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Anti-penetration performance of high entropy alloy–ceramic gradient composites 被引量:6
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作者 Wen-rui Wang Hui-fa Xie +3 位作者 Lu Xie Han-lin Li Xiao Yang Yi-nan Shen 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2018年第11期1320-1328,共9页
A high-entropy alloy–ceramic gradient composite of TiC–TiB_2/75vol% Al_(0.3) CoCrFe Ni was successfully prepared by combustion synthesis under an ultra-high gravity field, which is a low-cost method with high effici... A high-entropy alloy–ceramic gradient composite of TiC–TiB_2/75vol% Al_(0.3) CoCrFe Ni was successfully prepared by combustion synthesis under an ultra-high gravity field, which is a low-cost method with high efficiency. The ceramic particles were gradient distributed in the Al_(0.3) CoCrFe Ni matrix, and the hardness of the composite material gradually decreased along the thickness direction. The anti-penetration performance of the gradient composites was simulated using the ANSYS/LS-DYNA explicit simulation program. The results demonstrate that the distribution of the ceramic particles strongly affected the mechanical properties and the anti-penetration performance of the composites. With the same total ceramic volume fraction, the gradient composites exhibit better anti-penetration performance than the corresponding ceramic–metal interlayer composites. The more uneven the ceramic distribution, the greater the elastic modulus and yield stress of the surface layer and, thus, the better the anti-penetration performance. 展开更多
关键词 COMBUSTION synthesis GRADIENT composite anti-PENETRATION performance NUMERICAL simulation
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Preparation technology and anti-corrosion performances of black ceramic coatings formed by micro-arc oxidation on aluminum alloys 被引量:9
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作者 CHEN Ling HAN Jing YU Shengxue 《Rare Metals》 SCIE EI CAS CSCD 2006年第z2期146-149,共4页
In order to prepare ornamental and anti-corrosive coating on aluminum alloys, preparation technology of black micro-arc ceramic coatings on Al alloys in silicate based electrolyte was studied. The influence of content... In order to prepare ornamental and anti-corrosive coating on aluminum alloys, preparation technology of black micro-arc ceramic coatings on Al alloys in silicate based electrolyte was studied. The influence of content of Na2WO4 and combination additive in solution on the performance of black ceramic coatings was studied; the anticorrosion performances of black ceramic coatings were evaluated through whole-immersion test and electrochemical method in 3.5% NaCl solution at different pH value; SEM and XRD were used to analyze the surface morphology and phase constitutes of the black ceramic coatings. Experimental results indicated that, without combination additives, with the increasing of Na2WO4 content in the electrolyte, ceramic coating became darker and thicker, but the color was not black; after adding combination additive, the coating turned to be black; the black ceramic coating was multi-hole form in surface. There was a small quantity of tungsten existing in the black ceramic coating beside α-Al2O3 phase and β-Al2O3 phase. And aluminum alloy with black ceramic coating exhibited excellent anti-corrosion property in acid, basic and neutral 3.5% NaCl solution. 展开更多
关键词 aluminum alloy micro-arc oxidation black coating anti-corrosion performance
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Anti-Noise Performance of the FT Continuous Zoom Analysis Method for Discrete Spectrum 被引量:2
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作者 LINHuibin DING Kang XU Chuanyan 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2010年第6期774-779,共6页
As a discrete spectrum correction method, the Fourier transform (FT) continuous zoom analysis method is widely used in vibration signal analysis, but little effort had been made on this method's anti-noise performa... As a discrete spectrum correction method, the Fourier transform (FT) continuous zoom analysis method is widely used in vibration signal analysis, but little effort had been made on this method's anti-noise performance. It is widely believed that the analysis accuracy of the method can be substantially improved by increasing the zoom multiple, however, with the zoom multiple increases, the frequency estimation accuracy may decline sometimes in practices. Aiming at the problems above, this paper analyzes the sources of frequency estimation error when a harmonic signal mixed with and without noise is processed using the FT continuous zoom analysis. According to the characteristics that the local maximum of the zoom spectrum may be wrongly selected when the signal is corrupted with noise, the number of wrongly selected spectrum lines is deduced under different signal-to-noise ratio and local zoom multiple, and then the maximum frequency estimation error is given accordingly. The validity of the presented analysis is confirmed by simulations results. The frequency estimation accuracy of this method will not improve any more under the influence of noise, and there is a best zoom multiple, when the zoom multiple is larger than the best zoom multiple; the maximum frequency estimation error will fluctuate back and forth. The best zoom multiple curves under different signal-to-noise ratios given provide a theoretical basis for the choice of the appropriate zoom multiples of the FT continuous zoom analysis method in engineering applications. 展开更多
关键词 SPECTRUM spectrum correction zoom analysis anti-noise performance
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Performance Analysis of RFID Framed Slotted Aloha Anti-Collision Protocol 被引量:3
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作者 Emad Felemban 《Journal of Computer and Communications》 2014年第1期13-18,共6页
In this paper, we develop a novel mathematical model to estimate the probability distribution function of the number of tags discovered after a certain number of interrogation rounds. In addition, the pdfs of the numb... In this paper, we develop a novel mathematical model to estimate the probability distribution function of the number of tags discovered after a certain number of interrogation rounds. In addition, the pdfs of the number of rounds needed to discover all the tags are also calculated. The estimation of such pdfs will be helpful in estimating the number of interrogation rounds and the optimal parameter configuration of the RFID system which in turn will be helpful in estimating the time needed to discover all tags. Our results show that the proposed model accurately predicts the tags detection probability. We then use the proposed model to optimally configure the reader parameters (i.e. the frame size and the number of interrogation rounds). 展开更多
关键词 performance Modeling RFID WIRELESS NETWORKS anti-COLLISION PROTOCOL
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Influence of graphene on the anti-corrosion performance of epoxy-based coatings 被引量:1
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作者 DONG Ying LU Qiting YAO Qisheng 《Baosteel Technical Research》 CAS 2016年第3期15-20,共6页
In this work, graphene-modified epoxy-based anti-corrosion coatings were prepared and the influence of graphene on the anti-corrosion performance of the epoxy-based coatings was investigated with water contact angle t... In this work, graphene-modified epoxy-based anti-corrosion coatings were prepared and the influence of graphene on the anti-corrosion performance of the epoxy-based coatings was investigated with water contact angle test ,chemical solution immersion test, and electrochemical test. The water contact angle and chemical solution resistance of the epoxy-based coatings were improved with an increase in graphene content from 0 to 0.4%. These results prove that addition of graphene can significantly improve the hydrophobicity and impermeability of epoxy- based coatings. However, when the graphene content was increased to 0.5%, the performance of the epoxy-based coatings decreased because of graphene aggregation. Tafel polarization results show that graphene addition can significantly reduce the corrosion current density and corrosion potential of epoxy-based coatings, which enhance their anti-corrosion performance. 展开更多
关键词 GRAPHENE epoxy-based coating anti-corrosion performance Tafel polarization curve
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Design of Small Stone Asphalt Mixture based on Anti-skidding Performance 被引量:1
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作者 李蕊 裴建中 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2012年第4期789-793,共5页
Small stone asphalt mixture(SSAM) was designed by Bailey method and coarse aggregate voids-filling method.The optimum asphalt content was determined by Marshal test.Surface texture depth for SSAM with different void... Small stone asphalt mixture(SSAM) was designed by Bailey method and coarse aggregate voids-filling method.The optimum asphalt content was determined by Marshal test.Surface texture depth for SSAM with different voidage,and the BPN of SSAM and SMA before after wet track abrasion were measured.The experimental results indicate that the surface texture depth increases with the decreasing of asphalt aggregate ratio.The SSAM with the optimal asphalt content has a good skid resistance.BPN of asphalt mixture decreases with the increasing of wearing time,but the extent of reduction is different.The reduction rate of BPN for SSAM is smaller than that of SMA,indicating that SSAM has a good skid resistance attenuation capacity.Finally,the other properties of SSAM are also evaluated,showing that the splitting strength and modulus and SSAM are higher than those of SMA,and the other properties of SSAM,such as high-temperature performance and water stability can also satisfy the technical requirements. 展开更多
关键词 small stone asphalt mixture mixture design anti-skidding performance attenuation of skid resistance
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PREDICTION OF RIME ICE ACCRETION AND RESULTING EFFECT ON AIRFOIL PERFORMANCE 被引量:3
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作者 陈维建 张大林 《Transactions of Nanjing University of Aeronautics and Astronautics》 EI 2005年第1期9-15,共7页
The roughness effect based on the wall function method is introduced into the numerical simulation of the rime ice accretion and the resulting effect on the aerodynamic performance of the airfoil. Incorporating the tw... The roughness effect based on the wall function method is introduced into the numerical simulation of the rime ice accretion and the resulting effect on the aerodynamic performance of the airfoil. Incorporating the two-phase model of air/super-cooled droplets in the Eulerian coordinate system, this paper presents the simulation of the rime ice accretion on the NACA 0012 airfoil. The predicted rime ice shape is compared with those results of measurements and simulations by other icing codes. Also the resulting effects of rime ice on airfoil aerodynamic performance are discussed. Results indicate that the rime ice accretion leads to the loss of the maximum lift coefficient by 26%, the decrease of the stall angle by about 3° and the considerable increase of the drag coefficient. 展开更多
关键词 numerical simulation anti/de-icing rime ice ROUGHNESS aerodynamic performance
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Preparation of High Performance Non-dispersible Concrete 被引量:1
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作者 姜丛盛 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2004年第2期67-69,共3页
A new-type underwater non-dispersible concrete admixture NDA was prepared,its function mechanism was analyzed,and C40 high performance non-dispersible underwater concrete was manufactured by applying NDA.The results i... A new-type underwater non-dispersible concrete admixture NDA was prepared,its function mechanism was analyzed,and C40 high performance non-dispersible underwater concrete was manufactured by applying NDA.The results indicate that NDA has a suitable workability,low strength loss,and excellent anti-dispersion;the fresh non-dispersible underwater concrete with NDA has high anti-dispersion,excellent workability such as self-compacting and not bleeding;hardened non-dispersible underwater concrete with NDA has a high strength,high durability such as high anti-abrasion,impermeability and anticorrosion. 展开更多
关键词 non-dispersible underwater concrete high performance anti-WASHOUT
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Lubricating Performance of Rapeseed Oil Under Electromagnetic Field
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作者 Jiang Zeqi Liu Ping +3 位作者 Fang Jianhua Chen Boshui Gu Kecheng Wu Jiang 《China Petroleum Processing & Petrochemical Technology》 SCIE CAS 2018年第1期85-92,共8页
Considering electromagnetic effect when investigating tribological properties of rapeseed oil is benefical not only to the improvement of green lubrication, but also to the development of tribology theories and practi... Considering electromagnetic effect when investigating tribological properties of rapeseed oil is benefical not only to the improvement of green lubrication, but also to the development of tribology theories and practices. In the present paper, the tribological properties of rapeseed oil under different intensity of electromagnetic field and normal loads were evaluated on a modified tribo-tester. The results indicated that the electromagnetic field could improve the anti-wear and friction-reducing property of the rapeseed oil. Furthermore, the influencing mechanisms were discussed from the perspective of electromagnetism according to the analytical results of SEM, EDS and XPS techniques. 展开更多
关键词 RAPESEED oil ELECTROMAGNETIC field anti-WEAR PROPERTY FRICTION-REDUCING performance
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Reproductive and Growth Performance of Rabbit Fed Different Inclusion Levels of African Yam Bean (<i>Sphenostylis stenocarpa</i>)
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作者 Chikaodiri H. Onuoha Bassey J. Harry +1 位作者 James O. Fayenuwo Emmanuel S. Durotoye 《Open Journal of Animal Sciences》 2020年第2期301-312,共12页
A feeding trial was conducted to determine the effect of dietary inclusion of Processed African Yam Bean (AYB) at 0%, 10%, 20% and 30% levels respectively, on the growth and reproductive performance of Rabbits. The AY... A feeding trial was conducted to determine the effect of dietary inclusion of Processed African Yam Bean (AYB) at 0%, 10%, 20% and 30% levels respectively, on the growth and reproductive performance of Rabbits. The AYB inclusion was to ascertain the best (%) level that would give better performance in rabbits. Complete randomized design was used to allot twenty (20) grower rabbits of both sexes into four treatments in three replicate with each group having three does and two bucks. Each of the treatment diets formulated at different growth stages was fed to the rabbits. The rabbits were kept in hutches inside the rabbit house and given feed and water ad libitum. Growth and reproductive parameters were measured. The proximate analysis and anti-nutritional factor of processed AYB showed that it contained values of 26.88%, 92.97%, 5.26%, 61.89%, 7.04%, 3.79% and 2.17% for Crude protein, Dry matter, Crude fibre, Nitrogen-free extract, Moisture content, Ash content and Ether extract respectively while the anti-nutritional factor contained 0.11%, 14.02 mg/g, 0.19 mg/g, 0.21 mg/g, 0.14 mg/g, 0.21 mg/g, 0.13 mg/g and 0.01 mg/g of Tannin, Alkaloid, Oxalate, Phytate, Saponin, Flavonoids, Trypsin inhibitor and Lectin. From this study, the rabbit group on 10% AYB inclusion significantly (p 0.05) affected by the diets. The results of this experiment concluded that AYB can be included in the diet of rabbits with 10% inclusion giving a better reproductive performance and growth rate without any negative effect. 展开更多
关键词 Rabbits Africa YAM BEAN REPRODUCTIVE performance Growth anti-Nutritional Factor
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杭州世纪中心西天窗索夹抗滑移试验研究 被引量:1
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作者 朱明亮 张步宽 +1 位作者 夏杰 郭正兴 《建筑结构》 北大核心 2024年第7期107-112,共6页
索夹是预应力索结构中拉索与其他构件连接的重要节点构件,若索夹和拉索之间发生滑移,会产生较大的预应力损失,甚至改变结构的受力性能。杭州世纪中心西天窗采用箱形桁架+钢索结构,其结构特殊性决定了拉索在施工张拉和施工完成后的状态不... 索夹是预应力索结构中拉索与其他构件连接的重要节点构件,若索夹和拉索之间发生滑移,会产生较大的预应力损失,甚至改变结构的受力性能。杭州世纪中心西天窗采用箱形桁架+钢索结构,其结构特殊性决定了拉索在施工张拉和施工完成后的状态不同,即施工张拉时要求拉索对索夹是可相对滑移的,而施工完成后需要锁定拉索和索夹的相对位置,不允许发生滑移。通过拉索施工张拉、高强螺栓紧固力衰减、索夹顶推三个阶段的全过程模拟试验确定了索夹与拉索之间的摩擦力情况。试验结果表明,在拉索施工张拉阶段,索夹对索体产生的摩擦力较小,通过锌板垫层能够有效降低铸钢索夹节点处的摩擦损失,保证拉索张拉过程中索力的有效传递;高强螺栓终拧后12h内会产生不可忽视的紧固力损失;使用阶段索夹的抗滑移承载能力能够确保索夹节点安全。 展开更多
关键词 索夹 索结构 抗滑移性能 抗滑移试验 紧固力
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基于性能的通航桥梁抗船撞评估方法及应用研究 被引量:2
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作者 王永祥 贾小龙 孙红兰 《世界桥梁》 北大核心 2024年第1期95-102,共8页
为合理有效地开展通航桥梁抗船撞性能评估,提出基于性能的桥梁抗船撞标准化评估方法。基于现行《公路桥梁抗撞设计规范》(JTG/T 3360-02-2020),从抗撞性能等级确定、设防代表船型确定、船撞力计算、船撞效应计算以及抗撞性能验算等方面... 为合理有效地开展通航桥梁抗船撞性能评估,提出基于性能的桥梁抗船撞标准化评估方法。基于现行《公路桥梁抗撞设计规范》(JTG/T 3360-02-2020),从抗撞性能等级确定、设防代表船型确定、船撞力计算、船撞效应计算以及抗撞性能验算等方面,采用结构性能目标作为评估准则,建立桥梁抗撞性能评估各环节流程的标准化评估方法。以江苏扬中三桥为应用实例,运用该方法进行该桥20号墩抗撞性能评估,结果表明:20号墩桩基顺桥向抗弯性能不满足JX1级要求,其余验算结果满足要求,桥墩抗撞性能综合评估结果为不满足要求。参照评估结果该桥加装了浮动式防撞设施。桥梁抗撞性能评估标准化,可准确高效实现桥梁抗撞性能等级确定、船撞效应计算、抗撞性能验算等预期的评估功能要求。 展开更多
关键词 桥梁工程 船撞桥 现行规范 结构性能目标 抗撞性能 标准化评估方法 工程应用
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潮湿基材涂装对海洋平台通用配套涂层体系防腐性能影响研究
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作者 于萱 张国庆 +3 位作者 王文卿 阳利军 钱思成 汪杰 《合成材料老化与应用》 CAS 2024年第3期14-16,共3页
海洋石油工程股份有限公司制造场地分别位于天津、青岛和珠海,其中青岛场地夏季经常出现相对湿度超过85%对涂装不利的极端天气。在此环境下,基材表面的潮湿现象,极大影响施工效率并影响交付工期。该文对比环氧富锌+环氧云铁+聚氨酯、环... 海洋石油工程股份有限公司制造场地分别位于天津、青岛和珠海,其中青岛场地夏季经常出现相对湿度超过85%对涂装不利的极端天气。在此环境下,基材表面的潮湿现象,极大影响施工效率并影响交付工期。该文对比环氧富锌+环氧云铁+聚氨酯、环氧铝粉漆体系、环氧玻璃鳞片体系等三个涂层体系在潮湿基材以及经过Sa2.5除锈的基材涂装后防腐性能的影响。通过对防腐体系的附着力、耐盐雾、冷凝试验等测试,得出结论,在涂膜外观无缺陷的情况下,潮湿基材表面涂装对三个涂层体系防腐性能有不利影响,但仍能满足配套涂层体系的防腐要求。 展开更多
关键词 潮湿基材 防腐涂层 防腐性能
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高速冲击加载下碳纤维复合材料层合结构抗侵彻特性及响应机理
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作者 蔡宣明 潘成龙 +3 位作者 郭安肖 张迅 高玉波 范志强 《振动与冲击》 EI CSCD 北大核心 2024年第12期88-96,165,共10页
碳纤维复合材料层合结构在高冲击服役环境中常遭受外来物体冲击作用,使之出现一些不可预测的各种损伤形式,甚至会出现不可控的损伤模式。为确保这些结构的安全性和可靠性,对碳纤维复合材料层合结构抗冲击响应及防护机理展开了研究。以... 碳纤维复合材料层合结构在高冲击服役环境中常遭受外来物体冲击作用,使之出现一些不可预测的各种损伤形式,甚至会出现不可控的损伤模式。为确保这些结构的安全性和可靠性,对碳纤维复合材料层合结构抗冲击响应及防护机理展开了研究。以碳纤维复合材料层合结构作为研究对象,基于一级轻气炮构建高速冲击加载试验装置,探明了碳纤维复合材料层合结构能量吸收特性与冲击能量之间的联系规律,结合弹道极限方程,确定了其弹道极限,并明确了不同冲击速度作用下的损伤模式。同时引入内聚力单元进行数值模拟仿真研究,探明了碳纤维复合材料层合结构层与层之间内聚力单元的损伤模式,揭示了其在高速冲击加载环境下的损伤机制。研究结果为反向设计适用于高速冲击加载环境复合材料层合结构提供理论依据。 展开更多
关键词 冲击 复合材料层合结构 能量吸收 抗侵彻性能
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改性彩色沥青路面色彩耐久性与抗滑性能研究
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作者 马峰 邹彦哲 +1 位作者 傅珍 王蒙蒙 《功能材料》 CAS CSCD 北大核心 2024年第2期2161-2167,共7页
为提高彩色沥青路面色彩耐久性并研究其抗滑性能,采用有机硅-聚丙酸酯(silane-modified polyacrylate,SMP)对彩色沥青玛蹄脂碎石混合料(color stone mastic asphalt,CSMA)和彩色开级配抗滑表层(color open graded friction course,COGF... 为提高彩色沥青路面色彩耐久性并研究其抗滑性能,采用有机硅-聚丙酸酯(silane-modified polyacrylate,SMP)对彩色沥青玛蹄脂碎石混合料(color stone mastic asphalt,CSMA)和彩色开级配抗滑表层(color open graded friction course,COGFC)2种混合料改性,借助小型加速加载设备进行对彩色沥青路面进行色彩耐久性评价,并通过三维扫描仪进行路面纹理信息采集,分析路面三维参数与其抗滑性能之间的关系。结果表明,SMP改性剂可有效提高CSMA、COGFC两种混合料的抗磨耗能力,提升彩色沥青色彩耐久性;CSMA及COGFC路面抗滑性能受到不同三维参数的影响,路面的摩擦系数模型由各自相关因子控制,增加路面暴露的集料数量和使用尖角集料能使彩色沥青路面的抗滑性能得到提升。 展开更多
关键词 道路与铁道工程 彩色沥青路面 色彩耐久性 抗滑性能 改性剂
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电气化铁路接触网地震作用与抗震性能分析
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作者 杨佳 陈奋飞 +3 位作者 贾传果 吕峻逸 邢挺 张家玮 《铁道工程学报》 EI CSCD 北大核心 2024年第8期91-96,共6页
研究目的:高地震烈度区域电气化铁路沿线途经多条地震断裂带,接触网系统在地震作用下易出现损坏,影响列车的正常运行。本文结合高地震烈度区电气化铁路,基于接触网系统服役特性,开展了4柱3跨原型足尺振动台试验,建立并验证地震响应下的... 研究目的:高地震烈度区域电气化铁路沿线途经多条地震断裂带,接触网系统在地震作用下易出现损坏,影响列车的正常运行。本文结合高地震烈度区电气化铁路,基于接触网系统服役特性,开展了4柱3跨原型足尺振动台试验,建立并验证地震响应下的接触网系统有限元模型,开展地震作用下接触网系统的地震响应仿真计算,对比分析接触网导线、腕臂、定位器、支柱等关键装备的抗震性能,并比较分析不同的接触网导线工作张力、跨距以及锚段长度对接触网系统抗震性能的影响,提出高地震烈度区接触网系统的抗震设计原则及措施,全面分析与研究地震作用下接触网系统响应规律和抗震性能。本文提出的关于接触网系统抗震性能分析数据及研究结论,能有效补充和完善接触网抗震设计规范及标准,有力支撑铁路工程建设,提升电气化铁路防灾抗灾能力。研究结论:(1)地震激励对接触网腕臂装置的影响较小,定位器出现受压,导致钩环结构易脱落;(2)地震激励对接触网支柱、接触线具有十分明显的影响,可造成支柱柱底应力增大和接触线跨中位移增大;(3)锚段长度对抗震性能无明显影响,适当增大接触线工作张力、减小跨距可有效降低接触网系统的地震响应;(4)本研究成果可为轨道交通领域防灾减灾设计提供指导。 展开更多
关键词 接触网 高地震烈度 地震响应 抗震设计 性能
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钢橡胶组合防撞装置试验与动力性能研究
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作者 马海英 邱媛 +3 位作者 夏烨 王君杰 辛子亨 宋彦臣 《东南大学学报(自然科学版)》 EI CAS CSCD 北大核心 2024年第3期616-626,共11页
为减少船桥撞击损伤,提出一种新型的钢-橡胶组合防撞装置.首先设计3组大比例试验构件,通过拟静力试验研究装置整体受力性能、破坏模式以及承载力;然后通过试验验证有限元模型,明确了焊缝对结构受力的影响,进行了装置整体动力性能分析.... 为减少船桥撞击损伤,提出一种新型的钢-橡胶组合防撞装置.首先设计3组大比例试验构件,通过拟静力试验研究装置整体受力性能、破坏模式以及承载力;然后通过试验验证有限元模型,明确了焊缝对结构受力的影响,进行了装置整体动力性能分析.结果表明:钢-橡胶组合防撞装置由于填充轮胎的支撑作用,承载能力明显高于空筒防撞装置;钢-橡胶组合防撞装置具有很好的缓冲消能效果,在正撞和20°斜撞工况下耗能均达到35%以上,满足阻碍船舶与桥墩撞击的功能;回收轮胎不仅实现了一定的拨转功能,还起到耗能作用,轮胎填充能提升耗能5%以上,对船有回弹作用;同时,轮胎的填充不仅能提升自浮性能,更提升了装置整体性能. 展开更多
关键词 桥梁工程 防撞装置 数值模拟 防撞性能
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高效液相色谱法测定化妆品中19种非甾体抗炎药
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作者 张江维 张弦 +2 位作者 谭杰 梁柱业 关漪莲 《化学分析计量》 CAS 2024年第5期12-18,共7页
建立高效液相色谱法测定化妆品中19种非甾体抗炎药含量。化妆品样品经体积比为1∶1的乙腈-乙酸铵溶液超声提取,用C_(18)色谱柱(250 mm×4.6 mm,5μm)分离,以不同体积比的乙腈-乙酸铵溶液为流动相梯度洗脱,采用二极管阵列检测器检测... 建立高效液相色谱法测定化妆品中19种非甾体抗炎药含量。化妆品样品经体积比为1∶1的乙腈-乙酸铵溶液超声提取,用C_(18)色谱柱(250 mm×4.6 mm,5μm)分离,以不同体积比的乙腈-乙酸铵溶液为流动相梯度洗脱,采用二极管阵列检测器检测。布洛芬的检测波长为230 nm,醋氯芬酸、双氯芬酸钠检测波长为278 nm,其余16种非甾体的检测波长均为245 nm。19种非甾体的质量浓度在5~200μg/mL范围内与其对应的色谱峰面积线性关系良好,相关系数均大于0.999 5,检出限为0.2~8 mg/kg。空白样品的水剂和凝胶基质的加标平均回收率分别为93.1%~110.9%和91.3%~108.1%,测定结果的相对标准偏差分别为0.2%~3.5%和0.6%~4.2%(n=6)。该方法适用于化妆品中19种非甾体抗炎药的测定。 展开更多
关键词 高效液相色谱法 非甾体抗炎药 化妆品
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复合露酒的非挥发性成分鉴定及抗疲劳效应
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作者 陈颖 朱禹哲 +4 位作者 余美丽 刘方美 李存玉 郑云枫 彭国平 《中国酿造》 CAS 北大核心 2024年第8期86-92,共7页
该研究采用高效液相色谱-四级杆飞行时间串联质谱联用(HPLC-Q-TOF-MS/MS)法对复合露酒(38%vol)中的非挥发性化合物进行检测,并将复合露酒灌胃至小鼠22 d,考察其对小鼠负重游泳的影响,评价其抗疲劳的保健作用。结果表明,从复合露酒(0.225... 该研究采用高效液相色谱-四级杆飞行时间串联质谱联用(HPLC-Q-TOF-MS/MS)法对复合露酒(38%vol)中的非挥发性化合物进行检测,并将复合露酒灌胃至小鼠22 d,考察其对小鼠负重游泳的影响,评价其抗疲劳的保健作用。结果表明,从复合露酒(0.2257 g生药/mL)中共鉴定出52种非挥发性物质,包括皂苷类24种、黄酮类6种、核苷类4种、氨基酸类4种、生物碱类3种、其他11种。与模型组相比,低、中、高剂量组小鼠体质量减少量均极显著减少(P<0.01);中、高剂量组小鼠负重游泳时间均极显著延长(P<0.01);低、中剂量组小鼠血尿素氮(BUN)含量显著增加(P<0.01,P<0.05);低、中、高剂量组小鼠乳酸脱氢酶(LDH)活力、肝糖原(LG)含量显著增加(P<0.01,P<0.05),说明该款复合露酒非挥发性成分丰富,可增强身体对负荷的适应性,具有明显的抗疲劳效果,对功能性食品开发提供一定的基础。 展开更多
关键词 复合露酒 高效液相色谱-四级杆飞行时间串联质谱 非挥发性成分 抗疲劳
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基于等价输入干扰滑模观测器的磁悬浮轴承控制
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作者 黄刚 袁崧琳 +2 位作者 于惠钧 时鑫一 刘博龙 《轴承》 北大核心 2024年第7期80-86,94,共8页
针对磁悬浮轴承受到未知干扰而使转子偏离理想位置导致控制性能下降的问题,建立了存在未知干扰的磁悬浮轴承模型,基于模型设计了等价输入干扰系统,利用积分滑模观测器对系统状态量进行观测并结合等价输入干扰估计器协同实现对未知干扰... 针对磁悬浮轴承受到未知干扰而使转子偏离理想位置导致控制性能下降的问题,建立了存在未知干扰的磁悬浮轴承模型,基于模型设计了等价输入干扰系统,利用积分滑模观测器对系统状态量进行观测并结合等价输入干扰估计器协同实现对未知干扰的实时精准估计,通过控制端对等价输入干扰估计值进行前馈补偿,设计转子位置环的滑模控制器,通过复合控制提高系统的鲁棒性。与其他方法的仿真对比结果表明,所提方法能够提高轴承系统的抗扰性能,实现对转子位置的高精度控制。 展开更多
关键词 滑动轴承 磁力轴承 滑模控制 鲁棒性 抗干扰性
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