Some refractory linings that protect metallic vessels from the hot temperature of the products they contain are made of masonries with or without mortar.The joints play an important role,reducing the stresses in the m...Some refractory linings that protect metallic vessels from the hot temperature of the products they contain are made of masonries with or without mortar.The joints play an important role,reducing the stresses in the masonries during heating.Furthermore,the presence of these joints makes the behaviour of the masonry nonlinear and orthotropic.To perform a thermomechanical simulation using a finite element method of an industrial vessel that contains hundreds or thousands of bricks and joints,microscopic models are not suitable due to the high computational time and the management of the behaviour of the joints(opening/closing)which affects the convergence.To overcome these problems,it is proposed to replace the masonry by a homogeneous material that has a behaviour equivalent to the set of bricks and joints,using a periodic homogenization technique.Since the joints can be closed or open,the equivalent material will have a different behaviour according to the joint state.Furthermore,refractory materials have an elastic-viscoplastic behaviour at high temperatures.So,the equivalent material will have an orthotropic elastic-viscoplastic behaviour,requiring a nonlinear homogenisation technique.An overview of this approach developed at University of Orléans is presented with two industrial applications(blast-furnace and steel ladle).展开更多
The effect of refined precipitations and dispersed phases on the toughness of SS400 steel was investigated by rapid tempering with thermomechanical simulation tester, and the electromagnetic induction rapid tempering ...The effect of refined precipitations and dispersed phases on the toughness of SS400 steel was investigated by rapid tempering with thermomechanical simulation tester, and the electromagnetic induction rapid tempering process was simulated. The conventional tempering and rapid tempering process were proceeded respectively, and both samples were quenched in 10~ of agitated iced brine. The tempering temperatures were designed as 560, 620 and 680℃, respectively. Rapid tempering specimens were heated at a heating rate of 20 ℃/s, and all samples of these three tempering temperatures were maintained 30, 40 and 50 s with the Gleeble1500-D tester, respectively. The impact test at --40 ℃ were carried out on a Charpy impact machine (CBD-300) with a maximum measurement range of 300 J and the microstructures were analyzed in detail using optical microscope (OM) and scanning electron microscope (SEM). The experiment results show that the upper bainite, martensite and small amount of austenite were obtained in the rapidly quenched samples. In comparison to the conventional process, the matrix microstructure was changed from the larger size and bulk ferrite to the refined banding structure, and the cementites were obviously refined and precipitated inside the grains and along the grain boundaries. The cryogenic impact test implies that the maximum values of impact toughness with holding time of 30 or 50 s are achieved at tempering temperature of 620℃. Furthermore, a favorite value of impact toughness with holding time of 40 s is available.展开更多
Direct hot rolled dual phase steel production represents a challenging route, compared with cold rolled and intercritical annealing process, due to complex and sophisticated control of the hot strip mill processing pa...Direct hot rolled dual phase steel production represents a challenging route, compared with cold rolled and intercritical annealing process, due to complex and sophisticated control of the hot strip mill processing parameters. Instead, high technology compact slab production plant offers economic advantages, adequate control and prompt use of the advanced thermomechanical controlled rolling. The current work aims to obtain different structures and tensile properties by physical simulation of direct hot rolled niobium micro alloyed dual phase low carbon steel by varying the metallurgical temperatures of hot strip mill plant. This starts with adaptation of the chemical analysis of a low carbon content to fall far from the undesired peritectic region to avoid slab cracking during casting. Thermodynamic and kinetics calculations by Thermo-Calc 2020 and JMat pro software are used to define the transformation’s temperatures Ae1 and Ae3 as well as processing temperatures;namely of reheating, finishing rolling, step cooling and coiling temperatures. The results show that the increase of finishing rolling temperature from 780<span style="white-space:nowrap;">°</span>C to 840<span style="white-space:nowrap;">°</span>C or decreasing either of step cooling duration at ferrite bay from 7 to 4 seconds, enhances yield and tensile strengths, all due to more martensite volume fraction formation. The yield and tensile strengths also increase with decreasing coiling temperature from 330<span style="white-space:nowrap;">°</span>C to 180<span style="white-space:nowrap;">°</span>C, which is explained due to the increase of dislocation densities resulted from the sudden shape change during martensite formation at the lower coiling temperature in additional to the self-tempering of martensite formed at higher coiling temperatures which soften the dual phase steel.展开更多
Ultrafine grain size is often achieved by severe plastic deformation. A few techniques have been devel- oped to achieve severe plastic deformation,such as equal channel angular (ECA ) processing, torsion, and accumu...Ultrafine grain size is often achieved by severe plastic deformation. A few techniques have been devel- oped to achieve severe plastic deformation,such as equal channel angular (ECA ) processing, torsion, and accumulative roll bonding (ARB) techmpues. This paper will introduce a moftiaxis deformation technique which can achieve essentially unlimited strain with constant deformation volume. The mul- tiaxis deformation can be fully restrained or unrestrained.The bulk volume of a multiaxis restraint compression specimen can be easily machined into mechanical testing specimens for mechanical property measurement and other studies.展开更多
Deformation-induced ferrite transformation (DIFT) has been proved to be an effective approach to refine ferrite grains. This paper shows that the ferrite grains can further be refined through combination of DIFT and...Deformation-induced ferrite transformation (DIFT) has been proved to be an effective approach to refine ferrite grains. This paper shows that the ferrite grains can further be refined through combination of DIFT and V or V-N microalloying. Vanadium dissolved in γ matrix restrains DIFT. During deformation, vanadium carbonitrides rapidly precipitate due to strain-induced precipitation, which causes decrease in vanadium dissolved in matrix and indirectly accelerates DIFT. Under heavy deformation, deformation induced ferrite (DIF) grains in V microalloyed steel were finer than those in V free steel. The more V added to steel, the finer DIF grains obtained. Moreover, the addition of N to V microalloyed steels can remarkably accelerate precipitation of V, and then promote DIFT. However, DIF grains in V-N microalloyed steel easily coarsen.展开更多
Based on 30MnSiV steel, the deformation resistance was studied by using Gleeble 1500 thermomechanical simulator. The mathematical model of the deformation resistance is established by analyzing the relationship of the...Based on 30MnSiV steel, the deformation resistance was studied by using Gleeble 1500 thermomechanical simulator. The mathematical model of the deformation resistance is established by analyzing the relationship of the deformation temperature, deformation rate and deformation resistance. The regression equation is highly noticeable by means of regression analysis. The mathematical model corresponds to test data by means of the contrast.展开更多
Microstructures and critical phase-transformation temperature of boron-nickel added Nb-treated high strength low alloy (HSLA) H-beams cooled at different cooling rate, with different deformation were investigated. C...Microstructures and critical phase-transformation temperature of boron-nickel added Nb-treated high strength low alloy (HSLA) H-beams cooled at different cooling rate, with different deformation were investigated. Continuous cooling transformation (CCT) diagram of this new type of steel was obtained by using Gleeble 1500 ther- momechanical simulator. Microstructures and hardness, especially micro-hardness of the experimental steel were in- vestigated by optical microscopy (OM), scanning electron microscope (SEM), Rockwell and Vickers hardness tests. Phase analysis was also studied by X^ray diffraction (XRD). The results indicated that with increase of cooling rate, microstructures of continuous cooled specimens gradually transformed from polygonal ferrite and pearlite, grain boundary ferrite and bainite, bainite and martensite to single martensite. The CCT diagram revealed that slow cool- ing was needed to avoid austenite-bainite transformation to ensure toughness of this steel. By plastic deformation of 40%, austenite-ferrite transformation temperature increased by 46℃, due to deformation induced ferrite transfor- mation during continuous cooling, but Rockwell hardness has little change.展开更多
基金the PhD students(M.Ali,J.Brulin,M.Landreau,T.M.H Nguyen)who have participated to this study,the different compagnies(CPM,RHI-Magnesita,Saint-Gobain,and Tata Steel),the European Commission(ATHOR project,764987 Grant)the Federation for International Refractory Research and Education which have funded it.
文摘Some refractory linings that protect metallic vessels from the hot temperature of the products they contain are made of masonries with or without mortar.The joints play an important role,reducing the stresses in the masonries during heating.Furthermore,the presence of these joints makes the behaviour of the masonry nonlinear and orthotropic.To perform a thermomechanical simulation using a finite element method of an industrial vessel that contains hundreds or thousands of bricks and joints,microscopic models are not suitable due to the high computational time and the management of the behaviour of the joints(opening/closing)which affects the convergence.To overcome these problems,it is proposed to replace the masonry by a homogeneous material that has a behaviour equivalent to the set of bricks and joints,using a periodic homogenization technique.Since the joints can be closed or open,the equivalent material will have a different behaviour according to the joint state.Furthermore,refractory materials have an elastic-viscoplastic behaviour at high temperatures.So,the equivalent material will have an orthotropic elastic-viscoplastic behaviour,requiring a nonlinear homogenisation technique.An overview of this approach developed at University of Orléans is presented with two industrial applications(blast-furnace and steel ladle).
基金Sponsored by Natural Science Foundation of Inner Mongolia Autonomous Region of China (Grant No.2009MS0811)
文摘The effect of refined precipitations and dispersed phases on the toughness of SS400 steel was investigated by rapid tempering with thermomechanical simulation tester, and the electromagnetic induction rapid tempering process was simulated. The conventional tempering and rapid tempering process were proceeded respectively, and both samples were quenched in 10~ of agitated iced brine. The tempering temperatures were designed as 560, 620 and 680℃, respectively. Rapid tempering specimens were heated at a heating rate of 20 ℃/s, and all samples of these three tempering temperatures were maintained 30, 40 and 50 s with the Gleeble1500-D tester, respectively. The impact test at --40 ℃ were carried out on a Charpy impact machine (CBD-300) with a maximum measurement range of 300 J and the microstructures were analyzed in detail using optical microscope (OM) and scanning electron microscope (SEM). The experiment results show that the upper bainite, martensite and small amount of austenite were obtained in the rapidly quenched samples. In comparison to the conventional process, the matrix microstructure was changed from the larger size and bulk ferrite to the refined banding structure, and the cementites were obviously refined and precipitated inside the grains and along the grain boundaries. The cryogenic impact test implies that the maximum values of impact toughness with holding time of 30 or 50 s are achieved at tempering temperature of 620℃. Furthermore, a favorite value of impact toughness with holding time of 40 s is available.
文摘Direct hot rolled dual phase steel production represents a challenging route, compared with cold rolled and intercritical annealing process, due to complex and sophisticated control of the hot strip mill processing parameters. Instead, high technology compact slab production plant offers economic advantages, adequate control and prompt use of the advanced thermomechanical controlled rolling. The current work aims to obtain different structures and tensile properties by physical simulation of direct hot rolled niobium micro alloyed dual phase low carbon steel by varying the metallurgical temperatures of hot strip mill plant. This starts with adaptation of the chemical analysis of a low carbon content to fall far from the undesired peritectic region to avoid slab cracking during casting. Thermodynamic and kinetics calculations by Thermo-Calc 2020 and JMat pro software are used to define the transformation’s temperatures Ae1 and Ae3 as well as processing temperatures;namely of reheating, finishing rolling, step cooling and coiling temperatures. The results show that the increase of finishing rolling temperature from 780<span style="white-space:nowrap;">°</span>C to 840<span style="white-space:nowrap;">°</span>C or decreasing either of step cooling duration at ferrite bay from 7 to 4 seconds, enhances yield and tensile strengths, all due to more martensite volume fraction formation. The yield and tensile strengths also increase with decreasing coiling temperature from 330<span style="white-space:nowrap;">°</span>C to 180<span style="white-space:nowrap;">°</span>C, which is explained due to the increase of dislocation densities resulted from the sudden shape change during martensite formation at the lower coiling temperature in additional to the self-tempering of martensite formed at higher coiling temperatures which soften the dual phase steel.
文摘Ultrafine grain size is often achieved by severe plastic deformation. A few techniques have been devel- oped to achieve severe plastic deformation,such as equal channel angular (ECA ) processing, torsion, and accumulative roll bonding (ARB) techmpues. This paper will introduce a moftiaxis deformation technique which can achieve essentially unlimited strain with constant deformation volume. The mul- tiaxis deformation can be fully restrained or unrestrained.The bulk volume of a multiaxis restraint compression specimen can be easily machined into mechanical testing specimens for mechanical property measurement and other studies.
文摘Deformation-induced ferrite transformation (DIFT) has been proved to be an effective approach to refine ferrite grains. This paper shows that the ferrite grains can further be refined through combination of DIFT and V or V-N microalloying. Vanadium dissolved in γ matrix restrains DIFT. During deformation, vanadium carbonitrides rapidly precipitate due to strain-induced precipitation, which causes decrease in vanadium dissolved in matrix and indirectly accelerates DIFT. Under heavy deformation, deformation induced ferrite (DIF) grains in V microalloyed steel were finer than those in V free steel. The more V added to steel, the finer DIF grains obtained. Moreover, the addition of N to V microalloyed steels can remarkably accelerate precipitation of V, and then promote DIFT. However, DIF grains in V-N microalloyed steel easily coarsen.
文摘Based on 30MnSiV steel, the deformation resistance was studied by using Gleeble 1500 thermomechanical simulator. The mathematical model of the deformation resistance is established by analyzing the relationship of the deformation temperature, deformation rate and deformation resistance. The regression equation is highly noticeable by means of regression analysis. The mathematical model corresponds to test data by means of the contrast.
文摘Microstructures and critical phase-transformation temperature of boron-nickel added Nb-treated high strength low alloy (HSLA) H-beams cooled at different cooling rate, with different deformation were investigated. Continuous cooling transformation (CCT) diagram of this new type of steel was obtained by using Gleeble 1500 ther- momechanical simulator. Microstructures and hardness, especially micro-hardness of the experimental steel were in- vestigated by optical microscopy (OM), scanning electron microscope (SEM), Rockwell and Vickers hardness tests. Phase analysis was also studied by X^ray diffraction (XRD). The results indicated that with increase of cooling rate, microstructures of continuous cooled specimens gradually transformed from polygonal ferrite and pearlite, grain boundary ferrite and bainite, bainite and martensite to single martensite. The CCT diagram revealed that slow cool- ing was needed to avoid austenite-bainite transformation to ensure toughness of this steel. By plastic deformation of 40%, austenite-ferrite transformation temperature increased by 46℃, due to deformation induced ferrite transfor- mation during continuous cooling, but Rockwell hardness has little change.