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基于FAST和Sobol指数法的雷达系统效能敏感性分析
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作者 胡涛 申立群 +2 位作者 朱镜达 孙成会 董伟锋 《系统工程与电子技术》 EI CSCD 北大核心 2024年第2期561-569,共9页
为了以较小的代价快速提升对空探测雷达系统的综合效能,首先搭建了对空探测雷达系统综合效能的评估指标体系,在此基础上完成了综合效能评估模型的建立。选择两种基于方差原理的全局敏感性分析方法,即傅里叶幅度敏感性测试(Fourier ampli... 为了以较小的代价快速提升对空探测雷达系统的综合效能,首先搭建了对空探测雷达系统综合效能的评估指标体系,在此基础上完成了综合效能评估模型的建立。选择两种基于方差原理的全局敏感性分析方法,即傅里叶幅度敏感性测试(Fourier amplitudes sensitivity test,FAST)和Sobol指数法,分别从频域和时域对建立的评估模型进行敏感性分析。在基于FAST进行敏感性分析时,提出了21维输入指标所对应的特征频率集的选取方法;在基于Sobol指数法进行敏感性分析时,考虑了二阶及高阶敏感性指数的影响。对比FAST和Sobol指数法的分析结果,两种方法获得的敏感性分析结果具有较好的一致性。其中,功率和频率为对空探测雷达系统的主要影响指标,为雷达系统的研发和升级提供了可靠性依据。 展开更多
关键词 雷达系统 效能评估 敏感性分析 傅里叶幅度敏感性测试 sobol指数法
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Exploring the Application Effect of Flipped Classroom Combined with Problem-Based Learning Teaching Method in Clinical Skills Teaching of Standardized Training for Resident Doctors of Traditional Chinese Medicine 被引量:1
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作者 Jingjing Tang 《Journal of Biosciences and Medicines》 CAS 2023年第2期169-176,共8页
Objective: To explore the application effect of flipped classroom combined with problem-based learning teaching method in clinical skills teaching of standardized training for resident doctors of traditional Chinese M... Objective: To explore the application effect of flipped classroom combined with problem-based learning teaching method in clinical skills teaching of standardized training for resident doctors of traditional Chinese Medicine. Methods: The study used the experimental control method. The study lasted from September to November 2022. The subjects of this study were 49 students of standardized training for resident doctors of traditional Chinese Medicine from grades 2020, 2021 and 2022 of Dazhou integrated TCM & Western Medicine Hospital. They were randomly divided into experiment group (25) and control group (24). The experiment group adopted flipped classroom combined with problem-based learning teaching method, and the control group adopted traditional teaching method. The teaching content was 4 basic clinical skill projects, including four diagnoses of traditional Chinese Medicine, cardiopulmonary resuscitation, dressing change procedure, acupuncture and massage. The evaluation method was carried out by comparing the students’ performance and a self-designed questionnaire was used to investigate the students’ evaluation of the teaching method. Results: The test scores of total scores in the experimental group (90.12 ± 5.89) were all higher than those in the control group (81.47 ± 7.96) (t = 4.53, P P Conclusions: The teaching process of the flipped classroom combined with problem-based learning teaching method is conducive to improving the efficiency of classroom teaching, cultivating students’ self-learning ability, and enhancing students’ willingness to learn. 展开更多
关键词 standardized Training for Resident Doctors of Traditional Chinese Medicine Clinical Skills Teaching Flipped Classroom Problem-Based Learning Teaching method
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Sensitivity analysis of factors affecting gravity dam anti-sliding stability along a foundation surface using Sobol method
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作者 Bo Xu Shi-da Wang 《Water Science and Engineering》 EI CAS CSCD 2023年第4期399-407,共9页
The anti-sliding stability of a gravity dam along its foundation surface is a key problem in the design of gravity dams.In this study,a sensitivity analysis framework was proposed for investigating the factors affecti... The anti-sliding stability of a gravity dam along its foundation surface is a key problem in the design of gravity dams.In this study,a sensitivity analysis framework was proposed for investigating the factors affecting gravity dam anti-sliding stability along the foundation surface.According to the design specifications,the loads and factors affecting the stability of a gravity dam were comprehensively selected.Afterwards,the sensitivity of the factors was preliminarily analyzed using the Sobol method with Latin hypercube sampling.Then,the results of the sensitivity analysis were verified with those obtained using the Garson method.Finally,the effects of different sampling methods,probability distribution types of factor samples,and ranges of factor values on the analysis results were evaluated.A case study of a typical gravity dam in Yunnan Province of China showed that the dominant factors affecting the gravity dam anti-sliding stability were the anti-shear cohesion,upstream and downstream water levels,anti-shear friction coefficient,uplift pressure reduction coefficient,concrete density,and silt height.Choice of sampling methods showed no significant effect,but the probability distribution type and the range of factor values greatly affected the analysis results.Therefore,these two elements should be sufficiently considered to improve the reliability of the dam anti-sliding stability analysis. 展开更多
关键词 Gravity dam Anti-sliding stability Sensitivity analysis sobol method Latin hypercube sampling
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Effectiveness of Participatory Teaching Methods in the Standardized Training of Respiratory Medicine Residents
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作者 Yanbing Wang Jieru Feng 《Journal of Contemporary Educational Research》 2023年第10期179-184,共6页
Objective:To explore and analyze the application effect of participatory teaching method in the standardized training of respiratory medicine residents.Methods:The study period was from May 2022 to May 2023.20 doctors... Objective:To explore and analyze the application effect of participatory teaching method in the standardized training of respiratory medicine residents.Methods:The study period was from May 2022 to May 2023.20 doctors in the standardized training of respiratory medicine residency in our hospital were taken as research subjects and grouped into the participatory group(n=10)and the routine group(n=10)by using the random number lottery method.The participatory group practised participatory teaching methods,and the routine group practised routine teaching methods.The results of discharge assessment,teaching evaluation,and mini-Clinical Evaluation Exercise(mini-CEX)assessment were compared between the groups.Results:The theoretical assessment,operational assessment,and total scores of the participatory group were significantly higher than those of the routine group,and the difference was statistically significant(P<0.05).The teaching evaluation of independent learning,theoretical mastery,teamwork,clinical thinking,communication,and learning interest of the participatory group was significantly higher than that of the routine group,and the difference was statistically significant(P<0.05).The mini-CEX assessments of history inquiry,organizational effectiveness,professionalism,physical examination,clinical diagnosis,communication skills,and overall clinical competence of the participatory group were significantly better than those of the routine group,and the difference was statistically significant(P<0.05).The teaching satisfaction of the participatory group was significantly higher than that of the routine group,the difference was statistically significant(P<0.05).Conclusion:Participatory teaching methods can improve the overall level of doctors in the respiratory medicine residency standardized training,and the teaching satisfaction is improved. 展开更多
关键词 Participatory teaching method Respiratory medicine RESIDENCY standardized training
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Inspiration of Foreign Innovative Drug Pricing Methods and Medical Insurance Payment Standards to China
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作者 Rao Xiuli Sun Lihua 《Asian Journal of Social Pharmacy》 2023年第4期365-373,共9页
Objective To study the innovative drug pricing methods and medical insurance payment standards in foreign countries and to provide reference for China’s government.Methods The official websites were searched for info... Objective To study the innovative drug pricing methods and medical insurance payment standards in foreign countries and to provide reference for China’s government.Methods The official websites were searched for information and related literature,and literature review was used.Results and Conclusion In foreign countries,the clinical value of innovative drugs and their impact on medical insurance funds were comprehensively evaluated based on factors such as quality-adjusted life years,clinical benefit,and improvement of clinical benefit.Then,the evaluation results were taken as an important basis for whether innovative drugs were admitted to the medical insurance catalog and establishing medical insurance payment standards.By using international experience for reference,innovative drug pricing methods and medical insurance payment standards for China’s national conditions can be improved by establishing a basic database of clinical value and drug economic evaluation of innovative drugs,as well as innovative drug payment models based on decision thresholds. 展开更多
关键词 innovative drug pricing method payment standard medical insurance international experience
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基于Sobol灵敏度分析法的风电机组噪声特性研究
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作者 王金金 刘建桧 《环境与发展》 2024年第4期72-76,共5页
风电机组所产生的噪声主要来自于由其叶片引起的气动噪声,包括来流湍流噪声和翼型自身噪声两部分,目前已成为影响声环境的重要因素之一。本文以Amiet&Lowson半经验风电机组噪声预测模型为研究对象,通过引入Sobol全局灵敏度分析方法... 风电机组所产生的噪声主要来自于由其叶片引起的气动噪声,包括来流湍流噪声和翼型自身噪声两部分,目前已成为影响声环境的重要因素之一。本文以Amiet&Lowson半经验风电机组噪声预测模型为研究对象,通过引入Sobol全局灵敏度分析方法,探究了影响风电机组来流湍流噪声各因素的重要性。研究表明,影响风电机组噪声大小的因素依次为:来流速度、声源到观测点的距离、声波频率、翼型弦长、翼型展长、空气密度和翼段距离地面高度,其中来流速度为最主要因素,其次为声源到观测点距离和声波频率,以上三点因素与风电机组结构无关,表明改变风电机组结构对缓解噪声污染效果不大。对于风电机组本身结构而言,翼段弦长的影响最大,如需要通过结构的改变来降噪,此参数应该为最先考虑的对象,其次为翼型展长。 展开更多
关键词 风电机组 噪声 灵敏度分析 sobol
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Using Different Standardized Methods for Species Identification:A Case Study Using Beaks from Three Ommastrephid Species 被引量:4
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作者 HU Guanyu FANG Zhou +3 位作者 LIU Bilin CHEN Xinjun STAPLES Kevin CHEN Yong 《Journal of Ocean University of China》 SCIE CAS CSCD 2018年第2期355-362,共8页
The cephalopod beak is a vital hard structure with a stable configuration and has been widely used for the identification of cephalopod species. This study was conducted to determine the best standardization method fo... The cephalopod beak is a vital hard structure with a stable configuration and has been widely used for the identification of cephalopod species. This study was conducted to determine the best standardization method for identifying different species by measuring 12 morphological variables of the beaks of Illex argentinus, Ommastrephes bartramii, and Dosidicus gigas that were collected by Chinese jigging vessels. To remove the effects of size, these morphometric variables were standardized using three methods. The average ratios of the upper beak morphological variables and upper crest length of O. bartramii and D. gigas were found to be greater than those of I. argentinus. However, for lower beaks, only the average of LRL(lower rostrum length)/LCL(lower crest length), LRW(lower rostrum width)/LCL, and LLWL(lower lateral wall length)/LCL of O. bartramii and D. gigas were greater than those of I. argentinus. The ratios of beak morphological variables and crest length were found to be all significantly different among the three species(P < 0.001). Among the three standardization methods, the correct classification rate of stepwise discriminant analysis(SDA) was the highest using the ratios of beak morphological variables and crest length. Compared with hood length, the correct classification rate was slightly higher when using beak variables standardized by crest length using an allometric model. The correct classification rate of the lower beak was also found to be greater than that of the upper beak. This study indicates that the ratios of beak morphological variables to crest length could be used for interspecies and intraspecies identification. Meanwhile, the lower beak variables were found to be more effective than upper beak variables in classifying beaks found in the stomachs of predators. 展开更多
关键词 BEAK standardized methodS DISCRIMINANT analysis Illex argentinus Ommastrephes bartramii Dosidicus GIGAS
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Improved EEMD-based standardization method for developing long tree-ring chronologies 被引量:5
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作者 Xianliang Zhang Junxia Li +1 位作者 Xiaobo Liu Zhenju Chen 《Journal of Forestry Research》 SCIE CAS CSCD 2020年第6期2217-2224,共8页
Long tree-ring chronologies can be developed by overlapping data from living trees with data from fossil trees through cross-dating.However,low-frequency climate signals are lost when standardizing tree-ring series du... Long tree-ring chronologies can be developed by overlapping data from living trees with data from fossil trees through cross-dating.However,low-frequency climate signals are lost when standardizing tree-ring series due to the"segment length curse".To alleviate the segment length curse and thus improve the standardization method for developing long tree-ring chronologies,here we first calculated a mean value for all the tree ring series by overlapping all of the tree ring series.The growth trend of the mean tree ring width(i.e.,cumulated average growth trend of all the series)was determined using ensemble empirical mode decomposition.Then the chronology was developed by dividing the mean value by the growth trend of the mean value.Our improved method alleviated the problem of trend distortion.Long-term signals were better preserved using the improved method than in previous detrending methods.The chronologies developed using the improved method were better correlated with climate than those developed using conservative methods.The improved standardization method alleviates trend distortion and retains more of the low-frequency climate signals. 展开更多
关键词 standardization methods Tree rings Segment length curse DETRENDING
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基于Sobol指数法的舰艇防空作战效能敏感性分析 被引量:1
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作者 许俊飞 杨光 +1 位作者 姜思恒 吴玲 《兵器装备工程学报》 CAS CSCD 北大核心 2023年第7期189-196,共8页
为探索水面舰艇防空武器装备对作战效能的影响关系,构建了舰艇防空武器系统指标体系,在指标归一化的基础上建立基于幂指数法的舰艇防空作战效能评估模型;采用Sobol指数法分析了防空武器装备各个能力指标在全局变动时对舰艇防空作战效能... 为探索水面舰艇防空武器装备对作战效能的影响关系,构建了舰艇防空武器系统指标体系,在指标归一化的基础上建立基于幂指数法的舰艇防空作战效能评估模型;采用Sobol指数法分析了防空武器装备各个能力指标在全局变动时对舰艇防空作战效能的影响,基于主效应和全效应指数对各个指标进行敏感性排序,确定影响舰艇防空作战效能的关键因素,并分析了指标之间的交互效应对作战效能的影响。仿真结果表明,防空导弹命中概率、系统反应时间、飞行速度3个指标对舰艇防空作战效能的影响较大。该研究可为舰艇防空武器装备的论证工作提供参考和依据。 展开更多
关键词 作战效能评估 幂指数法 sobol指数法 蒙特卡洛法 敏感性
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Calculating the Number of Pregnant Women Receiving Standardized Services for PMTCT of HIV in Liangshan Prefecture,Based on the Equivalent Method 被引量:1
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作者 QU Shui Ling WANG Ai Ling +3 位作者 PAN Xiao Ping WANG Xiao Yan LUO Hui Ming ZHANG Tong 《Biomedical and Environmental Sciences》 SCIE CAS CSCD 2020年第10期745-749,共5页
Objective To calculate the number of pregnant women who receive standardized prevention of mother-to-child transmission(PMTCT)services for HIV annually.Methods HIV-positive pregnant women in six counties of Liangshan ... Objective To calculate the number of pregnant women who receive standardized prevention of mother-to-child transmission(PMTCT)services for HIV annually.Methods HIV-positive pregnant women in six counties of Liangshan Prefecture in 2017 were selected as study subjects.The entire process,from when the subjects first received the PMTCT of HIV services to the end,was divided into four stages,which were further divided into 25 phases.The equivalent coefficient was used to indicate the weight of workload in each phase.Seven experts were invited to score the equivalent coefficient;the number of pregnant women who received standardized services to prevent the transmission of HIV was calculated.Results A total of 663 HIV-positive pregnant women were registered in six Liangshan Prefecture counties in 2017.This figure was converted into 7,780 person-months devoted to HIV-positive pregnant women,with 260 person-months(3.34%)spent on the first antenatal care,1,510 person-months(19.41%)during pregnancy,378 person-months(4.86%)on delivery,and 5,632 person-months(72.39%)on post-partum period.The equivalent coefficient calculation showed that 314 HIV-positive pregnant women received standardized PMTCT services.Conclusion The number of pregnant women receiving standardized services for the PMTCT of HIV can be calculated accurately using the equivalent method to identify the gap between the level of PMTCT of HIV intervention services needed and the actual workload. 展开更多
关键词 Equivalent method standardized services PMTCT Pregnant women HIV
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Smart Society and Artificial Intelligence:Big Data Scheduling and the Global Standard Method Applied to Smart Maintenance 被引量:1
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作者 Ruben Foresti Stefano Rossi +2 位作者 Matteo Magnani Corrado Guarino Lo Bianco Nicola Delmonte 《Engineering》 SCIE EI 2020年第7期835-846,共12页
The implementation of artificial intelligence(AI)in a smart society,in which the analysis of human habits is mandatory,requires automated data scheduling and analysis using smart applications,a smart infrastructure,sm... The implementation of artificial intelligence(AI)in a smart society,in which the analysis of human habits is mandatory,requires automated data scheduling and analysis using smart applications,a smart infrastructure,smart systems,and a smart network.In this context,which is characterized by a large gap between training and operative processes,a dedicated method is required to manage and extract the massive amount of data and the related information mining.The method presented in this work aims to reduce this gap with near-zero-failure advanced diagnostics(AD)for smart management,which is exploitable in any context of Society 5.0,thus reducing the risk factors at all management levels and ensuring quality and sustainability.We have also developed innovative applications for a humancentered management system to support scheduling in the maintenance of operative processes,for reducing training costs,for improving production yield,and for creating a human–machine cyberspace for smart infrastructure design.The results obtained in 12 international companies demonstrate a possible global standardization of operative processes,leading to the design of a near-zero-failure intelligent system that is able to learn and upgrade itself.Our new method provides guidance for selecting the new generation of intelligent manufacturing and smart systems in order to optimize human–machine interactions,with the related smart maintenance and education. 展开更多
关键词 Smart maintenance Smart society Artificial intelligence Human-centered management system Big data scheduling Global standard method Society 5.0 Industry 4.0
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Analytical and Traveling Wave Solutions to the Fifth Order Standard Sawada-Kotera Equation via the Generalized exp(-Φ(ξ))-Expansion Method 被引量:1
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作者 M. Y. Ali M. G. Hafez +1 位作者 M. K. H. Chowdury M. T. Akter 《Journal of Applied Mathematics and Physics》 2016年第2期262-271,共10页
In this article, we propose a generalized exp(-Φ(ξ))-expansion method and successfully implement it to find exact traveling wave solutions to the fifth order standard Sawada-Kotera (SK) equation. The exact traveling... In this article, we propose a generalized exp(-Φ(ξ))-expansion method and successfully implement it to find exact traveling wave solutions to the fifth order standard Sawada-Kotera (SK) equation. The exact traveling wave solutions are established in the form of trigonometric, hyperbolic, exponential and rational functions with some free parameters. It is shown that this method is standard, effective and easily applicable mathematical tool for solving nonlinear partial differential equations arises in the field of mathematical physics and engineering. 展开更多
关键词 Generalized exp(-Φ(ξ))-Expansion method Fifth Order standard Sawada-Kotera Equation SOLITONS Periodic Wave Solutions
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Design Method of Equipment Optimization Development Based on Standardization Theory 被引量:2
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作者 Lv-bo MAI 《Defence Technology(防务技术)》 SCIE EI CAS 2013年第3期140-145,共6页
The matters of equipment optimization development are usually discrete,fuzzy and non-quantitative.It is difficult directly to optimize the equipment development with a mathematical model.A set of methods for designing... The matters of equipment optimization development are usually discrete,fuzzy and non-quantitative.It is difficult directly to optimize the equipment development with a mathematical model.A set of methods for designing the equipment optimization development with six dimensions and eight main elements is established based on the theory and method of standardization.The top-tier design space of systematic development of equipment is built up by the relations of basic models,series and model spectrums.The relations of time and space for equipment optimization development are established.The design processes of a six dimension systematic space are expounded.The connotation of each plan in the main system space is analyzed.A design method for an entire equipment is established with standardization theory.The coordinating design methods of equipment technical system and the optimization design methods of equipment integration are discussed.The design methods for universalization and serialization of components and parts are established.The design methods of equipment optimization development highlight the relations of the basic model of platform,the serialization of platform basic models,the modularization of equipment functions,the model spectrum of variant equipment,and the universalization and serialization of components and parts. 展开更多
关键词 优化设计方法 优化开发 化设备 标准化 优化发展 数学模型 设计空间 设备系统
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The Research on Methodology for Material Code Standardization in the Implementation of MRP-Ⅱ
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作者 孙虞 《Journal of Southeast University(English Edition)》 EI CAS 1996年第2期13-18,共6页
This paper analyses the current common problems of material code standardization in the implementation of MRP Ⅱ, and puts forward the basic ideas and methods for solving the problems, which has some reference value ... This paper analyses the current common problems of material code standardization in the implementation of MRP Ⅱ, and puts forward the basic ideas and methods for solving the problems, which has some reference value for the popularization of application o 展开更多
关键词 CODING standard methods
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Compilation Principles and Methods of China’s First Mongolian Standard in Meteorological Industry
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作者 Ying Chun Yu Gang Han Yanli 《Meteorological and Environmental Research》 CAS 2019年第4期118-121,共4页
Mongolian Terms Commonly Used in Meteorological Services that was issued by the China Meteorological Administration is China s first traditional Mongolian standard in meteorological industry. In the process of formula... Mongolian Terms Commonly Used in Meteorological Services that was issued by the China Meteorological Administration is China s first traditional Mongolian standard in meteorological industry. In the process of formulation, the compilation unit fully complied with the principles of scientificity, practicability, universality and versatility, and used literal translation, free translation, and the combination of literal translation and free translation to translate and compile 71 mongolian terms commonly used in meteorological services. The standard fills the blank of standardization construction of basic traditional Mongolian language in the meteorological industry of China. 展开更多
关键词 METEOROLOGY MONGOLIAN language standard COMPILATION PRINCIPLES and methodS
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LA-ICP-MS Calibrations for Intact Rock Samples with Internal Standard and Modified Constant-Sum Methods
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作者 Sheng Peng Qinhong Hu 《American Journal of Analytical Chemistry》 2012年第2期168-174,共7页
Laser ablation coupled with inductively coupled plasma-mass spectrometry (LA-ICP-MS) calibration was conducted with multiple spot analyses on eleven intact rock samples using both an internal standard (IS) method and ... Laser ablation coupled with inductively coupled plasma-mass spectrometry (LA-ICP-MS) calibration was conducted with multiple spot analyses on eleven intact rock samples using both an internal standard (IS) method and a modified constant-sum (MCS) method. Methods were then compared for reported bulk elemental composition of the rocks. The MCS method was based on the sum of eight major elements, which is spatially more stable than one single major ele-ment as used in the IS method, and is quite constant among different rock samples. Calibrations were performed with standard reference materials NIST SRM 610, 612, 614, and 616. Little difference was found between using a single standard and a set of standards, because of the good linearity shown by the reference materials. Comparison of the two calibration methods shows that the MCS method produced better and more stable results than the IS method for heterogeneous samples. With the MCS method, approximately 94% to 95% of the total measurements are within the range of ±100% relative deviation, compared with 82% to 86% with the IS method. The IS method resulted insubstantial overestimations for some rock samples (e.g., 648% for Basalt BCR-2 using NIST SRM 610 as the calibration standard), while the largest deviation with the MCS method was 216% for U in Eagle Ford shale #80 sample. For Quartz latite QLO-1, a relative homogeneous sample, the IS method generated slightly better results than the MCS method. Regardless of method, spatially heterogeneous distribution of elements in the intact rock at the scale of the laser spot is considered to be the main reason for the large relative deviations seen in our work compared to published results. 展开更多
关键词 LA-ICP-MS Quantitative Calibration Internal standard method MODIFIED Constant-Sum method
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Synthesis of an IS and Steviol Glycoside Analysis by a Validated Internal Standard Method
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作者 Jan M. C. Geuns Tom Struyf +2 位作者 Stijn Ceunen Gert Steurs Wim De Borggraeve 《American Journal of Analytical Chemistry》 2018年第11期547-559,共13页
The internal standard (IS) method is the best method for the analysis of samples, as it is independent of errors in injection volume, changes in sample volumes, and changes in sensitivity of the detector, etc. Use of ... The internal standard (IS) method is the best method for the analysis of samples, as it is independent of errors in injection volume, changes in sample volumes, and changes in sensitivity of the detector, etc. Use of an internal standard allows for the correction of losses due to sample clean-up of complex samples. An ideal IS is a compound that has properties very similar to, and that behaves as the compounds to be analysed. Ideally, only in the last step of analysis (HPLC), the IS should be well separated from the compounds of the mixture to be analysed. After testing several existing compounds with negative results, we decided to synthesise the 19-O-β-D-galactopyranosyl-13-O-β-D-glucopyranosyl-steviol as IS. This is the 19-galactosyl ester of steviolmonoside (13-O-β-D-glucopyranosyl-steviol). The IS was made according to published methods. Steviolmonoside (SM) was made from purified commercial rubusoside (Rub) by refluxing it in 10% KOH for 2 h. SM was precipitated and crystallized from MeOH. The hydroxyls of the glucose unit of SM were protected by acetylation. The acetylated SM was crystallized from acetone and dissolved in 1,2-dichloroethane. Then Ag2CO3 on Celite and tetra-acetylated galactopyranosyl bromide were added and the mixture was refluxed for 2 h. After cooling, BaO in MeOH was added to remove the acetyl groups. The 1,2-dichloroethane fraction was then extracted three times with equal volumes of water and the water fraction containing the IS was further purified on a C18 flash chromatography column. Traces of unreacted SM were removed by preparative HPLC on an Alltima C18 column (250 mm × 22 mm, particle size 10 μm) with AcCN:water (35:65, 20 ml/min). Detection was at 210 nm (KNAUER, “Smartline” UV detector 2500). The collected IS fraction from the HPLC was completely dried. Mixtures of steviol glycosides (SVglys) containing IS could be purified over SPE cartridges without change of the SVgly over IS ratio. The calibration curves for rebaudioside A (RebA) and stevioside (ST) were linear between 0.012 and 0.95 and between 0.013 and 1.13 mM for RebA and ST, respectively. The accuracy was checked by the standard addition method. It was concluded that the IS method gives an excellent precision and accuracy. 展开更多
关键词 STEVIOL GLYCOSIDES INTERNAL standard method VALIDATION Quantification PURIFICATION
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The Measurement and Uncertainty Analysis of Antenna Factor of Microwave Antennas Based on Standard Site Method
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作者 Chaochan Chen Hong Shi +1 位作者 Yi Miao Yu Sang 《International Journal of Communications, Network and System Sciences》 2017年第5期138-145,共8页
A method of Standard Site Method (SSM) in the American National Standards Institute’s ANSI C63.5 is described in the frequency ranges from 30 MHz to 1000 MHz. And a measurement system is set up for determining antenn... A method of Standard Site Method (SSM) in the American National Standards Institute’s ANSI C63.5 is described in the frequency ranges from 30 MHz to 1000 MHz. And a measurement system is set up for determining antenna factors (AF) of antennas on an Open Area Test Sites (OATS). AF of antennas including log-periodic antenna and biconical antenna is measured with SSM method by Shanghai Institute of Measurement and Testing Technology (SIMT), which shows good agreement to data measured by National Institute of Metrology (NIM). In the end, it analyzes the measurement uncertainty of SIMT in the 30 MHz to 1000 MHz frequency band and does comparison to that of NIM. 展开更多
关键词 ANTENNA FACTORS standard SITE method (SSM) MEASUREMENT UNCERTAINTY
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Current dependence coefficient determination for different DC standard resistors measurements based on Ⅴ-Ⅰ method
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作者 Rasha S M Ali M Helmy A Raouf 《Journal of Measurement Science and Instrumentation》 CAS CSCD 2016年第4期332-335,共4页
Current dependence and stability of the measured resistance value are very important for the accurate measurement of DC standard resistor. In this paper, the volt-ampere (V-I) measurement method has been applied ... Current dependence and stability of the measured resistance value are very important for the accurate measurement of DC standard resistor. In this paper, the volt-ampere (V-I) measurement method has been applied to study the current depend-ence of four different types of standard resistors. Diverse values are obtained through the investigation of their stability at dif-ferent currents. Therefore, the current dependence coefficient (CDC) can be determined for each one of the studied resistors. Research shows CDC depends on the applied current value, the measurement time and the resistor type, as clearly demonstra-ted in this research. 展开更多
关键词 current dependence coefficient standard resistors volt-ampere method resistor stability
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Quantitative Determination of Tetrachlorantraniliprole by(1)^H NMR Spectroscopy with Internal Standard Method
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作者 Lang Jie Dong Yan +2 位作者 Wang Qiang Yang Huibin Yu Haibo 《Plant Diseases and Pests》 CAS 2020年第5期35-37,共3页
[Objective]This study was to establish a rapid,specific and simple method for quantitative determination of tetrachlorantraniliprole by 1H NMR.[Method]1H NMR spectroscopy was acquired with deuterium DMSO as the solven... [Objective]This study was to establish a rapid,specific and simple method for quantitative determination of tetrachlorantraniliprole by 1H NMR.[Method]1H NMR spectroscopy was acquired with deuterium DMSO as the solvent and maleic acid as internal standard under the conditions of temperature 25℃,pulses width 8.0μs,delay time 5 s,and scanning times 8.[Result]The hydrogen proton peaks of tetrachlorantraniliprole(δ=10.55)and maleic acid(δ=6.27)were taken as quantitative peaks.The peak area ratio y(As/Ar)and mass ratio x(ms/mr)were linearly regressed,and the correlation coefficient was 0.9999.The RSD value of repeatability test was 0.38%,and the RSD value of stability test was 0.77%.The content of tetrachlorantraniliprole was determined as 99.6%.[Conclusion]1H NMR spectroscopy can be used for quantitative determination of tetrachlorantraniliprole without standard reference,which is rapid,accurate and simple. 展开更多
关键词 Tetrachlorantraniliprole qNMR Internal standard method Quantitative determination
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