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应用相位循环方法抑制TOSS谱的残余旋转边带
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作者 丁克洋 杜有如 叶朝辉 《波谱学杂志》 CAS CSCD 1993年第1期97-100,共4页
对π脉冲宽度的误差与频率偏置效应引起的TOSS谱的残余旋转边带进行了分析,证实了相位循环方法能够在一级近似下有效地抑制这种残余旋转边带。在比较宽的频率偏置范围内从实验上检验了相位循环方法的有效性。
关键词 相位循环 TOSS谱 残余旋转边带
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煤直接液化中油煤浆热溶产物的^(13)CNMR研究 被引量:7
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作者 张娉 潘铁英 +4 位作者 史新梅 周丽芳 常鸿雁 张德祥 高晋生 《波谱学杂志》 CAS CSCD 北大核心 2006年第1期41-47,共7页
研究油煤浆热溶产物的成分及含量的变化是控制煤直接液化工艺的重要因素之一.本文采用固体核磁共振研究了在高压釜中用不同溶剂在不同温度下(250~370℃)得到的神华煤及其热溶产物的一些变化规律.通过对神华煤及其热溶中间产物与抽余煤... 研究油煤浆热溶产物的成分及含量的变化是控制煤直接液化工艺的重要因素之一.本文采用固体核磁共振研究了在高压釜中用不同溶剂在不同温度下(250~370℃)得到的神华煤及其热溶产物的一些变化规律.通过对神华煤及其热溶中间产物与抽余煤的13CCP/MAS/TOSSNMR分析可知,神华煤经热溶处理后,脱除了一些含氧官能团以及某些脂肪烃结构.同时,一些芳香桥碳分子和被取代的芳香碳环发生了断裂,随着反应温度逐渐升高,由于不断供氢,四氢呋喃抽提物的芳香度逐渐降低,抽提率逐渐增大. 展开更多
关键词 固体核磁共振 ^13C CP/MAS/TOSS NMR 热溶产物 前沥青烯 芳香度
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煤及其液化产物的^(13)C CP/MAS/TOSS NMR和ESR研究 被引量:4
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作者 宋瑞 潘铁英 +4 位作者 史新梅 周丽芳 徐熠 张德祥 高晋生 《波谱学杂志》 CAS CSCD 北大核心 2010年第2期206-213,共8页
研究煤及其液化产物的成分和含量的变化是控制煤液化工艺的的重要因素之一.该文章用元素分析,13C CP/MAS/TOSS NMR和ESR的方法分析了不同煤化度的6种原煤,结果表明,不同煤阶的原煤的结构存在较大的差异,原煤的芳香度随着含碳量的增加而... 研究煤及其液化产物的成分和含量的变化是控制煤液化工艺的的重要因素之一.该文章用元素分析,13C CP/MAS/TOSS NMR和ESR的方法分析了不同煤化度的6种原煤,结果表明,不同煤阶的原煤的结构存在较大的差异,原煤的芳香度随着含碳量的增加而变大,芳烃碳原子百分率随芳香度增大而增大,芳香度增大则自由基浓度增大,光谱分裂因子(Landeg值)减小;另外,通过对其中5种原煤及其在CO+H2O气氛下液化得到的产物的ESR分析,推测并验证了原煤在液化阶段中的反应机理,不同煤阶的原煤在反应过程中的变化有所差异,从中可以推测并得到了一些原煤结构方面的信息. 展开更多
关键词 13C CP/MAS/TOSS NMR ESR 不同煤阶的煤 芳香度 液化产物
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促进区域振兴的儿童观光教育
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作者 徐涵(译) 《外国中小学教育》 CSSCI 北大核心 2015年第12期20-25,共6页
随着赴日游客的增多,日本成立了教师志愿者团体TOSS,栃木县举办了"儿童观光大使联合大会",该活动取得了一定效果,并获得了家长和儿童的肯定,并由此推广至日本多个地区。儿童观光教育可以促使儿童认识家乡魅力,发展多方面能力... 随着赴日游客的增多,日本成立了教师志愿者团体TOSS,栃木县举办了"儿童观光大使联合大会",该活动取得了一定效果,并获得了家长和儿童的肯定,并由此推广至日本多个地区。儿童观光教育可以促使儿童认识家乡魅力,发展多方面能力,学会为社会做出自己的贡献,为其未来建设家乡打下基础。为实现以上目的,笔者提出了教师应熟悉当地观光资源,国家应编制相关教材并在《学习指导要领》中增加观光教育相关内容的建议。 展开更多
关键词 TOSS 观光教育 区域振兴
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Shin Shin
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《国际防伪》 2007年第1期46-47,共2页
关键词 经营管理 产品改进 TOSS业务 代理业务 Shin Shin有限公司
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Automated Time Based Multi-Criteria Bug Triage Approach:Developer Working Efficiency and Social Network Based Developer Recommendation
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作者 YADAV Asmita SINGH Kumar Sandeep 《Journal of Shanghai Jiaotong university(Science)》 EI 2024年第3期566-578,共13页
In software development projects,bugs are common phenomena.Developers report bugs in open source repositories.There is a need to develop high quality developer prediction model that considers developer work satisfacti... In software development projects,bugs are common phenomena.Developers report bugs in open source repositories.There is a need to develop high quality developer prediction model that considers developer work satisfaction,keep within limited development cost,and improve bug resolution time.To address and resolve bug report as soon as possible is the main focus of triager when a new bug is reported.Thus,developer work efficiency is an important factor in bug-fixing.To address these issues,a proposed approach recommends a set of developers that could potentially share their knowledge with each other to fix new bug reports.The proposed approach is called developer working efficiency and social network based developer recommendation(DweSn).It is a composite model that builds developers'profile by using developer average bug fixing time,work efficiency to fix variety of bugs,as well as the developer's social interactions with other developers.A similarity measure is applied between new bug and bugs in corpus to extract the list of capable developers from the corpus.The proposed approach only selects those developers who are active and less loaded with work.The developer with the highest profile score is assigned the bugs.We evaluated our approach on the subset of five large open-source projects including Mozilla,Netbeans,Eclipse,Firefox and OpenOffice,and compared it with the state-of-the-art.The results demonstrate that combination of developers'efficiency with their average bug fixing time and interactions in their social network gives good accuracy and efficiently reduces bug tossing length.This approach shows an improvement in prediction accuracy,precision,recall,F-score and reduced bug tossing length up to 93.89%,93.12%,93.46%,93.27%and 93.25%,respectively.The proposed approach achieved a 93%hit ratio and 93.34%mean reciprocal rank,indicating that our proposed triager is able to efficiently assign bugs to correct developers. 展开更多
关键词 open-source repository bug report bug assignment tossing length bug triager developer social network developer recommendation
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Bug Triaging Based on Tossing Sequence Modeling 被引量:1
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作者 Sheng-Qu Xi Yuan Yao +2 位作者 Xu-Sheng Xiao Feng Xu Jian Lv 《Journal of Computer Science & Technology》 SCIE EI CSCD 2019年第5期942-956,共15页
Bug triaging, which routes the bug reports to potential fixers, is an integral step in software development and maintenance. To make bug triaging more efficient, many researchers propose to adopt machine learning and ... Bug triaging, which routes the bug reports to potential fixers, is an integral step in software development and maintenance. To make bug triaging more efficient, many researchers propose to adopt machine learning and information retrieval techniques to identify some suitable fixers for a given bug report. However, none of the existing proposals simultaneously take into account the following three aspects that matter for the efficiency of bug triaging: 1) the textual content in the bug reports, 2) the metadata in the bug reports, and 3) the tossing sequence of the bug reports. To simultaneously make use of the above three aspects, we propose iTriage which first adopts a sequence-to-sequence model to jointly learn the features of textual content and tossing sequence, and then uses a classification model to integrate the features from textual content, metadata, and tossing sequence. Evaluation results on three different open-source projects show that the proposed approach has significantly improved the accuracy of bug triaging compared with the state-of-the-art approaches. 展开更多
关键词 BUG triaging tossing SEQUENCE SOFTWARE REPOSITORY MINING
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Synthesis of La(Ⅲ), Y(Ⅲ) complexes with polyglycol aldehyde-amino acid Schiff base and their high resolution solid state ^(13)C NMR spectra
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作者 李宁 姚克敏 +2 位作者 楼开炎 沈联芳 袁汉珍 《Science China Chemistry》 SCIE EI CAS 1999年第6期599-604,共6页
La(Ⅲ) , Y(Ⅲ) complexes with diglycol aldehyde bis-arginine (H2DAAR) and tetraglycol aldehyde bis-lysine (H2TALY) Schiff bases were synthesized. They were characterized and formulated as La( H2DAAR) (NO3)3 ?6H2Oand Y... La(Ⅲ) , Y(Ⅲ) complexes with diglycol aldehyde bis-arginine (H2DAAR) and tetraglycol aldehyde bis-lysine (H2TALY) Schiff bases were synthesized. They were characterized and formulated as La( H2DAAR) (NO3)3 ?6H2Oand Y (H2TALY)(NO3)3 ·5H2Oseparately by elemental analyses. The obtained complexes were investigated in detail by high resolution solid state (HRSS) 13C NMR using cross polarization, magic angle spinning (CPMAS) , and total suppression of sidebands (TOSS)techniques. The results are supported by the liquid state 2D-1 H-13 C COSY NMR spectra. Some new information about the splitting peaks of 13C for -CH=N- group and alkene carbon bands, etc. in HRSS 13C NMR spectra are given. 展开更多
关键词 Ln (Ⅲ )complexes with Schiff base high resolution solid STATE 13C NMR liquid STATE 2D-1H-13C COSY NMR CPMAS TOSS.
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