Fast X-ray imaging beamline at SSRF

The fast X-ray imaging beamline(BL16U2)at Shanghai Synchrotron Radiation Facility(SSRF)is a new beamline that provides X-ray micro-imaging capabilities across a wide range of time scales,spanning from 100 ps toμs and ms.This beamline has been specifically designed to facilitate the investigation of a wide range of rapid phenomena,such as the deformation and failure of materials subjected to intense dynamic loads.In addition,it enables the study of high-pressure and high-speed fuel spray processes in automotive engines.The light source of this beamline is a cryogenic permanent magnet undulator(CPMU)that is cooled by liquid nitrogen.This CPMU can generate X-ray photons within an energy range of 8.7-30 keV.The beamline offers two modes of operation:monochromatic beam mode with a liquid nitrogen-cooled double-crystal monochromator(DCM)and pink beam mode with the first crystal of the DCM out of the beam path.Four X-ray imaging methods were implemented in BL16U2:single-pulse ultrafast X-ray imaging,microsecond-resolved X-ray dynamic imaging,millisecond-resolved X-ray dynamic micro-CT,and high-resolution quantitative micro-CT.Furthermore,BL16U2 is equipped with various in situ impact loading systems,such as a split Hopkinson bar system,light gas gun,and fuel spray chamber.Following the completion of the final commissioning in 2021 and subsequent trial operations in 2022,the beamline has been officially available to users from 2023.

Comparison of efficacy of lung ultrasound and chest X-ray in diagnosing pulmonary edema and pleural effusion in ICU patients: A single centre, prospective, observational study

Background and Aims While chest X-ray (CXR) has been a conventional tool in intensive care units (ICUs) to identify lung pathologies, computed tomography (CT) scan remains the gold standard. Use of lung ultrasound (LUS) in resource-rich ICUs is still under investigation. The present study compares the utility of LUS to that of CXR in identifying pulmonary edema and pleural effusion in ICU patients. In addition, consolidation and pneumothorax were analyzed as secondary outcome measures. Material and Methods This is a prospective, single centric, observational study. Patients admitted in ICU were examined for lung pathologies, using LUS by a trained intensivist;and CXR done within 4 hours of each other. The final diagnosis was ascertained by an independent senior radiologist, based on the complete medical chart including clinical findings and the results of thoracic CT, if available. The results were compared and analyzed. Results Sensitivity, specificity and diagnostic accuracy of LUS was 95%, 94.4%, 94.67% for pleural effusion;and 98.33%, 97.78%, 98.00% for pulmonary edema respectively. Corresponding values with CXR were 48.33%, 76.67%, 65.33% for pleural effusion;and 36.67%, 82.22% and 64.00% for pulmonary edema respectively. Sensitivity, specificity and diagnostic accuracy of LUS was 91.30%, 96.85%, 96.00% for consolidation;and 100.00%, 79.02%, 80.00% for pneumothorax respectively. Corresponding values with CXR were 60.87%, 81.10%, 78.00% for consolidation;and 71.3%, 97.20%, 96.00% for pneumothorax respectively. Conclusion LUS has better diagnostic accuracy in diagnosis of pleural effusion and pulmonary edema when compared with CXR and is thus recommended as an effective alternative for diagnosis of these conditions in acute care settings. Our study recommends that a thoracic CT scan can be avoided in most of such cases.

超新星遗迹和脉冲星风云的X射线偏振成像

年轻超新星遗迹和脉冲星风云中的高能粒子可以通过同步辐射产生X射线。对该辐射的偏振测量有助于揭示粒子加速区磁场的性质,进而研究粒子加速的机制。首颗X射线偏振成像卫星于2021年底发射升空,已揭示了数个年轻超新星遗迹和脉冲星风云的X射线偏振图像。观测显示,仙后A和第谷超新星遗迹的偏振度较低,平均值分别约为2.5%和9%;而蟹状星云和船帆脉冲星风云的偏振度较高,平均值分别约为20%和45%。结果表明脉冲星风云的磁场较为有序,而两个年轻超新星遗迹的粒子加速区磁场是高度湍动的,且激波附近的磁场结构呈现径向分布。未来,随着对IXPE的使用越来越广泛,以及与我国建设中的增强型X射线时变与偏振探测器(eXTP)等更多望远镜投入使用,以上两类天体的磁场构型和粒子加速模型将得到进一步的限定。

Journey through the birth, growth and maturity of X-ray astronomy

In this biographical account, I recall my scientific journey that began in 1961 when I joined as a Physics Trainee in the BARC Training School and after one year course was admitted in TIFR as a Research Associate. During 1962–1967, I worked on determination of the He^3 /He^4 ratio in cosmic rays using a gas Cerenkov counter and also used a scintillation + solid Cerenkov detector to measure flux of protons and helium nuclei in primary cosmic rays. I also developed a large area scintillation-Cerenkov detector with a spark chamber between them for measuring charge composition of primary cosmic rays. I joined the X-ray astronomy programme in 1967 initiated by Prof. B. V. Sreekantan and played a leading role in developing a balloon borne hard X-ray instrument for studying time variability and energy spectra of cosmic X-ray sources. We carried out a series of balloon experiments and studied temporal intensity variation and energy spectra of X-ray objects like Sco X-1, Cyg X-1, etc. Results on rapid intensity changes and spectra appeared in a series of publications based on which I obtained a Ph.D. degree in 1972. Immediately afterwards, I joined Prof. Gordon Garmire at Caltech as a Research Fellow (a post-doctoral position) to work with him on the low energy component of HEAO A-2 experiment. The instrument was developed and successfully realised. Working on this satellite experiment was a thrilling experience which exposed me to the technical complexities of space instruments. The HEAO-1 satellite was launched in 1978. During 1978–1979, Guenter Riegler and I, working at JPL, reported detection of intense soft X-rays from several classes of extragalactic and Galactic objects like new BL Lacs, a new AM Her binary, coronal X-rays from active stars, etc. After returning to TIFR, I developed a rocket experiment with K. P. Singh to map the spatial and spectral distribution of the Soft Diffuse X-ray Background. At the same time, I also designed 15 cm deep Xenon filled Proportional Counters (XPCs) of ~ 2500 cm^2 area for balloon experiments which were done during 1983–1990 and produced new results on several X-ray binaries. During this period I also developed a proportional counter (PC) based satellite instrument and submitted a proposal jointly with the astronomy group at the Indian Space Research Organization (ISRO) for an Indian X-ray Astronomy Experiment (IXAE). After success of the Polar Satellite Launch Vehicle (PSLV), the IXAE instrument was included on the top deck of the IRS-P3 satellite that was launched in March 1996. Despite the severe limitation of a polar orbit, the IXAE observed a good number of X-ray binaries and produced interesting results, with the most notable being quasi-regular bursts from a new transient, GRS 1915+105, which turned out to be an enigmatic black hole source. Following success of the IXAE, a proposal for an ambitious multiwavelength astronomy satellite, named ASTROSAT, with broad spectral coverage in the optical, NUV, FUV, soft X-ray and hard X-ray by a suite of instruments, was submitted to ISRO and finally approved by the Govt. of India in 2004. Over the next 10 years, the development and fabrication of the five ASTROSAT instruments were accomplished and a PSLV launch on Sept. 28, 2015 placed ASTROSAT in a 650 km circular orbit with 6 degree inclination. The ASTROSAT instruments have been performing well for ~4 years and have observed more than 500 cosmic sources. Results from ASTROSAT have appeared in a large number of journal publications. Successful realization and performance of ASTROSAT marks culmination of my research career. I formally retired as a Senior Professor from TIFR on 2006 April 30 on attaining the age of superannuation. However by agreement with TIFR, ISRO designated me ‘ISRO Chair Professor’, which was later renamed as ISRO Satish Dhawan Professor, and asked me to continue to lead ASTROSAT as PI. At the end of my tenure as ISRO Professor on 2011 April 30, I relinquished the PI position. I am at present affiliated with the MU-DAE Centre of Excellence for Basic Sciences, Mumbai University Campus at Mumbai as an Emeritus Professor.

上海光源储存环X-ray针孔相机系统设计

上海光源(SSRF)储存环X-ray针孔相机系统主要由X-ray引出前端、衰减片、小孔、靶片、相机、PXI控制器及图像采集等构成,数据采集处理软件在LabVIEW平台上开发,与控制系统的接口通过EPICS Shared Memory IOCcore技术实现。2009年8月开始的长时间在线运行证明引出前端是安全的,在300mA运行时,测量引出窗的最高温度≤36℃。该系统设计合理、性能稳定,可在线实时测量数十μm束团横向截面尺寸,从而实现3.9nm·rad发射度的测量。

Soft X ray Diagnosis on Seed Development and Observation on Seed Germination and Seedling Growth in Artificial Hybridization in Cunninghamia and Cryptomeria

An intergeneric artificial hybridization was conducted between Cunninghamia R. Br. and Cryptomeria D.Don The results are as follows:1. A considerable number of hybrid seeds shed from 76 pollinated cones were empty and a total of 628 looks plump. Soft X ray radiographs showed that, still and all, a majority of the “plump" seeds were embryoless (597, 95.6%) whereas some were partially developed (17,2.7%) and only a few were really full (14, 2.2%). 2. Germination test showed that all of the radiographed hybrid seeds with fully developed embryos were germinable whereas those with partially developed embryos were ungerminable. 3. Physiologically, the growth rate of hypocotyl, the date for shedding of seed coat and spreading of cotyledons, the elongation of epicotyl, and the branching of shoot of the 11 month old seedlings showed a tendency to fall behind those of the female parent; morphologically, the 11 month old hybrid seedlings with linear leaves appeared rather short, slender and weak, whereas the seedlings of the female parents with linear_lanceolate leaves appeared rather tall, stout and strong. 4. It is considered that the hybrid may be true and the crossability reveals a close phylogenetic affinity of Cunninghamia with Cryptomeria.

INTERFACIAL BONDING IN AS DEPOSITED AND ANNEALED Co/C SOFT X RAY MULTILAYER MIRRORS

Interfacial bonding in as deposited and annealed Co/C soft X ray multilayer structures is investigated by X ray photo electron spectroscopy (XPS).It is found that there is interdiffusion between cobalt and carbon in the as deposited Co/C multilayers,and this is confirmed by structure characterization using low angle X ray diffraction (LAXD).The calculation of the chemical shifts in Co C system based on Miedemas macroscopic atom model suggests that it is impossible to detect the chemical shift experimentally in the Co C compound,which is consistent with the XPS results.The presence of metallic carbide bonding is evidenced through the nature of the carbon bonding in survey taken at Co C and C Co interfaces of annealed samples.Our results also indicate that XPS is a direct method to probe the chemical bonding at the interfaces.

A Straightforward Method of Calculating Finely the Soft X-Ray Spectra of Hydrogenlike Highly Ionized-States

A new method of calculating finely the soft X ray spectra of hydrogenlike highly ionized states is presented. It is based on the relation of the ionicity and the ionization energies of hydrogenlike atoms and the new model of potential function of hydrogenlike atoms. The relativistic revision and the spin orbit couping of excitation energy levels are taken into account. The calculated results are in good agreement with the experiments.

胞元结构X-Ray三维成像及其FEM模拟

采用微纳米X-Ray断面成像技术,通过对含有CaCl2生物淀粉膨化结构材料三维成像规律的研究,确定了胞元体结构形态,并分析了断层胞元分布规律.建立了带有微细孔洞结构材料三维几何描述模型,通过理论建模和数字编程实现了与非线性有限元的连接,分析了微米级胞体材料受载后的场变量分布.

联合应用近红外线、高频超声、钼靶x—ray对乳腺癌的早期诊断分析

目的：比较应用近红外线、高频超声、钼靶x—ray各自对乳腺癌早期诊断的价值，探讨联合应用近红外线、高频超声、钼靶x—ray对乳腺癌早期诊断的价值。方法：对81例经近红外线扫描、经B超检查、钼钯X线检查的病例进行回顾性总结，对三种影像学方法在乳腺癌诊断中的价值和优缺点进行了分析比较。结论诊断符合率分别为：近红外线83％，B超92．5％，钼钯X线93％，联合应用96％。联合应用近红外线、高频超声、钼靶x—ray有助于提高乳腺癌的诊断率和判断手术范围及术后效果，具有较大的临床价值。

DIFFERENTIAL SCANNING CALORIMETRY AND X-RAY DIFFRACTION STUDIES ON AGING BEHAVIOR OF Zn-Al ALLOYS

Decomposition processes of the quenched Zn-Al alloys were studied by differential scanning calorimetry (DSC), X-ray diffraction (XRD) and transmission electron microscopy (TEM). The results show that the stabilities of supersaturated solid solution (SSS) of Zn-Al alloy and α' phase formed by quenching would reduce with the increase of Zn content and the precipitation of η-Zn phases even when aging at ambient temperature, so that the exothermic precipitation peak in DSC curve would disappear. The activation energy of the η-Zn precipitation and the reaction enthalpy were calculated and measured. The kinetics of α' decomposition or η-Zn formation was determined by XRD. The microstructure change during aging was observed by TEM.

Exploring the Dynamic X-ray Universe:Scientific Opportunities for the Einstein Probe Mission

Time-domain astrophysics will enter a golden era towards the end of this decade with the advent of major facilities across the electromagnetic spectrum and in the multi-messenger realms of gravitational wave and neutrino.In the soft X-ray regime,the novel micro-pore lobster-eye optics provides a promising technology to realise,for the first time,focusing X-ray optics for wide-angle monitors to achieve a good combination of sensitivity and wide field of view.In this context Einstein Probe,a soft X-ray all-sky monitor mission,was proposed and selected as a candidate mission of priority in the space science programme of the Chinese Academy of Sciences.This paper reviews the most important science developments and key questions in this field towards 2020 and beyond,and how to achieve them technologically.It also introduces the Einstein Probe mission,including its key science goals and mission definition,as well as some of the key technological issues.

Study of NdCl_3-FeCl_3-Graphite Intercalation Compounds by X-Ray Photoelectron Spectroscopy

NdCl 3 FeCl 3 graphite intercalation compounds were synthesized by molten salt exchange method. The state of the intercalates and the relative contents of Nd, Fe, Cl, C in the product were determined by X ray photoelectron spectroscopy(XPS). From the XPS data, it is concluded that the binding energy of Fe2p electrons is about 711 20～710 3 eV, the binding energy of Nd3d electrons is about 983 08～983 20 eV, and Fe in the product has two valence states (Fe 3+ and Fe 2+ ).

X-ray Powder Diffraction Data and Crystal Structure of NiSbY

X-ray powder diffraction data and crystal structure of NiSbY compound were studied by X-ray powderdiffraction. The compound belongs to the space group F43 m with MgAgAs structure type, and the parameters Z=4, a=0.63075(2) nm.

X-RAY POWDER DIFFRACTION DATA AND STRUCTURAL PARAMETERS FOR RECOMPOUND NdCo_0.6Sb_2

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X-ray elastic constant determination and residual stress of two phase TiAl-based intermetallic alloy

To evaluate the residual stress in TiAl based alloys by X ray diffraction, X ray elastic constants (REC) of a γ TiAl alloy were determined. From these results, the stress state of a given phase in a duplex TiAl based alloy under a uniaxial tensile loading has been characterized by X ray diffraction. The results show that the X ray elastic constants and the microscopic stresses of the given phase are different from the apparent elastic constants and the macroscopic stresses of the alloy. The reason of the different distribution of the alloy was also discussed. [

Crystal Structure and X-ray Powder Diffraction Data for Rare Earth Compound PrNiSn

The compound PrNiSn was studied by X ray powder diffraction technique. The crystal structure and the X ray diffraction data for this compound at room temperature were reported. The compound PrNiSn is orthorhombic with lattice parameters a =0.74569(3) nm, b =0.76851(5) nm, c =0.45676(8) nm, V =0.26176 nm 3, Z =4 and D x=8.076 g·cm -3 , space group Pna2 1(33). The figure of merit F N for the compound is F 30 =54 (0.0093, 60).

X-RAY POWDER DIFFRACTION DATA AND STRUCTURE REFINEMENT OF COMPOUND ErNi_2Si_2

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X-RAY POWDER DIFFRACTION DATA AND STRUCTURAL REFINEMENT OF Er3Co6Sn5

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Nested grazing incidence optics for x ray detection

Grazing incidence optics （GIO） is the most important compound in an x-ray detection system; it is used to concentrate the x-ray photons from outer space. A nested planar GIO for x-ray concentration is designed and developed by authors in this paper; planar segments are used as the reflection mirror instead of curved segments because of the simple process and low cost. After the complex assembling process with a special metal supporter, a final circle light spot of φ 12 mm was obtained in the visible light testing experiment of GIO; the effective area of 1710.51 mm^2@ 1 keV and 530 mm^2@8 keV is obtained in the x-ray testing experiment with the GIO-SDD combination, which is supposed to be a concentrating detector in xray detection systems.