Pre-heat treatment is a vital step before cold ring rolling and it has significant effect on the microstructure and mechanical properties of rolled rings.The 100Cr6 steel rings were subjected to pre-heat treatment and...Pre-heat treatment is a vital step before cold ring rolling and it has significant effect on the microstructure and mechanical properties of rolled rings.The 100Cr6 steel rings were subjected to pre-heat treatment and subsequent cold rolling process.Scanning electron microscopy and tensile tests were applied to investigate microstructure characteristic and mechanical property variations of 100Cr6 steel rings undergoing different pre-heat treatings.The results indicate that the average diameter of carbide particles,the tensile strength and hardness increase,while the elongation decreases with the decrease of cooling rate.The cooling rate has minor effect on the yield strength of sample.After cold ring rolling,the ferrite matrix shows a clear direction along the rolling direction.The distribution of cementite is more homogeneous and the cementite particles are finer.Meanwhile,the hardness of the rolled ring is higher than that before rolling.展开更多
The reformation of (Bi,Pb)-2223 from the liquid or melt is very important for a melting process of (Bi,Pb)-2223 tape. By combination of quenching experiment with X-ray diffraction (XRD) analysis, the effect of cooling...The reformation of (Bi,Pb)-2223 from the liquid or melt is very important for a melting process of (Bi,Pb)-2223 tape. By combination of quenching experiment with X-ray diffraction (XRD) analysis, the effect of cooling rate on the evolution of three superconducting phases in the (Bi,Pb)-2223 core of Ag-sheathed tape was investigated. The results show that (Bi,Pb)-2223 reformation from the melt seems to experience different routes during slowly cooling at different rates. One is that (Bi,Pb)-2223 phase reformed directly from the melt, and no Bi-2212 participate in this process. The other is that (Bi,Pb)-2223 is converted from the intermediate product, Bi-2212, which formed from the melt during the first cooling stage. Due to the inherent sluggish formation kinetics of (Bi,Pb)-2223 from Bi-2212, only partial (Bi,Pb)-2223 can finally be reformed with the second route.展开更多
After water cooling, there is a big temperature difference between the center and the surface of strip, which leads to the heat transfer from the center to the surface, and the surface temperature can rise in a short ...After water cooling, there is a big temperature difference between the center and the surface of strip, which leads to the heat transfer from the center to the surface, and the surface temperature can rise in a short time. The finite element method was used to simulate the phenomena of re-reddening on the surface of strip and to analyze the temperature field of hot roiled strip during laminar cooling, and the periodical variation curve of the cooling rate was obtained during water cooling and subsequent re-reddening. The results show that the critical line of the cooling rate is at 1/3 of the half-thickness from the strip surface. The regression model of the relation of rereddening temperature, time, and distance from the surface was obtained in the re-reddening region. Re-reddening regularity on the surface of strip under the condition of different thickness and cooling rate was also studied.展开更多
In this study, the effect of cooling rates on microstructures and mechanical properties in a Al-bearing hot-rolled transformation- induced plasticity steel was investigated. The experiments were carried out using hot ...In this study, the effect of cooling rates on microstructures and mechanical properties in a Al-bearing hot-rolled transformation- induced plasticity steel was investigated. The experiments were carried out using hot simulation machine and hot rolling mill, where the samples were cooled at different cooling rates. The results showed that with the increase in cooling rates, film-like retained austenite gradually disappeared and only blocky retained austenite was retained at higher cooling rates. The volume fraction of retained austenite was 9-11% at cooling rates of 0.05-1 ℃/s and 4-6% at cooling rates of 5-10 ℃/s. In addition, martensite/austenite island was observed because of the heterogeneous carbon distribution. The samples cooled at 0.05℃/s and 0.5 ℃/s exhibited excellent mechanical properties, with tensile strengths of 712 MPa and 726 MPa, total elongations of 42% and 36% and strength and ductility balances of 29.91 GPa% and 26.15 GPa%, respectively. During plastic deformation, the instantaneous work hardening exponent of the sample cooled at 0.05 ℃/s increased continuously until it reached the maximum value, while the instantaneous work hardening exponent of the sample cooled at 0.5℃/s remained stable.展开更多
Solidification process of 231 t 30Cr2Ni4MoV ingot manufactured by slow cooling process was studied using experimental and numerical simulations, which tackled the problems of high cost and long period in large ingot s...Solidification process of 231 t 30Cr2Ni4MoV ingot manufactured by slow cooling process was studied using experimental and numerical simulations, which tackled the problems of high cost and long period in large ingot studying. Based on the numerical results of large ingot, five characteristic locations under different temperature gradients and cooling rates chosen from the large ingot were simulated. The experiments were performed under the same temperature conditions as in numerical simulations with specialized instrument. The influences of temperature gradient in the solid-liquid interface and solidification rate on the size and morphology of solidification structure were analyzed at cooling rate ranging from 10-3 to 10 2℃ s-1. Solidification macrostructure and microstructure showed that no columnar dendrite was found in any specimen. The grain size and secondary dendrite arm spacing decreased at larger cooling rate, and the relationship between secondary dendrite arm spacing and local solidification time or cooling rate was determined.展开更多
The occurrence of γ phase, a high\|pressure polymorph of olivine (α phase), in the shock veins of Si\| xiangkou chondrite was due to a greater cooling rate (>10 000℃·s -1 ) in the veins. Because γ phas...The occurrence of γ phase, a high\|pressure polymorph of olivine (α phase), in the shock veins of Si\| xiangkou chondrite was due to a greater cooling rate (>10 000℃·s -1 ) in the veins. Because γ phase partially reverted to β phase and no back\|transformation from β phase to α phase took place, the shock veins of Peace River chondrite with a cooling rate of 1 000\2 000℃·s -1 contain a great amount of β phase. In the shock veins of Mbale chondrite with a cooling rate of <500℃·s -1 , the majority of γ phase reverted to α phase. The heat dissipation in shock veins took place after a stage of shock compression of chondrite parent body, and the parent body was broken into fragmental pieces. Cooling rate in the shock veins constrained the back\|transformations of (Mg,Fe)\-2SiO\-4 high\|pressure polymorphs.展开更多
采用Gleeble-3800热模拟试验机研究了热轧DP双相钢的TMCP(Thermo Mechanical Control Process)工艺,分析工艺参数、变形量、冷却速度和缓冷时间对含Nb热轧双相钢显微组织性能的影响。研究发现:增大变形量和延长缓冷时间,铁素体含量增加...采用Gleeble-3800热模拟试验机研究了热轧DP双相钢的TMCP(Thermo Mechanical Control Process)工艺,分析工艺参数、变形量、冷却速度和缓冷时间对含Nb热轧双相钢显微组织性能的影响。研究发现:增大变形量和延长缓冷时间,铁素体含量增加,可获得细小铁素体组织;轧后冷却速度越大,马氏体总含量越多,铁素体晶粒尺寸越细小。大的终轧变形量和轧后适当延长缓冷时间是获得工业生产理想双相钢的工艺保证。展开更多
基金Project(2011CB706605)supported by the National Basic Research Program of ChinaProject(2011CDA12)supported by the Innovative Research Groups of the Natural Science Foundation of Hubei Province,ChinaProjects(2012-Ia-017,2013-IV-014)supported by the Fundamental Research Funds for the Central Universities,China
文摘Pre-heat treatment is a vital step before cold ring rolling and it has significant effect on the microstructure and mechanical properties of rolled rings.The 100Cr6 steel rings were subjected to pre-heat treatment and subsequent cold rolling process.Scanning electron microscopy and tensile tests were applied to investigate microstructure characteristic and mechanical property variations of 100Cr6 steel rings undergoing different pre-heat treatings.The results indicate that the average diameter of carbide particles,the tensile strength and hardness increase,while the elongation decreases with the decrease of cooling rate.The cooling rate has minor effect on the yield strength of sample.After cold ring rolling,the ferrite matrix shows a clear direction along the rolling direction.The distribution of cementite is more homogeneous and the cementite particles are finer.Meanwhile,the hardness of the rolled ring is higher than that before rolling.
文摘The reformation of (Bi,Pb)-2223 from the liquid or melt is very important for a melting process of (Bi,Pb)-2223 tape. By combination of quenching experiment with X-ray diffraction (XRD) analysis, the effect of cooling rate on the evolution of three superconducting phases in the (Bi,Pb)-2223 core of Ag-sheathed tape was investigated. The results show that (Bi,Pb)-2223 reformation from the melt seems to experience different routes during slowly cooling at different rates. One is that (Bi,Pb)-2223 phase reformed directly from the melt, and no Bi-2212 participate in this process. The other is that (Bi,Pb)-2223 is converted from the intermediate product, Bi-2212, which formed from the melt during the first cooling stage. Due to the inherent sluggish formation kinetics of (Bi,Pb)-2223 from Bi-2212, only partial (Bi,Pb)-2223 can finally be reformed with the second route.
基金Item Sponsored by National Natural Science Foundation of China(50504007)State Basic Research Key Projects (973) of China(2006CB605208-1)
文摘After water cooling, there is a big temperature difference between the center and the surface of strip, which leads to the heat transfer from the center to the surface, and the surface temperature can rise in a short time. The finite element method was used to simulate the phenomena of re-reddening on the surface of strip and to analyze the temperature field of hot roiled strip during laminar cooling, and the periodical variation curve of the cooling rate was obtained during water cooling and subsequent re-reddening. The results show that the critical line of the cooling rate is at 1/3 of the half-thickness from the strip surface. The regression model of the relation of rereddening temperature, time, and distance from the surface was obtained in the re-reddening region. Re-reddening regularity on the surface of strip under the condition of different thickness and cooling rate was also studied.
基金support from the National Natural Science Foundation of China (No. 51504063)
文摘In this study, the effect of cooling rates on microstructures and mechanical properties in a Al-bearing hot-rolled transformation- induced plasticity steel was investigated. The experiments were carried out using hot simulation machine and hot rolling mill, where the samples were cooled at different cooling rates. The results showed that with the increase in cooling rates, film-like retained austenite gradually disappeared and only blocky retained austenite was retained at higher cooling rates. The volume fraction of retained austenite was 9-11% at cooling rates of 0.05-1 ℃/s and 4-6% at cooling rates of 5-10 ℃/s. In addition, martensite/austenite island was observed because of the heterogeneous carbon distribution. The samples cooled at 0.05℃/s and 0.5 ℃/s exhibited excellent mechanical properties, with tensile strengths of 712 MPa and 726 MPa, total elongations of 42% and 36% and strength and ductility balances of 29.91 GPa% and 26.15 GPa%, respectively. During plastic deformation, the instantaneous work hardening exponent of the sample cooled at 0.05 ℃/s increased continuously until it reached the maximum value, while the instantaneous work hardening exponent of the sample cooled at 0.5℃/s remained stable.
基金Acknowledgements This work was financially supported by the National Natural Science Foundation of China (51704210), the National Key Research and Development Program of China (No. 2017YFB0701802) and Natural Science Foundation of Hebei Province (E2017105016).
文摘Solidification process of 231 t 30Cr2Ni4MoV ingot manufactured by slow cooling process was studied using experimental and numerical simulations, which tackled the problems of high cost and long period in large ingot studying. Based on the numerical results of large ingot, five characteristic locations under different temperature gradients and cooling rates chosen from the large ingot were simulated. The experiments were performed under the same temperature conditions as in numerical simulations with specialized instrument. The influences of temperature gradient in the solid-liquid interface and solidification rate on the size and morphology of solidification structure were analyzed at cooling rate ranging from 10-3 to 10 2℃ s-1. Solidification macrostructure and microstructure showed that no columnar dendrite was found in any specimen. The grain size and secondary dendrite arm spacing decreased at larger cooling rate, and the relationship between secondary dendrite arm spacing and local solidification time or cooling rate was determined.
文摘The occurrence of γ phase, a high\|pressure polymorph of olivine (α phase), in the shock veins of Si\| xiangkou chondrite was due to a greater cooling rate (>10 000℃·s -1 ) in the veins. Because γ phase partially reverted to β phase and no back\|transformation from β phase to α phase took place, the shock veins of Peace River chondrite with a cooling rate of 1 000\2 000℃·s -1 contain a great amount of β phase. In the shock veins of Mbale chondrite with a cooling rate of <500℃·s -1 , the majority of γ phase reverted to α phase. The heat dissipation in shock veins took place after a stage of shock compression of chondrite parent body, and the parent body was broken into fragmental pieces. Cooling rate in the shock veins constrained the back\|transformations of (Mg,Fe)\-2SiO\-4 high\|pressure polymorphs.
文摘采用Gleeble-3800热模拟试验机研究了热轧DP双相钢的TMCP(Thermo Mechanical Control Process)工艺,分析工艺参数、变形量、冷却速度和缓冷时间对含Nb热轧双相钢显微组织性能的影响。研究发现:增大变形量和延长缓冷时间,铁素体含量增加,可获得细小铁素体组织;轧后冷却速度越大,马氏体总含量越多,铁素体晶粒尺寸越细小。大的终轧变形量和轧后适当延长缓冷时间是获得工业生产理想双相钢的工艺保证。