大。界面键槽处理方式能显著提高UHPC-石材界面黏结强度、界面剪切刚度,且在改变破坏形态的同时有效提升试件的延性,当键槽深度为20 mm时,试件表现出较好的界面黏结性能。另外,试件剪切荷载-位移曲线包含滑移前阶段和滑移后阶段,凿毛试件在滑移后阶段没有经历塑性变形。相同界面处理方式下,UHPC-石材的界面抗剪强度与界面劈裂抗拉强度呈正相关关系。 展开更多
关键词 UHPC-石材界面 劈裂抗拉试验 剪切试验 键槽处理 黏结强度 界面剪切刚度
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应用于三维集成的金铟键合技术研究
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作者 栾华凯 侯芳 +2 位作者 孙超 吴焱 禹淼 《固体电子学研究与进展》 CAS 2024年第2期157-160,172,共5页
由于埋置芯片耐受温度的限制,圆片级低温键合技术是MEMS三维集成的关键工艺之一。金属In凭借自身熔点低而金属间化合物(Intermetallic compound, IMC)熔点高且性质稳定的特点,使得Au-In固液扩散键合法成为颇具前景的低温键合技术之一。... 由于埋置芯片耐受温度的限制,圆片级低温键合技术是MEMS三维集成的关键工艺之一。金属In凭借自身熔点低而金属间化合物(Intermetallic compound, IMC)熔点高且性质稳定的特点,使得Au-In固液扩散键合法成为颇具前景的低温键合技术之一。本文采用Au-In二元共晶化合物进行圆片级低温键合,在键合衬底上先后制备了0.4μm的SiO/SiN介质层、3.5μm的Au层和1.7μm的In层,然后分别研究了先预加热键合极板再贴合圆片和先贴合再加热两种键合方式。电性能测试、An/In组分分析和剪切试验结果表明:先贴合再加热的键合样品芯片形成了性质稳定的IMC组分,具有良好的电学互连特性稳定性,且剪切强度达到100 MPa。一定样本容量的实验结果证明隔绝键合前Au-In的相互扩散能够有效增强键合的可靠性。 展开更多
关键词 低温键合 金铟共晶 固液扩散键合 剪切强度
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CNT toughened aluminium and CFRP interface for strong adhesive bonding 被引量:1
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作者 Gang Han Bo Tan +3 位作者 Fei Cheng Binhua Wang Yee-Kwong Leong Xiaozhi Hu 《Nano Materials Science》 EI CAS CSCD 2022年第3期266-275,共10页
This study presents a simple technique for strengthening the adhesive-bond strength between aluminium(Al)substrate and carbon fibre reinforced polymer(CFRP) utilising resin pre-coating(RPC) with carbon nanotubes(CNTs)... This study presents a simple technique for strengthening the adhesive-bond strength between aluminium(Al)substrate and carbon fibre reinforced polymer(CFRP) utilising resin pre-coating(RPC) with carbon nanotubes(CNTs). The CNT-containing RPC solution with 90 wt% acetone and 10 wt% resin(without hardener) was applied onto Al substrates, where micro-/nano-vertical channels had been created by chemical or mechanical surface treatments to accommodate CNTs. RPC was able to fill all micro-/nano-cavities over the Al substrate surface, then CNTs were pulled into those vertical micro-channels by the capillary action generated from acetone evaporation.Normal epoxy adhesive(resin + hardener) was applied after the CNT-containing RPC treatment. CNTs bridging across the interface between the adhesive joint and Al substrate and sealing of micro-/nano-cavities by RPC effectively enhanced the interfacial shear bond strength between the Al substrate and CFRP by 30–100%depending on the Al substrate surface profiles. Al substrates with two different chemical treatments were compared in this study for the effectiveness of CNT interfacial reinforcement. Results from a steel substrate after sandblasting were also included for comparison. 展开更多
关键词 shear bond strength Interfacial toughening CNT Resin pre-coating(RPC) Chemical surface treatment Aluminium/CFRP Laminate
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An in Vitro Comparison of Bonding Effectiveness of Different Adhesive Strategies on Erbium:Yttrium-Alluminum-Garnet Laser Irradiated Dentin 被引量:1
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作者 Daniele Scaminaci Russo Jacopo Buti Luca Giachetti 《Open Journal of Stomatology》 2016年第1期1-11,共11页
Background: To date there is not a material considered ideal for the lased dentin. Objective: To compare the bond strength to human lased dentin of self-etch and etch-and-rinse adhesive systems, a self-adhesive resin ... Background: To date there is not a material considered ideal for the lased dentin. Objective: To compare the bond strength to human lased dentin of self-etch and etch-and-rinse adhesive systems, a self-adhesive resin composite and a glass-ionomer cement. Methods: Forty human molars were sectioned to obtain a 2 mm-thick slab of mid-coronal dentin. The occlusal surface of each slab was polished by SiC paper (P600) for 10 s. Then an half part of dentin slabs was randomly selected for receiving treatment with 2.94 μm Er:YAG laser (DEKA, Smart 2940D Plus) with 10 Hz at 100 mJ, pulse duration of 230 μs with contact tip. Dentin slabs were randomly divided into four groups (n = 10). Six conical frustum-shaped build-ups were constructed on the occlusal surface of each dentin slab using bonding agents (OptiBond Solo Plus Group 1;OptiBond All-in-one Group 2) combined with a resin composite (Premise Flow), self-adhesive resin composites (Vertise Flow Group 3) and a glass-ionomer cement (Ketac-Fil Group 4). Specimens were subjected to μSBS test. Data were analyzed by a mixed model and Tukey’s test. Results: Measured bond strengths were (mean ± standard deviation): 20.8 ± 5.5 MPa (laser treatment) and 15.6 ± 4.5 MPa (SiC paper) for Group 1, 18.9 ± 5.3 MPa (laser treatment) and 14.0 ± 4.3 MPa (SiC paper) for Group 2, 7.9 ± 2.8 MPa (laser treatment) and 4.3 ± 2.2 MPa (SiC paper) for Group 3, 4.7 ± 1.9 MPa (laser treatment) and 2.6 ± 1.2 MPa (SiC paper) for Group 4. The inferential analysis showed that the dentin laser treatment significantly affected the bond strength within each individual group. On dentin treated with laser the bond strengths recorded for build-ups constructed with etch and rinse and self-etch adhesive systems were significantly higher than those recorded for build-ups constructed with self-adhesive resin composite and glass-ionomer cement (p < 0.0001). Similarly, on dentin treated with SiC paper the bond strengths recorded for build-ups constructed with etch and rinse and self-etch adhesive systems were significantly higher than those recorded for build-ups constructed with self-adhesive resin composite and glass-ionomer cement (p < 0.0001). Conclusion: Er:YAG laser treatment has increased the shear bond strength of all the adhesive materials used. 展开更多
关键词 Adhesion Micro shear bond strength Test DENTIN Restorative Materials
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