We analyze a large-scale molecular dynamics simulation of work hardening in a model system of a ductile solid. With tensile loading, we observe emission of thousands of dislocations from two sharp cracks. The dislocat...We analyze a large-scale molecular dynamics simulation of work hardening in a model system of a ductile solid. With tensile loading, we observe emission of thousands of dislocations from two sharp cracks. The dislocations interact in a complex way, revealing three fundamental mechanisms of work-hardening in this ductile material. These are (1) dislocation cutting processes, jog formation and generation of trails of point defects; (2) activation of secondary slip systems by Frank-Read and cross-slip mechanisms; and (3) formation of sessile dislocations such as Lomer-Cottrell locks. We report the discovery of a new class of point defects referred to as trail of partial point defects, which could play an important role in situations when partial dislocations dominate plasticity. Another important result of the present work is the rediscovery of the Fleischer-mechanism of cross-slip of partial dislocations that was theoretically proposed more than 50 years ago, and is now, for the first time, confirmed by atomistic simulation. On the typical time scale of molecular dynamics simulations, the dislocations self-organize into a complex sessile defect topology. Our analysis illustrates numerous mechanisms formerly only conjectured in textbooks and observed indirectly in experiments. It is the first time that such a rich set of fundamental phenomena have been revealed in a single computer simulation, and its dynamical evolution has been studied. The present study exemplifies the simulation and analysis of the complex nonlinear dynamics of a many-particle system during failure using ultra-large scale computing.展开更多
Three characteristic points in the deformation history of a fractured tensile specimen are selected tocalculate two values of n( n1 and n2 ) to represent the hardening ability of material during the homogeneous plas-t...Three characteristic points in the deformation history of a fractured tensile specimen are selected tocalculate two values of n( n1 and n2 ) to represent the hardening ability of material during the homogeneous plas-tic deformation and the following large plastic deformation. Experimental results obtained with mild streel andred copper show that n determined using the three-point method proposed is better to describe the hardening a-bility of material. It is therefore concluded that three-point method can be used to describe the hardening prop-erty of material during both homogeneous deformation and large plastic deformation.展开更多
The instantaneous thermal expansion behavior of-two-phase heterogeneous materials subjected to a uniform temperature change is explored in the present study. The matrix phase is assumed to be a work-hardening ductile ...The instantaneous thermal expansion behavior of-two-phase heterogeneous materials subjected to a uniform temperature change is explored in the present study. The matrix phase is assumed to be a work-hardening ductile metal and the dispersive phase is assumed to consist of either aligned or randomly-oriented, elastic,, spheroidal inhomogeneities. The plastic flow and decreasing stiffness of the matrix during Eshelby's transformation strain of the equivalent inclusions are accounted for by using the deformation theory of plasticity. The explicit results of the instantaneous overall thermal expansion coefficients and the critical inelastic temperature changes are presented for aligned disc- and fiber-inclusions. For the spherical and randomly-oriented spheroidal inclusion, the present study demonstrates that when the yielding of the composites is governed by the average matrix stress, the overall response is always elastic in spite of the temperature change.展开更多
The work-hardening behaviour in an Fe-Mn-Si-Cr-Ni alloy has been investigated using tensile test at different temperatures and TEM observation. It was found that besides the intersection of εmartensite, the intersect...The work-hardening behaviour in an Fe-Mn-Si-Cr-Ni alloy has been investigated using tensile test at different temperatures and TEM observation. It was found that besides the intersection of εmartensite, the intersections of ε martensite with stacking fault and the cross-slip of dislocation which is difficult to occur in the alloy with low stacking fault energy are also important factors to the temperature dependent work-hardening behaviour.展开更多
X-ray diffraction Fourier profile analysis has been performed for polycrystalline α-brass plate with 31.55 wt-% Zn after a series of uniaxial tensile tests with different strain rates. Dislocation density p and confi...X-ray diffraction Fourier profile analysis has been performed for polycrystalline α-brass plate with 31.55 wt-% Zn after a series of uniaxial tensile tests with different strain rates. Dislocation density p and configuration parameter M may be presented as a function of ap- plied stress σ_a.A mechanism of alternative long-range and short-range strain hardening has been proposed.展开更多
The effect of C,Mn and heat-treatment on work-hardening of austenitic Mn steel and the work-hardening mechanism have been investigated under non-severe impact loading condition.The results show that the ability of wor...The effect of C,Mn and heat-treatment on work-hardening of austenitic Mn steel and the work-hardening mechanism have been investigated under non-severe impact loading condition.The results show that the ability of work-hardening in- creases with the increase of C and aging tempera- ture but decreases with Mn.The work-hardening with high austenitic stability results mainly from dislocations,and that with low austenitic stability results mainly from combined effects of strain-in- duced martensite and high density of dislocations under non-severe impact loading conditions.The wear resistance of medium manganese steel (Mn7) is 1.64-2.46 times that of Hadfield steel (Mnl3).展开更多
Work-hardening behaviour of type 316 austenitic stainless steel having difFerent initial dislocation structures introduced by swaging to various levels is analysed by a simplified Kock's model which takes into acc...Work-hardening behaviour of type 316 austenitic stainless steel having difFerent initial dislocation structures introduced by swaging to various levels is analysed by a simplified Kock's model which takes into account the structural changes through the dislocation accumulation and annihilation process during deformation. The dislocation accumulation and annihilation factors show a temperature and structure dependence. The dislocation annihilation factor shows a plateau or decreasing tendency in the dynamic strain ageing (DSA) temperature range. This is attributed as either due to dislocation accumulation being more pronounced than dislocation annihilation or as due to precipitates being formed at DSA temperatures acting as obstacles to dislocation motion in the DSA temperature range.展开更多
The metastable austenite was transformed to martensite by prestrain tension of SUS304 stainless steel to study the influence of transformed martensite on its subsequent work-hardening behavior under the uniaxial tensi...The metastable austenite was transformed to martensite by prestrain tension of SUS304 stainless steel to study the influence of transformed martensite on its subsequent work-hardening behavior under the uniaxial tensile condition. The X-ray diffractometer (XRD) was employed to detect the transformed martensite. Results showed that the volume fraction of transformed martensite increases with increasing prestrain. The pre-transformed martensite in the microstructure remarkably affects the deformation behavior of the steel, and the strength increases and the elongation decreases. The work-hardening curve of prestrained specimens observably changes with true strain. The work-hardening exponent n of stainless steel decreases with the increase of pre-transformed martensite. The achievement is a significant contribution to the process design during pressing.展开更多
A dynamic shakedown theorem for an elasto-kinematic work-hardenlng material with an arbitrary convex yield surface is reviewed. An upper displacement bound for this dynamic shakedown structure is derived. Except for t...A dynamic shakedown theorem for an elasto-kinematic work-hardenlng material with an arbitrary convex yield surface is reviewed. An upper displacement bound for this dynamic shakedown structure is derived. Except for the condition necessary for shakedown of the structure, no other restriction is imposed, which eliminates some of the difficulties appearing in Previous works.展开更多
A new approach is proposed to characterize the work-hardening behavior of metals based on the stress-strain data from uniaxial extension testing.With this new approach,the yield strength as a function of the plastic w...A new approach is proposed to characterize the work-hardening behavior of metals based on the stress-strain data from uniaxial extension testing.With this new approach,the yield strength as a function of the plastic work can be determined by directly fitting a wellchosen single-variable shape function to any given uniaxial data from the initial yielding up to the strength limit,in an explicit sense with no need to carry out the usual tedious trial-and-error procedures in treating nonlinear elastoplastic rate equations toward identifying numerous unknown parameters.Numerical examples show that the simulation results with the new approach are in accurate agreement with the test data.展开更多
Innovative pulsed current-assisted multi-pass rolling tests were conducted on a 12-roll mill during the rolling deformation processing of SUS304 ultra-thin strips.The results show that in the first rolling pass,the ro...Innovative pulsed current-assisted multi-pass rolling tests were conducted on a 12-roll mill during the rolling deformation processing of SUS304 ultra-thin strips.The results show that in the first rolling pass,the rolling reduction rate of a conventionally rolled sample(at room temperature)is 33.8%,which can be increased to 41.5%by pulsed current-assisted rolling,enabling the formation of an ultra-thin strip with a size of 67.3μm in only one rolling pass.After three passes of pulsed current-assisted rolling,the thickness of the ultra-thin strip can be further reduced to 51.7μm.To clearly compare the effects of a pulsed current on the microstructure and mechanical response of the ultra-thin strip,ultra-thin strips with nearly the same thickness reduction were analyzed.It was found that pulsed current can reduce the degree of work-hardening of the rolled samples by promoting dislocation detachment,reducing the density of stacking faults,inhibiting martensitic phase transformation,and shortening the total length of grain boundaries.As a result,the ductility of ultra-thin strips can be effectively restored to approximately 16.3%while maintaining a high tensile strength of 1118 MPa.Therefore,pulsed current-assisted rolling deformation shows great potential for the formation of ultra-thin strips with a combination of high strength and ductility.展开更多
The impact of grain size, ranging from 0.9 μm to 9 μm, on the mechanical properties of commercially pure Mg is investigated at temperatures of 4K, 78K, and 298K. The mechanisms governing plastic flow are influenced ...The impact of grain size, ranging from 0.9 μm to 9 μm, on the mechanical properties of commercially pure Mg is investigated at temperatures of 4K, 78K, and 298K. The mechanisms governing plastic flow are influenced by both grain size and temperature. At 4K and 78K, dominant deformation modes in Mg involve dislocation glide and extension twinning, regardless of grain size. The interactions between basal and non-basal dislocations and dislocations with grain boundaries promote an unusually high rate of work hardening in the plastic regime, leading to premature failure. The yield stress follows the Hall-Petch relationship σy~ k/√d, with the slope k increasing with decreasing temperature. At 298K, in addition to dislocation glide and twinning, grain boundary sliding(GBS) becomes significant in samples with grain sizes below 3 μm, considerably enhancing the material's deformability. GBS activation provides an additional recovery mechanism for dislocations accumulating at grain boundaries, facilitating their absorption during sliding and rotation. Analysis of σ Θ relationship suggests that the basal slip is the dominant dislocation mode in Mg at 298K. Decreasing grain size suppresses dislocation activity and twinning and increases GBS, resulting in lower Θ and σ Θ values. Suppressing conventional deformation modes coupled with enhanced GBS yields stress softening, breaking down the Hall-Petch relationship in Mg below 3 μm grain size, leading to an inverse Hall-Petch behaviour. The work reports new data on the strength, ductility, work hardening and fracture behaviour, and their variations with Mg grain size across different temperature regimes.展开更多
This study has evaluated the effect of different levels of cold rolling(from 0 to 50%)on the microstructural,magnetic,and mechanical properties and the corrosion behavior of 316L austenitic stainless steel in Na Cl...This study has evaluated the effect of different levels of cold rolling(from 0 to 50%)on the microstructural,magnetic,and mechanical properties and the corrosion behavior of 316L austenitic stainless steel in Na Cl(1 mol/L)+H_2SO_4(0.5 mol/L)solution.Microstructural examinations using optical microscopy revealed the development of a morphological texture from coaxial to elongated grains during the cold-rolling process.Phase analysis carried out on the basis of X-ray diffraction confirmed the formation of the ferromagneticα′-martensite phase under the stresses applied during cold rolling.This finding is in agreement with magnetic measurements using a vibrating sample magnetometer.Mechanical properties determined by tensile and Vickers microhardness tests demonstrated an upward trend in the hardness-to-yield strength ratio with increasing cold-rolling percentage,representing a reduction in the material’s work-hardening ability.Uniform and localized corrosion parameters were estimated via potentiodynamic polarization corrosion tests and electrochemical impedance spectroscopy.In contrast to the uniform corrosion,wherein the corrosion current density increased with increasing cold-working degree because of the high density of microstructural defects,the passive potential range and breakdown potential increased by cold working,showing greater resistance to pit nucleation.Although pits were formed,the cold-rolled material repassivation tendency decreased because of the broader hysteresis anodic loop,as confirmed experimentally by observation of the microscopic features after electrochemical cyclic polarization evaluations.展开更多
The tensile and fracture behaviors of AA6061 alloy were investigated in order to provide quantitative data about this alloy at cryogenic temperatures.Specimens of AA6061 alloy were solution heat treated before tensile...The tensile and fracture behaviors of AA6061 alloy were investigated in order to provide quantitative data about this alloy at cryogenic temperatures.Specimens of AA6061 alloy were solution heat treated before tensile tests at 298,173 and 77 K and tested at strain rates in the range from 0.1 to 0.0001 s^(−1).The results indicate the suppression of the Portevin−Le Chatelier(PLC)effect and dynamic strain aging(DSA)at 77 K.In contrast,at 298 K,a remarkable serrated flow,characteristic of the PLC effect,is observed.Furthermore,the tensile behavior at 77 K,compared with that observed at 173 and 298 K,shows a simultaneous increase in strength,uniform elongation,modulus of toughness,strain-hardening exponent and strain rate sensitivity,which is related to a decrease in the dynamic recovery rate at low temperature.These responses are reflected on the fracture morphology,since the dimple size decreases at 77 K,while the area covered by dimples increases.Comparisons of the Johnson−Cook model show that a good agreement can be obtained for tests at 173 and 77 K,in which DSA is suppressed.展开更多
By defining the yield stress in a latent hardening test as the first deviation from the elastic straight line, the yielding and hardening behavior on a latent system in the positive and negative slip direction was stu...By defining the yield stress in a latent hardening test as the first deviation from the elastic straight line, the yielding and hardening behavior on a latent system in the positive and negative slip direction was studied in aluminium single crystals. It is shown that the yield stresses on both the positive and negative latent systems are about equal to or a little lower than the maximum resolved shear stress in the primary test, but much higher than that of the active system. The Influence of relative orientation and prestrain on latent hardening and initial work-hardening in the secondary test was also investigated, and it was found that there is a considerable effect on initial work-hardening, but none on latent hardening. With reasonable approximation, a hardening rule for single crystal could be proposed from the experimental results, that is, except for the yield stress on the system negative to the active system that is very low, hardening on the other systems is nearly the same as self-hardening.展开更多
To prolong the life-span of crush hammers in the pyrite concentrate workplace of Ganbazi Coal Preparation Plant of Chongqing Nantong Mining Ltd., we used a progressive damage constitutive model based on the ductile an...To prolong the life-span of crush hammers in the pyrite concentrate workplace of Ganbazi Coal Preparation Plant of Chongqing Nantong Mining Ltd., we used a progressive damage constitutive model based on the ductile and shear damage fracture energy to analyze the hammer wear failure caused by the impact and abrasion on the hammer surface by pyrite, and carried out simulation analysis with the explicit algurithm on hammer leftovers from the plant during the process of coarser pyrite comminution. The simulation results are consistent with hammer wear failure caused by pyrite impact. Then we proposed corrective measures to prolong hammer life-span. Results of the production test in the Ganbazi Coal Preparation Plant showed that non-clearance hammers can avoid wear erosion, and adding steel bonded tungsten carbides F3002 prolonged the hammer life- span. The effect of austenitic manganese steel work-hardening was not prominent. Therefore, the hammer failure was mainly caused by superficial abrasion instead of fatigue cracks appearing when grains acted on the hardening layer.展开更多
The current work is devoted to the investigation of oxygen impact on the structure and properties of titanium. For this purpose, oxygen was introduced into titanium during chamber electro-slag remelting by three diffe...The current work is devoted to the investigation of oxygen impact on the structure and properties of titanium. For this purpose, oxygen was introduced into titanium during chamber electro-slag remelting by three different methods: alloying by oxygen-rich residues from the Kroll process to final values between 0.053 wt.-% and 0.40 wt.-%, by reaction with the gas phase to 0.27 wt.-% and by introduction of TiO2 nanoparticles to 0.73 wt.-%. The influence of oxygen on microstructure of titanium during crystallization, heat treatment and deformation is determined as well as the effect of oxygen on the hardness and the mechanical properties of the material in different structural states. Furthermore, control methods of the structure formation process by thermal effects are proposed. Results show that the chamber electroslag remelting allows obtaining a homogeneous structure of the ingot in the investigated range of oxygen content in titanium. The hardness does not vary by more than 10 percent in longitudinal or radial direction in any of the remelted ingots.展开更多
The influences of rolling reduction and aluminum sheet initial thickness(AIT)on the thickness fluctuation of aluminum layer(TFA)of embedded aluminum?steel composite sheet produced by cold roll bonding were investigate...The influences of rolling reduction and aluminum sheet initial thickness(AIT)on the thickness fluctuation of aluminum layer(TFA)of embedded aluminum?steel composite sheet produced by cold roll bonding were investigated,the formation mechanism of TFA was analyzed and method to improve the thickness uniformity of the aluminum layer was proposed.The results showed that when the reduction increased,TFA increased gradually.When the reduction was lower than40%,AIT had negligible effect on the TFA,while TFA increased with the decrease of AIT when the reduction was higher than40%.The non-uniformities of the steel surface deformation and the interfacial bonding extent caused by the work-hardened steel surface layer,were the main reasons for the formation of TFA.Adopting an appropriate surface treatment can help to decrease the hardening extent of the steel surface for improving the deformation uniformity during cold roll bonding process,which effectively improved the aluminum thickness uniformity of the embedded aluminum/steel composite sheets.展开更多
The restoration mechanisms for static recrystallization of work-hardened austenite were investigated by using double-pass compression tests performed on medium-carbon steel containing chromium and molybdenum. The soft...The restoration mechanisms for static recrystallization of work-hardened austenite were investigated by using double-pass compression tests performed on medium-carbon steel containing chromium and molybdenum. The softening fraction was defined by 2% offset method. The results show that Avrami exponent of about 0.21 is insensitive to deformation temperature, indicating that the action of steel grade should be considered. The time of 50% recrystallization (t0.5) decreases noteworthily with the increase of deformation temperature. Apparent activation energy for static recrystallization of 195 kJ/mol, which is close to that of vanadium microalloyed steel, is obtained by calculating. The increasing trend of the driving force for recrystallization is opposite to that of the deformation temperature, which is attributed to the number of operative slip system increasing as temperature increasing.展开更多
文摘We analyze a large-scale molecular dynamics simulation of work hardening in a model system of a ductile solid. With tensile loading, we observe emission of thousands of dislocations from two sharp cracks. The dislocations interact in a complex way, revealing three fundamental mechanisms of work-hardening in this ductile material. These are (1) dislocation cutting processes, jog formation and generation of trails of point defects; (2) activation of secondary slip systems by Frank-Read and cross-slip mechanisms; and (3) formation of sessile dislocations such as Lomer-Cottrell locks. We report the discovery of a new class of point defects referred to as trail of partial point defects, which could play an important role in situations when partial dislocations dominate plasticity. Another important result of the present work is the rediscovery of the Fleischer-mechanism of cross-slip of partial dislocations that was theoretically proposed more than 50 years ago, and is now, for the first time, confirmed by atomistic simulation. On the typical time scale of molecular dynamics simulations, the dislocations self-organize into a complex sessile defect topology. Our analysis illustrates numerous mechanisms formerly only conjectured in textbooks and observed indirectly in experiments. It is the first time that such a rich set of fundamental phenomena have been revealed in a single computer simulation, and its dynamical evolution has been studied. The present study exemplifies the simulation and analysis of the complex nonlinear dynamics of a many-particle system during failure using ultra-large scale computing.
文摘Three characteristic points in the deformation history of a fractured tensile specimen are selected tocalculate two values of n( n1 and n2 ) to represent the hardening ability of material during the homogeneous plas-tic deformation and the following large plastic deformation. Experimental results obtained with mild streel andred copper show that n determined using the three-point method proposed is better to describe the hardening a-bility of material. It is therefore concluded that three-point method can be used to describe the hardening prop-erty of material during both homogeneous deformation and large plastic deformation.
基金This work was supported by the National Science Foundation under the Grant 19302017 and 59472031
文摘The instantaneous thermal expansion behavior of-two-phase heterogeneous materials subjected to a uniform temperature change is explored in the present study. The matrix phase is assumed to be a work-hardening ductile metal and the dispersive phase is assumed to consist of either aligned or randomly-oriented, elastic,, spheroidal inhomogeneities. The plastic flow and decreasing stiffness of the matrix during Eshelby's transformation strain of the equivalent inclusions are accounted for by using the deformation theory of plasticity. The explicit results of the instantaneous overall thermal expansion coefficients and the critical inelastic temperature changes are presented for aligned disc- and fiber-inclusions. For the spherical and randomly-oriented spheroidal inclusion, the present study demonstrates that when the yielding of the composites is governed by the average matrix stress, the overall response is always elastic in spite of the temperature change.
文摘The work-hardening behaviour in an Fe-Mn-Si-Cr-Ni alloy has been investigated using tensile test at different temperatures and TEM observation. It was found that besides the intersection of εmartensite, the intersections of ε martensite with stacking fault and the cross-slip of dislocation which is difficult to occur in the alloy with low stacking fault energy are also important factors to the temperature dependent work-hardening behaviour.
文摘X-ray diffraction Fourier profile analysis has been performed for polycrystalline α-brass plate with 31.55 wt-% Zn after a series of uniaxial tensile tests with different strain rates. Dislocation density p and configuration parameter M may be presented as a function of ap- plied stress σ_a.A mechanism of alternative long-range and short-range strain hardening has been proposed.
文摘The effect of C,Mn and heat-treatment on work-hardening of austenitic Mn steel and the work-hardening mechanism have been investigated under non-severe impact loading condition.The results show that the ability of work-hardening in- creases with the increase of C and aging tempera- ture but decreases with Mn.The work-hardening with high austenitic stability results mainly from dislocations,and that with low austenitic stability results mainly from combined effects of strain-in- duced martensite and high density of dislocations under non-severe impact loading conditions.The wear resistance of medium manganese steel (Mn7) is 1.64-2.46 times that of Hadfield steel (Mnl3).
文摘Work-hardening behaviour of type 316 austenitic stainless steel having difFerent initial dislocation structures introduced by swaging to various levels is analysed by a simplified Kock's model which takes into account the structural changes through the dislocation accumulation and annihilation process during deformation. The dislocation accumulation and annihilation factors show a temperature and structure dependence. The dislocation annihilation factor shows a plateau or decreasing tendency in the dynamic strain ageing (DSA) temperature range. This is attributed as either due to dislocation accumulation being more pronounced than dislocation annihilation or as due to precipitates being formed at DSA temperatures acting as obstacles to dislocation motion in the DSA temperature range.
基金Item Sponsored by National Natural Science Foundation of China (50675128 50975166)
文摘The metastable austenite was transformed to martensite by prestrain tension of SUS304 stainless steel to study the influence of transformed martensite on its subsequent work-hardening behavior under the uniaxial tensile condition. The X-ray diffractometer (XRD) was employed to detect the transformed martensite. Results showed that the volume fraction of transformed martensite increases with increasing prestrain. The pre-transformed martensite in the microstructure remarkably affects the deformation behavior of the steel, and the strength increases and the elongation decreases. The work-hardening curve of prestrained specimens observably changes with true strain. The work-hardening exponent n of stainless steel decreases with the increase of pre-transformed martensite. The achievement is a significant contribution to the process design during pressing.
文摘A dynamic shakedown theorem for an elasto-kinematic work-hardenlng material with an arbitrary convex yield surface is reviewed. An upper displacement bound for this dynamic shakedown structure is derived. Except for the condition necessary for shakedown of the structure, no other restriction is imposed, which eliminates some of the difficulties appearing in Previous works.
基金This study was carried out under the support of the start-up fund from Jinan University(Guangzhou)the fund from the Natural Science Foundation of China(No.11372172).
文摘A new approach is proposed to characterize the work-hardening behavior of metals based on the stress-strain data from uniaxial extension testing.With this new approach,the yield strength as a function of the plastic work can be determined by directly fitting a wellchosen single-variable shape function to any given uniaxial data from the initial yielding up to the strength limit,in an explicit sense with no need to carry out the usual tedious trial-and-error procedures in treating nonlinear elastoplastic rate equations toward identifying numerous unknown parameters.Numerical examples show that the simulation results with the new approach are in accurate agreement with the test data.
基金This work was supported by the fund of the National Natural Science Foundation of China(51974196)Major Program of National Natural Science Foundation of China(U22A20188)+1 种基金Science and Technology Innovation Teams of Shanxi Province(202304051001025)Central Government Guides the Special Fund Projects of Local Scientific and Technological Development(YDZX20191400002149).
文摘Innovative pulsed current-assisted multi-pass rolling tests were conducted on a 12-roll mill during the rolling deformation processing of SUS304 ultra-thin strips.The results show that in the first rolling pass,the rolling reduction rate of a conventionally rolled sample(at room temperature)is 33.8%,which can be increased to 41.5%by pulsed current-assisted rolling,enabling the formation of an ultra-thin strip with a size of 67.3μm in only one rolling pass.After three passes of pulsed current-assisted rolling,the thickness of the ultra-thin strip can be further reduced to 51.7μm.To clearly compare the effects of a pulsed current on the microstructure and mechanical response of the ultra-thin strip,ultra-thin strips with nearly the same thickness reduction were analyzed.It was found that pulsed current can reduce the degree of work-hardening of the rolled samples by promoting dislocation detachment,reducing the density of stacking faults,inhibiting martensitic phase transformation,and shortening the total length of grain boundaries.As a result,the ductility of ultra-thin strips can be effectively restored to approximately 16.3%while maintaining a high tensile strength of 1118 MPa.Therefore,pulsed current-assisted rolling deformation shows great potential for the formation of ultra-thin strips with a combination of high strength and ductility.
基金Financial support from National Science Centre of Poland under the OPUS project No.2021/43/B/ST5/00730 is gratefully acknowledgedsupport from the Natural Sciences and Engineering Research Council of Canada(NSERC)。
文摘The impact of grain size, ranging from 0.9 μm to 9 μm, on the mechanical properties of commercially pure Mg is investigated at temperatures of 4K, 78K, and 298K. The mechanisms governing plastic flow are influenced by both grain size and temperature. At 4K and 78K, dominant deformation modes in Mg involve dislocation glide and extension twinning, regardless of grain size. The interactions between basal and non-basal dislocations and dislocations with grain boundaries promote an unusually high rate of work hardening in the plastic regime, leading to premature failure. The yield stress follows the Hall-Petch relationship σy~ k/√d, with the slope k increasing with decreasing temperature. At 298K, in addition to dislocation glide and twinning, grain boundary sliding(GBS) becomes significant in samples with grain sizes below 3 μm, considerably enhancing the material's deformability. GBS activation provides an additional recovery mechanism for dislocations accumulating at grain boundaries, facilitating their absorption during sliding and rotation. Analysis of σ Θ relationship suggests that the basal slip is the dominant dislocation mode in Mg at 298K. Decreasing grain size suppresses dislocation activity and twinning and increases GBS, resulting in lower Θ and σ Θ values. Suppressing conventional deformation modes coupled with enhanced GBS yields stress softening, breaking down the Hall-Petch relationship in Mg below 3 μm grain size, leading to an inverse Hall-Petch behaviour. The work reports new data on the strength, ductility, work hardening and fracture behaviour, and their variations with Mg grain size across different temperature regimes.
基金Shahid Chamran University of Ahvaz for supporting this research
文摘This study has evaluated the effect of different levels of cold rolling(from 0 to 50%)on the microstructural,magnetic,and mechanical properties and the corrosion behavior of 316L austenitic stainless steel in Na Cl(1 mol/L)+H_2SO_4(0.5 mol/L)solution.Microstructural examinations using optical microscopy revealed the development of a morphological texture from coaxial to elongated grains during the cold-rolling process.Phase analysis carried out on the basis of X-ray diffraction confirmed the formation of the ferromagneticα′-martensite phase under the stresses applied during cold rolling.This finding is in agreement with magnetic measurements using a vibrating sample magnetometer.Mechanical properties determined by tensile and Vickers microhardness tests demonstrated an upward trend in the hardness-to-yield strength ratio with increasing cold-rolling percentage,representing a reduction in the material’s work-hardening ability.Uniform and localized corrosion parameters were estimated via potentiodynamic polarization corrosion tests and electrochemical impedance spectroscopy.In contrast to the uniform corrosion,wherein the corrosion current density increased with increasing cold-working degree because of the high density of microstructural defects,the passive potential range and breakdown potential increased by cold working,showing greater resistance to pit nucleation.Although pits were formed,the cold-rolled material repassivation tendency decreased because of the broader hysteresis anodic loop,as confirmed experimentally by observation of the microscopic features after electrochemical cyclic polarization evaluations.
基金We would like to acknowledge the Sao Paulo Research Foundation(FAPESP)(Grant No.2014/15091-7 and 2016/10997-0)the Conselho Nacional de Desenvolvimento Científico e Tecnológico-Brazil(CNPq)(Grant No.449009/2014-9)This study was financed in part by the Coordenacao de Aperfeicoamento de Pessoal de Nivel Superior-Brazil(CAPES)-Finance Code 001.Danielle Cristina Camilo MAGALHÃES acknowledges CNPq for her PhD scholarship(Grant No.153181/2013-3).
文摘The tensile and fracture behaviors of AA6061 alloy were investigated in order to provide quantitative data about this alloy at cryogenic temperatures.Specimens of AA6061 alloy were solution heat treated before tensile tests at 298,173 and 77 K and tested at strain rates in the range from 0.1 to 0.0001 s^(−1).The results indicate the suppression of the Portevin−Le Chatelier(PLC)effect and dynamic strain aging(DSA)at 77 K.In contrast,at 298 K,a remarkable serrated flow,characteristic of the PLC effect,is observed.Furthermore,the tensile behavior at 77 K,compared with that observed at 173 and 298 K,shows a simultaneous increase in strength,uniform elongation,modulus of toughness,strain-hardening exponent and strain rate sensitivity,which is related to a decrease in the dynamic recovery rate at low temperature.These responses are reflected on the fracture morphology,since the dimple size decreases at 77 K,while the area covered by dimples increases.Comparisons of the Johnson−Cook model show that a good agreement can be obtained for tests at 173 and 77 K,in which DSA is suppressed.
文摘By defining the yield stress in a latent hardening test as the first deviation from the elastic straight line, the yielding and hardening behavior on a latent system in the positive and negative slip direction was studied in aluminium single crystals. It is shown that the yield stresses on both the positive and negative latent systems are about equal to or a little lower than the maximum resolved shear stress in the primary test, but much higher than that of the active system. The Influence of relative orientation and prestrain on latent hardening and initial work-hardening in the secondary test was also investigated, and it was found that there is a considerable effect on initial work-hardening, but none on latent hardening. With reasonable approximation, a hardening rule for single crystal could be proposed from the experimental results, that is, except for the yield stress on the system negative to the active system that is very low, hardening on the other systems is nearly the same as self-hardening.
文摘To prolong the life-span of crush hammers in the pyrite concentrate workplace of Ganbazi Coal Preparation Plant of Chongqing Nantong Mining Ltd., we used a progressive damage constitutive model based on the ductile and shear damage fracture energy to analyze the hammer wear failure caused by the impact and abrasion on the hammer surface by pyrite, and carried out simulation analysis with the explicit algurithm on hammer leftovers from the plant during the process of coarser pyrite comminution. The simulation results are consistent with hammer wear failure caused by pyrite impact. Then we proposed corrective measures to prolong hammer life-span. Results of the production test in the Ganbazi Coal Preparation Plant showed that non-clearance hammers can avoid wear erosion, and adding steel bonded tungsten carbides F3002 prolonged the hammer life- span. The effect of austenitic manganese steel work-hardening was not prominent. Therefore, the hammer failure was mainly caused by superficial abrasion instead of fatigue cracks appearing when grains acted on the hardening layer.
文摘The current work is devoted to the investigation of oxygen impact on the structure and properties of titanium. For this purpose, oxygen was introduced into titanium during chamber electro-slag remelting by three different methods: alloying by oxygen-rich residues from the Kroll process to final values between 0.053 wt.-% and 0.40 wt.-%, by reaction with the gas phase to 0.27 wt.-% and by introduction of TiO2 nanoparticles to 0.73 wt.-%. The influence of oxygen on microstructure of titanium during crystallization, heat treatment and deformation is determined as well as the effect of oxygen on the hardness and the mechanical properties of the material in different structural states. Furthermore, control methods of the structure formation process by thermal effects are proposed. Results show that the chamber electroslag remelting allows obtaining a homogeneous structure of the ingot in the investigated range of oxygen content in titanium. The hardness does not vary by more than 10 percent in longitudinal or radial direction in any of the remelted ingots.
基金Project(2013AA031301)supported by National High-tech Research and Development Program of ChinaProject(51104016)supported by National Natural Science Foundation of ChinaProject(BM2014006)supported by Jiangsu Key Laboratory for Clad Materials,China
文摘The influences of rolling reduction and aluminum sheet initial thickness(AIT)on the thickness fluctuation of aluminum layer(TFA)of embedded aluminum?steel composite sheet produced by cold roll bonding were investigated,the formation mechanism of TFA was analyzed and method to improve the thickness uniformity of the aluminum layer was proposed.The results showed that when the reduction increased,TFA increased gradually.When the reduction was lower than40%,AIT had negligible effect on the TFA,while TFA increased with the decrease of AIT when the reduction was higher than40%.The non-uniformities of the steel surface deformation and the interfacial bonding extent caused by the work-hardened steel surface layer,were the main reasons for the formation of TFA.Adopting an appropriate surface treatment can help to decrease the hardening extent of the steel surface for improving the deformation uniformity during cold roll bonding process,which effectively improved the aluminum thickness uniformity of the embedded aluminum/steel composite sheets.
文摘The restoration mechanisms for static recrystallization of work-hardened austenite were investigated by using double-pass compression tests performed on medium-carbon steel containing chromium and molybdenum. The softening fraction was defined by 2% offset method. The results show that Avrami exponent of about 0.21 is insensitive to deformation temperature, indicating that the action of steel grade should be considered. The time of 50% recrystallization (t0.5) decreases noteworthily with the increase of deformation temperature. Apparent activation energy for static recrystallization of 195 kJ/mol, which is close to that of vanadium microalloyed steel, is obtained by calculating. The increasing trend of the driving force for recrystallization is opposite to that of the deformation temperature, which is attributed to the number of operative slip system increasing as temperature increasing.