Influence of cooling rate on phase transformation and microstructure of Ti-50.9%Ni shape memory alloy

Heat treatment of Ti-50.9%Ni （mole fraction） alloy was studied by differential scanning calorimetry, X-ray diffraction, scanning electron microscopey and energy dispersive X-ray analysis to investigate the influence of cooling rate on transformation behavior and microstructures of NiTi shape memory alloy. The experimental results show that three-stage phase transformation can be induced at a very low cooling rate such as cooling in furnace. The cooling rate also has a great influence on the phase transformation temperatures. Both martensitic start transformation temperature （Ms） and martensitic finish transformation temperature （Mf） decrease with the decrease of the cooling rate, and decreasing the cooling rate contributes to enhancing the M→A austenite transformation temperature. The phase transformation hysteresis （Af-Mf） increases with the decrease of the cooling rate. Heat treatment is unable to eliminate the textures formed in hot working of NiTi sample, but can weaken the intensity of them. The cooling rate has little influence on the grain size.

Effects of long-term fertilization on soil gross N transformation rates and their implications

Application of fertilizer has been found to significantly affect soil N cycling. However, a comprehensive understanding of the effects of long-term fertilization on soil gross N transformation rates is still lacking. We compiled data of observations from 10 long-term fertilization experiments and conducted a meta-analysis of the effects of long-term fertilization on soil gross N transformation rates. The results showed that if chemical fertilizers of N, P and K were applied in balance, soil p H decreased very slightly. There was a significantly positive effect of long-term fertilization, either chemical or organic fertilizers or their combinations, on gross N mineralization rate compared to the control treatment（the mean effect size ranged from 1.21 to 1.25 at 95% confidence intervals（CI） with a mean of 1.23）, mainly due to the increasing soil total N content. The long-term application of organic fertilizer alone and combining organic and chemical fertilizer could increase the mineralization-immobilization turnover, thus enhance available N for plant while reduce N losses potential compared to the control treatment. However, long-term chemical fertilizer application did not significantly affect the gross NH4＋ immobilization rate, but accelerated gross nitrification rate（1.19; 95% CI： 1.08 to 1.31）. Thus, long-term chemical fertilizer alone would probably induce higher N losses potential through NO3– leaching and runoff than organic fertilizer application compared to the control treatment. Therefore, in the view of the effects of long-term fertilization on gross N transformation rates, it also supports that organic fertilizer alone or combination of organic and chemical fertilizer could not only improve crop yield, but also increase soil fertility and reduce the N losses potential.

Influence of temperature rate on transitory internal friction during reverse martensitic transformation for Ti_(50)Ni_(27)Cu_(23) alloy

Internal friction （IF） spectra during reverse martensitic transformation from 35 to 135°C at different temperature rates of 0.5,0.75,and 1°C/min for Ti50Ni27Cu23 shape memory alloy （SMA） samples were measured with a dynamic mechanical analyzer,respectively.The IF spectra were characterized by IF peak increasing progressively and peak shifting toward high temperature with an increase in temperature rate.An iterative approach was used to calculate the precise intrinsic and approximate transitory IF contributions to the normal IF spectrum.The quantitatively analyzed results indicate that the transitory IF of this alloy is nonlinearly dependent on the temperature rate and obeys a power law with a power coefficient of 0.55.The predicted and experimental IF spectra at different temperature rates of 0.75 and 1°C/min agree well with each other,respectively.

A MODEL FOR BAINITIC TRANSFORMATION KINETICS WITH PARABOLIC NUCLEATION RATE

Based on the assumptions of parabolic variation of nucleation rate versus time and transformation kinetics depending mainly on nucleation rate, a different model for bainitic transformation kinetics in hypoeutectoid steels was established. And this model was proved to be effective in the description of bainitic transformation by comparison with the result of conventional Avrami equation.

Influence of Heating Rate on Double Reversible Transformation in CuZnAlMnNi Shape Memory Alloy

The influence of heating rate on double reversible transformation in CuZnAlMnNi shape memory alloy was investigated by differential scanning calorimetry. It was found that rapid heating inhibits X -->M transformation but is favorable to the reverse martensite transformation, giving rise to the approach of the two transformation peaks. With the decrease of heating rate, the two transformation peaks separate gradually.

Dynamics of Nitrogen Transformation and Removal in a Pilot High Rate Pond

The transformation and removal of nitrogen was studied in a pilot high rate pond with a surface area of 10.2 m2 and water depth of 60 cm. The pilot unit received wastewater from an existing field scale primary facultative pond at the University of Dar es Salaam. Wastewater samples were collected from the influent and effluent of high rate pond and were analyzed for physical-chemical parameters in the laboratory and in situ. An appropriate model complexity was selected, from which a conceptual model was then developed to model various processes in the system using STELLA 6.0.1 software. The study demonstrated that dominant nitrogen transformation processes in HRP were nitrification and denitrification, which transformed 0.95 and 0.87 gN/m2·d, respectively. These were followed by mineralization (0.37 gN/m2·d), ammonia uptake by microorganisms (0.34 gN/m2·d), volatilization (0.30 gN/m2·d), sedimentation (0.24 gN/m2·d), and regeneration (0.15 gN/m2·d). Uptake of nitrate was not observed because of microorganisms preference for ammonia, which was abundant in the pond. The major nitrogen transformation mechanisms in high rate pond were denitrification, net sedimentation and volatilization, which accounted for 69.1%, 7.1% and 23.8% of the total permanent removal mechanisms of nitrogen in High Rate Pond.

Improvement of Misclassification Rates of Classifying Objects under Box Cox Transformation and Bootstrap Approach

Discrimination and classification rules are based on different types of assumptions. Also, all most statistical methods are based on some necessary assumptions. Parametric methods are the best choice if it follows all the underlying assumptions. When assumptions are violated, parametric approaches do not provide a better solution and nonparametric techniques are preferred. After Box-Cox transformation, when assumptions are satisfied, parametric methods provide fewer misclassification rates. With this problem in mind, our concern is to compare the classification accuracy of parametric and non-parametric approaches with the aid of Box-Cox transformation and Bootstrapping. We carried Support Vector Machines (SVMs) and different discrimination and classification rules to classify objects. The attention is to critically compare the SVMs with Linear discrimination Analysis (LDA), and Quadratic discrimination Analysis (QDA) for measuring the performance of these techniques before and after Box-Cox transformation using misclassification rates. From the apparent error rates, we observe that before Box-Cox transformation, SVMs perform better than existing classification techniques, on the other hand, after Box-Cox transformation, parametric techniques provide fewer misclassification rates compared to nonparametric method. We also investigated the performances of classification techniques using the Bootstrap approach and observed that Bootstrap-based classification techniques significantly reduce the classification error rate than the usual techniques of small samples. Thus, this paper proposes to apply classification techniques under the Bootstrap approach for classifying objects in case of small sample. A real and simulated datasets application is carried out to see the performance.

Cooling rate effects on the structure and transformation behavior of Cu-Zn-Al shape memory alloys

Different fragments of a hot-rolled and homogenized Cu–Zn–Al shape memory alloy（SMA） were subjected to thermal cycling by means of a differential scanning calorimetric（DSC） device. During thermal cycling, heating was performed at the same constant rate of increasing temperature while cooling was carried out at different rates of decreasing temperature. For each cooling rate, the temperature decreased in the same thermal interval. During each cooling stage, an exothermic peak（maximum） was observed on the DSC thermogram. This peak was associated with forward martensitic transformation. The DSC thermograms were analyzed with PROTEUS software： the critical martensitic transformation start（Ms） and finish（Mf） temperatures were determined by means of integral and tangent methods, and the dissipated heat was evaluated by the area between the corresponding maximum plot and a sigmoid baseline. The effects of the increase in cooling rate, assessed from a calorimetric viewpoint, consisted in the augmentation of the exothermic peak and the delay of direct martensitic transformation. The latter had the tendency to move to lower critical transformation temperatures. The martensite plates changed in morphology by becoming more oriented and by an augmenting in surface relief, which corresponded with the increase in cooling rate as observed by scanning electron microscopy（SEM） and atomic force microscopy（AFM）.

Effect of Weak Light on the Photoassimilates Distribution and Transformation of Young Grape Plants

The effect of weak light on the photoassimilates distribution and transformation of young Jingyu grape plants ( Vitis vinefera L. cv. Jingyu) were studied by shading. Compared to the grape grown under natural light intensity environment, the net photosynthetic rate diurnal variation curve of experimental plants grown in weak light intensity environment was remarkably lower. Its leaf and stem biomass ratio increased when light intensity decreased, the root and new shoot biomass ratio showed an opposite trend. The 14 C-photoassimilates was mostly distributed to young leaves and stem, a little was distributed to root. The metabolism of 14C-photoassimilates distributed to the entire grape body were also changed under weak light intensity environment.

基于Transformer和CNN特征融合的非接触式心率检测算法

心率失调是心血管疾病的常见危险因素,如何及时地对心率失调作出预警,成为了研究的热点。传统的心率检测是接触式的,检测十分不便。远程光电容积脉搏波描记法(Remote photoplethysmography,rPPG)的提出旨在实现无须接触的测量,在许多场景中具有巨大的应用价值。然而,非接触式的测量方法容易受到环境和受试者运动的影响。针对这些问题,本文提出了基于Transformer全局表达和CNN局部特征融合的非接触式心率检测模型(TC-Net)。本文搭建了一个并联的Transformer网络和CNN网络的TC-Net模型。本模型包括两个分支,CNN分支用于提取rPPG信号的局部区域特征,Transformer用于提取rPPG信号的全局表达。由于全局表达特征和局部特征两者特征长度不一,本文提出了特征交互模块,该模块通过卷积层和上下采样模块以对齐两个分支的特征长度。随后,TC-Net通过特征交互模块将局部特征和全局表达进行融合得到最终用于检测的特征向量。最后,在远程心率测量评估中最广泛使用基准之一MAHNOB-HCI数据集上进行对比验证,模型在误差偏差(MAE)、均方根误差(RMSE)和平均绝对百分比误差(MAPE)等三个指标上都达到了最佳水平。因此,本文提出的非接触式心率检测模型TC-Net基于Transformer全局表达和CNN局部特征融合,具有较高的准确性和鲁棒性。此外,TC-Net仅由简单的几层卷积层和注意力层搭建而成,模型复杂度低,便于后续投入实际应用。

EFFECTS OF TEST TEMPERATURE AND STRAIN RATE ON THE MECHANICAL PROPERTIES IN AN INTERCRITICALLYHEAT-TREATED BAINITE-TRANSFORMED STEEL

Larger amount of austenite could be retained in an intercritically heat-treated bainite- transformed steel. The elongation and the strength-ductility balance of the steel could be enhanced considerably due to strain-induced martensite transformation and transformation- induced plasticity (TRIP) of retained austenite. The effects of test temperature and strain rate on the mechanical properties and strain induced transformation behavior of retained austenite in the steel were investigated. Total elongation and strength-ductility balance of the specimen reached maximum when it strained at a strain rate of 2.8×10-4s-1 and at 350℃. The relation between test temperature and tensile properties showed the same tendency at three kinds of strain rates. Flow stress increased considerably with decreasing the strain rate.

Spreading rate dependence of morphological characteristics in global oceanic transform faults

We quantified the systematic variations in global transform fault morphology,revealing a first-order dependence on the spreading rate.(1)The average age offset of both the full transform and transform sub-segments decrease with increasing spreading rate.(2)The average depth of both the transform valley and adjacent ridges are smaller in the fast compared to the slow systems,reflecting possibly density anomalies associated with warmer mantle at the fast systems and rifting at the slow ridges.However,the average depth difference between the transform valley and adjacent ridges is relatively constant from the fast to slow systems.(3)The nodal basin at a ridge-transform intersection is deeper and dominant at the ultraslow and slow systems,possibly reflecting a lower magma supply and stronger viscous resistance to mantle upwelling near a colder transform wall.In contrast,the nodal high,is most prominent in the fast,intermediate,and hotspot-influenced systems,where robust axial volcanic ridges extend toward the ridge-transform intersection.(4)Statistically,the average transform valley is wider at a transform system of larger age offset,reflecting thicker deforming plates flanking the transform fault.(5)The maximum magnitude of the transform earthquakes increases with age offset owing to an increase in the seismogenic area.Individual transform faults also exhibit significant anomalies owing to the complex local tectonic and magmatic processes.

Effect of plunger number on hydraulic transformer's flow pulsation rate

In order to supply theoretical guidance to hydraulic transformer's design and application,the effect of the number of plungers in hydraulic transformer on its flow characteristic is analyzed,theoretical analysis and simulation are done on hydraulic transformer's flow characteristic when the number of plungers is different.Based on the working principle of swash plate piston hydraulic components,mathematical models of instantaneous flow and flow pulsation rate are built,and simulation study is done with MATLAB.As a result,the effect is found,and some conclusions worth referring to are obtained.

MICROSTRUCTURE TRANSFORMATION IN THE WELDING HEAT AFFECTED ZONE OF 800MPa GRADE ULTRA FINE STRUCTURED STEEL

The transformation behavior and microstructure development in the heat affected zone(HAZ)of 800MPa grade ultra fine structured steel was investigated.It was found that the HAZ has intermediate temperature transformation characteristics in a wide range of cooling rates,with the bainite sheaves consisting of bainite ferrite plates without carbide precipitation and retained austenite in the fast cooling regime.At relatively high cooling rates,which corresponded to low heat inputs,the hardness of the simulated HAZ was above that of the base metal.When the cooling rate was below 9C/s,the welding HAZ would have an obvious softening.The analysis of transformation rates in continuous cooling processes was completed by numerical differential method.The result indicated that the microstructure transformation rate of the HAZ in 800MPa grade ultra fine structured steel changed sharply to slow speeds when the cooling time t8/5 is longer than 7s.

Gross nitrogen transformations and N2O emission sources in sandy loam and silt loam soils

The soil type is a key factor influencing N(nitrogen)cycling in soil;however,gross N transformations and N_(2)O emission sources are still poorly understood.In this study,a laboratory 15N tracing experiment was carried out at 60%WHC(water holding capacity)and 25℃to evaluate the gross N transformation rates and N_(2)O emission pathways in sandy loam and silt loam soils in a semi-arid region of Heilongjiang Province,China.The results showed that the gross rates of N mineralization,immobilization,and nitrification were 3.60,1.90,and 5.63 mg N/(kg·d)in silt loam soil,respectively,which were 3.62,4.26,and 3.13 times those in sandy loam soil,respectively.The ratios of the gross nitrification rate to the ammonium immobilization rate(n/ia)in sandy loam soil and silt loam soil were all higher than 1.00,whereas the n/ia in sandy loam soil(4.36)was significantly higher than that in silt loam soil(3.08).This result indicated that the ability of sandy loam soil to release and conserve the available N was relatively poor in comparison with silt loam soil,and the relatively strong nitrification rate compared to the immobilization rate may lead to N loss through NO_(3)–leaching.Under aerobic conditions,both nitrification and denitrification made contributions to N_(2)O emissions.Nitrification was the dominant pathway leading to N_(2)O production in soils and was responsible for 82.0%of the total emitted N_(2)O in sandy loam soil,which was significantly higher than that in silt loam soil(71.7%).However,the average contribution of denitrification to total N_(2)O production in sandy loam soil was 17.9%,which was significantly lower than that in silt loam soil(28.3%).These results are valuable for developing reasonable fertilization management and proposing effective greenhouse gas mitigation strategies in different soil types in semiarid regions.

Roll angular rate extraction based on modified spline-kernelled chirplet transform

The roll angular rate is much crucial for the guidance and control of the projectile.Yet the high-speed rotation of the projectile brings severe challenges to the direct measurement of the roll angular rate.Nevertheless,the radial magnetometer signal is modulated by the high-speed rotation,thus the roll angular rate can be achieved by extracting the instantaneous frequency of the radial magnetometer signal.The objective of this study is to find out a precise instantaneous frequency extraction method to obtain an accurate roll angular rate.To reach this goal,a modified spline-kernelled chirplet transform(MSCT)algorithm is proposed in this paper.Due to the nonlinear frequency modulation characteristics of the radial magnetometer signal,the existing time-frequency analysis methods in literature cannot obtain an excellent energy concentration in the time-frequency plane,thereby leading to a terrible instantaneous frequency extraction accuracy.However,the MSCT can overcome the problem of bad energy concentration by replacing the short-time Fourier transform operator with the Chirp Z-transform operator based on the original spline-kernelled chirplet transform.The introduction of Chirp Z-transform can improve the construction accuracy of the transform kernel.Since the construction accuracy of the transform kernel determines the concentration of time-frequency distribution,the MSCT can obtain a more precise instantaneous frequency.The performance of the MSCT was evaluated by a series of numerical simulations,high-speed turntable experiments,and real flight tests.The evaluation results show that the MSCT has an excellent ability to process the nonlinear frequency modulation signal,and can accurately extract the roll angular rate for the high spinning projectiles.

Chirp-Rate Resolution of Fractional Fourier Transform in Multi-component LFM Signal

Distinguishing close chirp-rates of different linear frequency modulation （LFM） signals under concentrated and complicated signal environment was studied. Firstly, detection and parameter estimation of multi-component LFM signal were used by discrete fast fractional Fourier transform （FrFT）. Then the expression of chirp-rate resolution in fractional Fourier domain （FrFD） was deduced from discrete normalize time-frequency distribution, when multi-component LFM signal had only one center frequency. Furthermore, the detail influence of the sampling time, sampling frequency and chirp-rate upon the resolution was analyzed by partial differential equation. Simulation results and analysis indicate that increasing the sampling time can enhance the resolution, but the influence of the sampling frequency can he omitted. What＇s more, in multi-component LFM signal, the chirp-rate resolution of FrFT is no less than a minimal value, and it mainly dependent on the biggest value of chirp-rates, with which it has an approximately positive exponential relationship.

Dynamic Observation of Bainite Transformation in a Fe-C-Mn-Si Superbainite Steel

The dynamic observations of bainitic transformation in a Fe-C-Mn-Si superbainite steel were conducted on a high temperature laser scanning confocal microscope. It is indicated that the mutual intersection of bainite sheaves often occurs during growth of bainite ferrite, resulting in an interlocked bainite microstructure. Moreover, bainite transformation is promoted by higher austenization temperature and the longer and finer bainite platelets are obtained. Further, The average growth rate of bainite after austenization at 1 100 ℃ is calculated as 5.8 μm·s -1. In situ observation investigation makes it possible to identify bainite transformation in real time during isothermal holding.

CALCULATION OF TRANSFORMATION VOLUME FRACTION TO HQ590 HOT ROLLED STRIP STEEL DURING CONTINUOUS COOLING

On the basis of phase transformation kinetics, the transformation of γ→α,P,B have been investigated through considering the effect of deformation. The calculation methods of volume fraction have also been given. Comparing with common method, the simulated results are in more agreement with experiment results.

DECAY RATE OF FOURIER TRANSFORMS OF SOME SELF-SIMILAR MEASURES

This paper is concerned with the Diophantine properties of the sequence {ξθn}, where 1 ≤ξ 〈 θ and θ is a rational or an algebraic integer. We establish a combinatorial proposition which can be used to study such two cases in the same manner. It is shown that the decay rate of the Fourier transforms of self-similar measures μλ with λ = θ-1 as the uniform contractive ratio is logarithmic. This generalizes some results of Kershner and Bufetov-Solomyak, who consider the case of Bernoulli convolutions. As an application, we prove that μλ ahaost every x is normal to any base b ≥ 2, which implies that there exist infinitely many absolute normal numbers on the corresponding self-similar set. This can be seen as a complementary result of the well-known Cassels-Schmidt theorem.