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Pulsed Eddy Current Non-destructive Testing and Evaluation:A Review 被引量:31
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作者 Ali Sophian Guiyun Tian Mengbao Fan 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2017年第3期500-514,共15页
Pulsed eddy current (PEC) non-destructive test- ing and evaluation (NDT&E) has been around for some time and it is still attracting extensive attention from researchers around the globe, which can be witnessed th... Pulsed eddy current (PEC) non-destructive test- ing and evaluation (NDT&E) has been around for some time and it is still attracting extensive attention from researchers around the globe, which can be witnessed through the reports reviewed in this paper. Thanks to its richness of spectral components, various applications of this technique have been proposed and reported in the lit- erature covering both structural integrity inspection and material characterization in various industrial sectors. To support its development and for better understanding of the phenomena around the transient induced eddy currents, attempts for its modelling both analytically and numeri- cally have been made by researchers around the world. This review is an attempt to capture the state-of-the-art development and applications of PEC, especially in the last 15 years and it is not intended to be exhaustive. Future challenges and opportunities for PEC NDT&E are also presented. 展开更多
关键词 Non-destructive testing - Pulsed eddy currentsMaterial characterization Structural integrity Non-destructive evaluation
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ON RELATION BETWEEN SIZE DEVIATION OF RAW SILK AND TESTING-LENGTH
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作者 白伦 《苏州大学学报(工科版)》 CAS 1996年第S3期23-33,共11页
Based on the auto- corrclation coefficient model.we gave an expression ofsize deviation of raw silk when testing- length is equal to a fraction for the unitlength,and discussed how the ratio of the size deviatinons by... Based on the auto- corrclation coefficient model.we gave an expression ofsize deviation of raw silk when testing- length is equal to a fraction for the unitlength,and discussed how the ratio of the size deviatinons by different testing-length fluctuates with the pseudo- cycle.Using these results as a basis,weexamined how the size deviation with the continuous property of raw silk sizechanges when changing the testing- length from 450 m to ll2.5m.Then weexamined the problem of quality control of raw silk. 展开更多
关键词 testing-length. SIZE deviation. auto-correlation coefficient.Continuos property of RAW SILK SIZE
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Testing of Anti-stripping Property of Friction Spun Core Yarn
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作者 丁辛 宋允 《Journal of China Textile University(English Edition)》 EI CAS 1998年第3期66-69,共4页
Friction spun core yarn has two components: filament core and staple fiber sheath. Under axial rubbing action, the failure mode of the core yarn is the stripping of the sheath from the core. This paper introduces a me... Friction spun core yarn has two components: filament core and staple fiber sheath. Under axial rubbing action, the failure mode of the core yarn is the stripping of the sheath from the core. This paper introduces a method to test the anti - stripping property of the core yarn. With a modified Universal Testing Machine, the stripping resistance of friction spun core yarn can be continuously measured. Some factors Influencing the measurements are discussed in detail. The testing results are compared with those from a Y731 Yarn Abrasion Tester and fur - ther confirmed by weaving practice. 展开更多
关键词 FRICTION SPUN CORE YARN anti - STRIPPING PROPERTY STRIPPING resistance testing.
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CPAP和Auto-CPAP治疗重度OSAHS患者的临床疗效比较 被引量:16
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作者 岳英明 孟琨 邱小建 《首都医科大学学报》 CAS 北大核心 2018年第1期120-127,共8页
目的探讨持续气道正压通气呼吸机(continuous positive airway pressure,CPAP)与自动调节持续气道正压通气呼吸机(Auto-CPAP)治疗重度阻塞性睡眠呼吸暂停低通气综合征(obstructive sleep apnea-hypopnea syndrome,OSAHS)患者的治疗效果... 目的探讨持续气道正压通气呼吸机(continuous positive airway pressure,CPAP)与自动调节持续气道正压通气呼吸机(Auto-CPAP)治疗重度阻塞性睡眠呼吸暂停低通气综合征(obstructive sleep apnea-hypopnea syndrome,OSAHS)患者的治疗效果和依从性,及治疗前后肺功能变化情况。方法通过多导睡眠图(polysomnography,PSG)选取重度OSAHS患者60例,PSG正常对照组56例,均行肺功能检查(pulmonary function test,PFT)。将重度OSAHS患者采用随机数字表分为CPAP组和Auto-CPAP组各30例,分别接受CPAP和Auto-CPAP治疗,观察治疗前和治疗后第1个月、第3个月、第6个月的PSG参数、呼吸机治疗所需压力、平均每晚呼吸机使用时间、Epworth嗜睡量表评分(Epworth Sleepiness Scale,ESS)及肺功能指标变化。结果 (1)重度OSAHS患者组与正常对照组用力肺活量(forced vital capacity,FVC)、1秒用力呼出容积(forced expiratory volume in one second,FEV1)、1秒用力呼出容积实测值与预计值比值(FEV1%)、FEV1/FVC、肺总量(total lung capacity,TLC)实测值与预计值比值(实测值与预计值比值)、一氧化碳弥散量(carbon monoxide diffusing capacity,DLCO)实测值与预计值比值、气道总阻力(airway resistance 5,R5)实测值与预计值比值差异无统计学意义(P>0.05),闭合总量(closing capacity,CC)/功能残气量(functional residual capacity,FRC)%(P=0.038)、50%最大呼气流速(peak expiratory flow,PEF50)实测值与预计值比值(P=0.041)、最大呼气中段流速(maximum midexpiratory flow,MMEF)实测值与预计值比值(P=0.037)差异有统计学意义;(2)治疗后第1个月、第3个月、第6个月,CPAP组和Auto-CPAP组呼吸暂停低通气指数(apnea-hypopnea index,AHI)、夜间平均血氧饱和度(nighttime mean pulse oxygen saturation,M Sa O2)、夜间最低血氧饱和度(nighttime the lowest pulse oxygen saturation,L Sa O2)、睡眠潜伏期(sleep latency,SL)、睡眠效率(sleep efficiency,SE)、FVC、FEV1、FEV1%、FEV1/FVC、TLC实测值与预计值比值、DLCO实测值与预计值比值、R5实测值与预计值比值、CC/FRC%、PEF50实测值与预计值比值、MMEF实测值与预计值比值、ESS指标比较,差异均无统计学意义(P>0.05),Auto-CPAP组觉醒次数(wake after sleep onset,WASO),Ⅰ期+Ⅱ期、Ⅲ期+Ⅳ期及快速动眼(rapid eye movement,REM)期睡眠各占总睡眠时间(total sleep time,TST)的比例、呼吸机治疗所需压力、平均每晚呼吸机使用时间与CPAP组比较,差异有统计学意义(P<0.05);两组第1个月、第3个月、第6个月的AHI、WASO、Ⅰ期+Ⅱ期比例、ESS指标均较治疗前降低,差异有统计学意义(P<0.05),M Sa O2、L Sa O2、Ⅲ期+Ⅳ期比例、REM比例指标均较治疗前升高,差异有统计学意义(P<0.05),SL和SE指标较治疗前升高,差异无统计学意义(P>0.05);两组第1个月、第3个月、第6个月的肺功能指标FVC、FEV1、FEV1%、FEV1/FVC、TLC实测值与预计值比值、DLCO实测值与预计值比值、R5实测值与预计值比值、CC/FRC%、PEF50实测值与预计值比值、MMEF实测值与预计值比值较治疗前,差异无统计学意义(P>0.05)。所有接受无创呼吸机治疗病例均无明显不良反应。结论重度OSAHS患者早期肺功能受损病变主要发生在小气道且该病变呈不可逆趋势。CPAP和Auto-CPAP对于重度OSAHS患者临床治疗效果相当,但Auto-CPAP对患者睡眠结构改善更佳且依从性更好。 展开更多
关键词 阻塞性睡眠呼吸暂停低通气综合征 持续气道正压通气 自动调节持续气道正压通气 多导睡眠图 肺功能
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LDRA TestBed在CTCS2-200C扩展单元软件测试中的应用 被引量:1
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作者 周永健 范明 +1 位作者 张淼 赵东旭 《机车电传动》 北大核心 2016年第5期102-106,共5页
介绍了LDRA Test Bed软件测试工具和CTCS2-200C扩展单元,以CTCS2-200C为例,通过对软件进行静态和动态测试,参照EN 50128:2011标准,提高了整个软件开发生命周期中的各项验证和确认活动效率,降低了软件的风险。
关键词 软件测试 test BED EN 50128 CTCS2-200C扩展单元 列控车载系统
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The 0-1 test algorithm for chaos and its applications 被引量:5
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作者 孙克辉 刘璇 朱从旭 《Chinese Physics B》 SCIE EI CAS CSCD 2010年第11期200-206,共7页
To determine whether a given deterministic nonlinear dynamic system is chaotic or periodic, a novel test approach named zero-one (0-1) test has been proposed recently. In this approach, the regular and chaotic motio... To determine whether a given deterministic nonlinear dynamic system is chaotic or periodic, a novel test approach named zero-one (0-1) test has been proposed recently. In this approach, the regular and chaotic motions can be decided by calculating the parameter K approaching asymptotically to zero or one. In this study, we focus on the 0-1 test algorithm and illustrate the selection of parameters of this algorithm by numerical experiments. To validate the reliability and the universality of this algorithm, it is applied to typical nonlinear dynamic systems, including fractional-order dynamic system. 展开更多
关键词 CHAOS 0-1 test fractional-order system Lyapunov exponent
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The Study of the Auto Disk Brake Air Test 被引量:1
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作者 LI Lei Lü Hai-yuan +7 位作者 WANG Xiao-dong LI Sheng-liang YANG Shi-jun SUN Ai-qin ZHANG Peng YANG Zhi-cheng CHEN Long HU Ai-ying 《International Journal of Plant Engineering and Management》 2012年第3期169-172,共4页
In the paper weakness of air leakage system in our company is discussed firstly. Secondly the improved scheme of air leakage system including auto-control is designed. Then, the tooling with role of location and recov... In the paper weakness of air leakage system in our company is discussed firstly. Secondly the improved scheme of air leakage system including auto-control is designed. Then, the tooling with role of location and recovery is developed. At last the application of design optimization is processed. The result reveals that the system of air leakage detection is very valuable and important to manufacture. 展开更多
关键词 auto disk brake air leakage test PISTON
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基于Test Method 1311法重结晶α-半水石膏重金属元素的浸出特性研究 被引量:1
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作者 余智 吴晓琴 +1 位作者 许勇 叶智 《安全与环境工程》 CAS 2017年第5期94-99,共6页
以脱硫石膏及其常压盐溶液法重结晶得到的α-半水石膏为研究对象,采用改进的Tessier流程和Test Method 1311法研究两种石膏晶体重金属元素的赋存形态和浸出特性,并对其进行环境效应评价。结果表明:重结晶过程能够释放脱硫石膏中的重金... 以脱硫石膏及其常压盐溶液法重结晶得到的α-半水石膏为研究对象,采用改进的Tessier流程和Test Method 1311法研究两种石膏晶体重金属元素的赋存形态和浸出特性,并对其进行环境效应评价。结果表明:重结晶过程能够释放脱硫石膏中的重金属元素并使其赋存形态改变;重结晶后石膏晶体中的重金属组分短期内可达到释放平衡,其中Cr、Pb、Ni元素的最大浸出量明显低于对应的脱硫石膏,As元素的浸出量几乎不变;α-半水石膏的环境友好性优于脱硫石膏,但仍具有污染环境的潜在风险。 展开更多
关键词 脱硫石膏 Α-半水石膏 重结晶 test Method 1311法 重金属元素 赋存形态 浸出特性
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Test of Normality of Waist Measurement Data of Young Male and Female Adults based on the Quantile - Quantile Plot
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作者 F. Z. Okwonu J. N. Igabari 《Journal of Statistical Science and Application》 2017年第3期118-126,共9页
This paper investigates the normality of some real data set obtained from waist measurements of a group of 49 young adults. The quantile - quantile (Q-Q) plot and the analysis of correlation coefficients for the Q-Q... This paper investigates the normality of some real data set obtained from waist measurements of a group of 49 young adults. The quantile - quantile (Q-Q) plot and the analysis of correlation coefficients for the Q-Q plot is used to determine the normality or otherwise of the data set. In this regards, the probabilities of the quantiles were computed, modified and plotted. Thereafter the correlation coefficients for the quantile - quantile plots were obtained. Results indicate that at 0.1 level of significance, the data for young adult males of the sample were not normally distributed, and had a mean value that is within the range of low risk, healthwise, whereas the distribution of the data for young female adults showed reasonable normality, but also with a mean value that is within the range of low risk in terms of health condition. 展开更多
关键词 Correlation coefficient probability plot quantile - quantile plot test of normality waist measurement young adults.
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Expression of Auto-antiboby in Patients wih Acute Pancreatitis and its Clinical Significance
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作者 张进祥 郑启昌 崔天盆 《Journal of Huazhong University of Science and Technology(Medical Sciences)》 SCIE CAS 2003年第1期32-34,共3页
The expression of an auto-antibody in patients with edematous acute pancreatitis and its possible clinical significance was investiaged. Eighteen cases of acute pancreatitis were chosen as experimental group and 25 su... The expression of an auto-antibody in patients with edematous acute pancreatitis and its possible clinical significance was investiaged. Eighteen cases of acute pancreatitis were chosen as experimental group and 25 subjects served as control group. Venous blood samples were taken in both groups at 4 time points: at the day of admission, the 2nd, 4th and 7th day of hospitalization. By using indirect immuno-fluorescence tests the expression of auto-antibody in the samples was semiquantitatively detected. Other biochemical indexes, such as serum amylase, urine amylase, were determined simultaneously. As well, the clinical signs or symptoms were mornitored. It was found that the expression of the auto-antibody was gradually enhanced with the development of acute pancreatitis. The inceased positive expression of auto-antibody showed a correlationship with the improvement of biochemical indexes (r=0.951) and clinical manifestations (r=0.996). There was significant difference between experimental and control groups (P<0.05). During the recovery period of acute pancreatitis, gradually increased auto-antibody expression was detectable. This antibody is against the interstitial structure of the pancreas. 展开更多
关键词 auto-ANTIBODY acute pancreatitis indirect immuno-fluorescence test
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Method of militarysoftware securityand vulnerability testing based on process mutation
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作者 金丽亚 王荣辉 肖庆 《Journal of Measurement Science and Instrumentation》 CAS 2013年第3期228-230,共3页
To solve the problems caused by military software security issues,this paper firstly introduces a new software fault injection technique,namely main static fault injection method:program mutation.And then source code ... To solve the problems caused by military software security issues,this paper firstly introduces a new software fault injection technique,namely main static fault injection method:program mutation.And then source code for testing this algorithm is put forward.On this basis buffer overflow testing based on program mutation is conducted.Finally several military software source codes for buffer overflow testing are tested using deficiency tracking system(DTS)tool,Experimental results show the effectiveness of the proposed algorithm. 展开更多
关键词 military software testing fault injection buffer overflow source code scanningCLC number:TP311.562 Document code:AArticle ID:1674-8042(2013)03-0228-03
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The Test Area of Suizhong 36-1 Oil Field Fully Under Commission
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作者 Yan Hao 《China Oil & Gas》 CAS 1995年第3期14-14,共1页
TheTestAreaofSuizhong36-1OilFieldFullyUnderCommission¥//Suizhong36-lOilfieldlocatedin.LiaodongGulf,coveringa... TheTestAreaofSuizhong36-1OilFieldFullyUnderCommission¥//Suizhong36-lOilfieldlocatedin.LiaodongGulf,coveringanareaof48km2Theoi... 展开更多
关键词 test The test Area of Suizhong 36-1 Oil Field Fully Under Commission
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Relationship between Growth Hormone and Cytokines in Short Children Undergoing Growth Hormone Stimulation Testing
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作者 Kimberly Tafuri Denise Dixon +2 位作者 Katherine Markarian Andrew Lane Thomas A. Wilson 《International Journal of Clinical Medicine》 2015年第12期912-918,共7页
Background: The relationship between growth hormone (GH) and cytokines remains unclear. Several studies have suggested that GH increases tumor necrosis factor (TNF)-α production in both children and adults. However, ... Background: The relationship between growth hormone (GH) and cytokines remains unclear. Several studies have suggested that GH increases tumor necrosis factor (TNF)-α production in both children and adults. However, a number of studies have demonstrated a negative correlation between GH and TNF α. The aim of this study is to explore the relationship between endogenous GH secretion and certain pro and anti-inflammatory cytokines in short children undergoing GH stimulation testing for evaluation for GH deficiency. Methods: Plasma growth hormone, TNF α, CRP, IL-6, IL1-β, IL-4 and IL-10 levels are obtained at baseline and every 30 minutes for 150 minutes following two provocative agents (clonidine, and either arginine or glucagon). Results: Among the 23 children, 7 are found to be GH deficient. No significant differences in baseline TNF α levels are found between GH deficient and GH sufficient children. No correlation is identified between TNF α levels and GH levels during stimulation testing. Furthermore, no relationship is found between GH and pro-inflammatory cytokines or GH and anti-inflammatory cytokines. Conclusion: Our results do not demonstrate an acute relationship between endogenous GH secretion and the cytokines examined. 展开更多
关键词 GROWTH HORMONE Tumor Necrosis Factor-α CYTOKINES CRP IL-6 IL1-β IL-4 IL-10 GROWTH HORMONE STIMULATION testing CLONIDINE Arginine Glucagon
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The Changes of Baroreflex Sensitivity During Head-up Tilt Test and Its Clinical Significance in the Patients with Vasovagal Syncope
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作者 胡兆霆 吕艳青 杨钧国 《South China Journal of Cardiology》 CAS 2001年第2期65-68,共4页
Objective To study thechanges of baroreflex sensitivity (BRS) during head - up tilt test (HUT) in patients with vasovagal syncope (VS), and to examine the relationship between baroreflex sensitivity and neurohormonal ... Objective To study thechanges of baroreflex sensitivity (BRS) during head - up tilt test (HUT) in patients with vasovagal syncope (VS), and to examine the relationship between baroreflex sensitivity and neurohormonal factors. Furthermore, to investigate the effects of the changes of BRS on VS. Methods Forty - two patients with unexplained syncope (Among the 42 patients, there were 22 patients with positive HUT and 20 patients with negative HUT respectively) and 20 healthy volunteers (with negative HUT) underwent passive head - up tilt testing, Ante-cubital vein blood samples were taken before and after HUT, or at syncope. The fasting plasma endothelin , serum nitric oxide (NO), serum NE were measured, the BRS was assessed on the basis of the linear regression slope the RR interval versus systolic arterial blood pressure during the increment in blood pressure after intravenous administration of phenylephrine. Results (1) During the syncope, the BRS significantly reduced in HUT(+) group than baseline. At the end of tilt, the level of plasma ET, serum NO in patients with positive HUT significantly increased compared with baseline or normal controls, and the plasma concentration of NE also had the trend of increase. (2) By multiple regression analysis, a significant negative correlation was found between baroreceptor sensitivity and the plasma ET, NO at the end of HUT in patients with positive HUT, but there was no relationship between BRS and NE. Conclusions During the syncope occure, the BRS in patients with VS decreased significantly compared with normal controls. The abnormal plasma ET, NO concen-tration might contribute to the mechanism of VS. 展开更多
关键词 Vasovagal syncope Head - up tilt test Endothelin Nitric oxide Baroreflex Sensitivity
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GMAW(STT)和AUTO-FCAW组合焊接与GTAW+FCAW组合焊接对比试验
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作者 邵国庆 孟秀文 +2 位作者 李军 宫丽彦 刘海仁 《船电技术》 2022年第4期53-55,60,共4页
为分析管子对接焊半自动焊接工艺(手工GMAW(STT)和自动FCAW组合)的优劣,本文介绍了该半自动工艺与传统GTAW和FCAW手工组合焊接工艺的对比试验。对比分析两种焊接工艺的焊接质量、效率、人员工作强度等。为后续推广管子对接焊缝GMAW(STT... 为分析管子对接焊半自动焊接工艺(手工GMAW(STT)和自动FCAW组合)的优劣,本文介绍了该半自动工艺与传统GTAW和FCAW手工组合焊接工艺的对比试验。对比分析两种焊接工艺的焊接质量、效率、人员工作强度等。为后续推广管子对接焊缝GMAW(STT)和自动FCAW组合焊接奠定基础,对推进高效焊、自动焊的应用有一定的指导作用。 展开更多
关键词 GMAW(STT) FCAW GTAW 管子 对接焊 试验
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Investigation on the Structure of Chute-feed and Card Auto-leveller and Their Selection of Technological Processes
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作者 程隆棣 《Journal of China Textile University(English Edition)》 EI CAS 1998年第3期62-65,共4页
Based on the structure of chute - feed and autoleveHer, an analysis of their working principle and the verification of their practical production results have been carried out. Finally, the future investigation direet... Based on the structure of chute - feed and autoleveHer, an analysis of their working principle and the verification of their practical production results have been carried out. Finally, the future investigation direetiom of chute - feed and card autuleveller are put forward. 展开更多
关键词 CHUTE - FEED CARD auto - leveller IRREGULARITY among shifts.
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基于IWOA-ELM-AE的电力资产信息管理系统异常数据检测方法
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作者 李凯 靳书栋 +2 位作者 刘宏志 王艳梅 杨晓营 《沈阳工业大学学报》 CAS 北大核心 2024年第3期255-262,共8页
针对当前电力资产信息管理系统难以准确自主发现异常数据的问题,提出了一种基于IWOA-ELM-AE的电力资产信息管理系统异常数据检测方法。在管理系统框架下分析了可能存在的异常类型,将改进鲸鱼优化算法(IWOA)用于优化极限学习机自编码器(E... 针对当前电力资产信息管理系统难以准确自主发现异常数据的问题,提出了一种基于IWOA-ELM-AE的电力资产信息管理系统异常数据检测方法。在管理系统框架下分析了可能存在的异常类型,将改进鲸鱼优化算法(IWOA)用于优化极限学习机自编码器(ELM-AE),建立了电力信息系统异常数据优化检测模型。将模型应用于电力资产信息异常数据检测,并建立性能评估指标体系以衡量其效果。结果表明:所提方法的检测性能评估结果与传统模型相比具有显著优势,能够更为准确地检测电力资产信息中存在的异常数据。 展开更多
关键词 信息管理系统 电力资产 异常数据检测 极限学习机 自编码器 鲸鱼优化算法 检测性能 评估指标
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自动固相微萃取(SPM E)GC-MS、GC-MS-MS法检测环境水中有机磷杀虫剂的研究 被引量:6
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作者 魏立青 郭杰 +1 位作者 蒋华宇 种法运 《分析测试学报》 CAS CSCD 北大核心 2004年第z1期226-230,共5页
  固相微萃取(solid-phase microextraction,SPME)是20世纪90年代发展起来的一种样品前处理技术,与传统的液-液提取、液-固提取相比,SPME更适用于提取、浓缩液态或气态的挥发性和半挥发性物质,SPME技术可将采样、萃取、浓缩和样本引...   固相微萃取(solid-phase microextraction,SPME)是20世纪90年代发展起来的一种样品前处理技术,与传统的液-液提取、液-固提取相比,SPME更适用于提取、浓缩液态或气态的挥发性和半挥发性物质,SPME技术可将采样、萃取、浓缩和样本引入集中于一个步骤完成,尤其随着自动SPME与GC-MS等联用技术的日益完善,使SPME技术优点得到更充分的发挥.…… 展开更多
关键词 Organophosphate insecticides auto Solid-phase microextraction(auto-SPME) Gas chromatographymass spectrometry(GC - MS) Gas chromatography - multiple mass spectrometry(GC - MS - MS)
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基于IVI-Signal标准的自动测试系统驱动研究 被引量:3
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作者 张光轶 许爱强 牛双诚 《计算机测量与控制》 CSCD 2007年第2期151-153,共3页
建立通用测试软件平台,实现测试程序集和仪器资源的无关性设计是通用ATS的发展方向;驱动程序作为连接测试程序集和仪器资源的桥梁,在“无关性设计”中起着决定性作用;在分析自动测试系统基本理论和基于IVI-Signal标准的ATS软件平台体系... 建立通用测试软件平台,实现测试程序集和仪器资源的无关性设计是通用ATS的发展方向;驱动程序作为连接测试程序集和仪器资源的桥梁,在“无关性设计”中起着决定性作用;在分析自动测试系统基本理论和基于IVI-Signal标准的ATS软件平台体系基础上,运用组件技术划分信号角色、定义信号接口,根据仪器资源信号能力提出资源配置文件设计方法并给出XML语言实例,提供了基于测试资源信号能力的驱动设计方案,验证了IVI-Signal标准的可行性,为进一步工程实现提供了依据。 展开更多
关键词 自动测试系统 接口 信号角色 信号驱动
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ETC-ATD-GC/MS法测试墙纸中挥发性有机物 被引量:3
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作者 朱海欧 陈进 +3 位作者 卢志刚 李翔 张彰 张桂珍 《中国造纸》 CAS 北大核心 2014年第2期25-29,共5页
采用环境测试舱(ETC)、自动热脱附仪(ATD)和气相色谱/质谱(GC/MS)联用技术,研究并建立了墙纸中15种挥发性有机物(VOCs)的分析方法.对ATD实验条件、吸附剂选择等研究发现,与常规吸附剂Tenax TA相比,吸附剂Carbopack B/Carbosieve... 采用环境测试舱(ETC)、自动热脱附仪(ATD)和气相色谱/质谱(GC/MS)联用技术,研究并建立了墙纸中15种挥发性有机物(VOCs)的分析方法.对ATD实验条件、吸附剂选择等研究发现,与常规吸附剂Tenax TA相比,吸附剂Carbopack B/CarbosieveTM S-Ⅲ对VOC单体具有更好的吸附性能,更适合于有机物的吸附捕集.本方法对VOC单体的最小检出限(LODs)范围为0.01 ~0.4 μg/m3,方法的加标回收率为90% ~109%,相对标准偏差(RSD)小于11%.用该法测试多种市售墙纸的VOCs,发现墙纸释放VOCs的种类与墙纸材料有较大关联.纸基墙纸的释放量较低,只释放少量的1-丁醇和丙二醇;无纺墙纸和PVC墙纸释放出较多的甲苯、苯乙烯、2-乙基-1-己醇、壬醛和萘等;而金属墙纸则释放出较多的直链或支链烷烃. 展开更多
关键词 墙纸 挥发性有机物(VOCs) 测试舱 热脱附 质谱法
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