Poor casting properties restrict the application of high strength casting Al-5.0%Cu alloy. The addition of element can improve the casting properties of this alloy. Effect of Si on the casting properties of Al-5.0%Cu ...Poor casting properties restrict the application of high strength casting Al-5.0%Cu alloy. The addition of element can improve the casting properties of this alloy. Effect of Si on the casting properties of Al-5.0%Cu alloy was studied. It has been found that the addition of Si can improve the casting properties of Al-5.0%Cu alloy obviously. With the increase of Si content, the hot cracking tendency of the alloy decreases significantly, and the fluidity of the alloy increases firstly and then decreases slowly. When the content of Si element is higher than 2wt.%, the fluidity of the alloy increases greatly with the increasing of Si content.展开更多
The preparation procedure of DD5 single crystal castings was optimized. The microstructure characteristics of DD5 single crystal superalloy were investigated by microstructure observation and segregation behavior exam...The preparation procedure of DD5 single crystal castings was optimized. The microstructure characteristics of DD5 single crystal superalloy were investigated by microstructure observation and segregation behavior examination. The results show that the grain orientation is optimized by constraining the spiral crystallizer in [001] orientation and spatial scale. Also, the γ' phase of inter-dendrites is larger and more irregular than that in dendrite arms. High temperature tensile tests of DD5 single crystal castings exhibit that the peak stress increases with increasing temperature, while the area reduction shows an opposite trend, when the temperature is below 800℃; meanwhile, when the temperature is between 800℃ and 1000℃, the fracture stress of the alloy is the same as the peak stress. The fracture mode changes from shear to ductile with increasing temperature from 600℃ and 1000℃.展开更多
Centrifugal casting was applied to produce cylindrical castings using SiCp/Al composite slurry,which contained 20%SiC particles.The castings comprised a particle free zone and a particle rich zone.The amount of SiC pa...Centrifugal casting was applied to produce cylindrical castings using SiCp/Al composite slurry,which contained 20%SiC particles.The castings comprised a particle free zone and a particle rich zone.The amount of SiC particles had a dramatic transformation from the particle rich zone to the particle free zone,and the maximum content of SiC particles in the particle rich zone reached up to 40 vol%.The ultimate tensile strength(UTS) of the as-cast SiCp / Al composites in the particle rich zone was 143 MPa,and the fracture was caused by the desorption of SiC particles from matrix alloy.The coefficient of thermal expansion(CTE) of the SiC_p / Al composites in the range of 20 and 100 ℃ was determined as 16.67×10^(-6) s^(-1),and the experimental CTE was lower than the predicted data based on the Kerner's model.The results show that the decrease in CTE in the case of the composites at high temperature stage can be attributed to the solute concentration of Si in Al and the plastic deformation of the matrix alloy in the composites with void architecture.展开更多
The microstructure and mechanical properties of as-cast A356(Al–Si) alloy castings were investigated. A356 alloy was cast into three different molds composed of sand, ferrochrome(Fe–Cr) slag, and a mixture of sa...The microstructure and mechanical properties of as-cast A356(Al–Si) alloy castings were investigated. A356 alloy was cast into three different molds composed of sand, ferrochrome(Fe–Cr) slag, and a mixture of sand and Fe–Cr. A sodium silicate–CO_2 process was used to make the necessary molds. Cylindrical-shaped castings were prepared. Cast products with no porosity and a good surface finish were achieved in all of the molds. These castings were evaluated for their metallography, secondary dendrite arm spacing(SDAS), and mechanical properties, including hardness, compression, tensile, and impact properties. Furthermore, the tensile and impact samples were analyzed by fractography. The results show that faster heat transfer in the Fe–Cr slag molds than in either the silica sand or mixed molds led to lower SDAS values with a refined microstructure in the products cast in Fe–Cr slag molds. Consistent and enhanced mechanical properties were observed in the slag mold products than in the castings obtained from either sand or mixed molds. The fracture surface of the slag mold castings shows a dimple fracture morphology with a transgranular fracture nature. However, the fracture surfaces of the sand mold castings display brittle fracture. In conclusion, products cast in Fe–Cr slag molds exhibit an improved surface finish and enhanced mechanical properties compared to those of products cast in sand and mixed molds.展开更多
Mg matrix composites with SiC particles ranging from 5vol%-25vol% were prepared using stirring casting method. Die casting, squeezing casting, and extrusion were applied for inhibiting or eliminating the defects such ...Mg matrix composites with SiC particles ranging from 5vol%-25vol% were prepared using stirring casting method. Die casting, squeezing casting, and extrusion were applied for inhibiting or eliminating the defects such as gas porosity and shrinkage void. Through die casting and squeezing casting, most of the defects in Mg matrix composites could be eliminated, but the mechanical properties were improved limitedly. On the other hand, after hot extrusion, not only most of the defects of as-cast composites ingots were eliminated, but also the mechanical properties were improved markedly. With the addition of SiC, the tensile strength, yield strength and elastic modulus of as extrusion SiCp/AZ61 composites increased remarkably, and the elongation decreased obviously.展开更多
The purpose of this study was to prepare high-quality Al-Si-Mg-Mn alloy with a good combination of strength and ductility employing the vacuum-assisted high-pressure die cast process. An orthogonal study of heat treat...The purpose of this study was to prepare high-quality Al-Si-Mg-Mn alloy with a good combination of strength and ductility employing the vacuum-assisted high-pressure die cast process. An orthogonal study of heat treatments was conducted to design an optimized T6 heat treatment process for both Al-10%Si-0.3%Mg-Mn and Al-11%Si-0.6%Mg-Mn alloys. The results demonstrate that no obvious blisters and warpage were observed in these two alloys with solid solution treatment. After the optimal T6 heat treatment of 530°C×3 h + 165°C×6 h, Al-11%Si-0.6%Mg-Mn alloy has better mechanical properties, of which tensile strength, yield strength and elongation reached 377.3 MPa, 307.8 MPa and 9%, respectively. The improvement of mechanical properties can be attributed to the high density of needle-like β″(Mg_5Si_6) precipitation after aging treatment and the fine and spherical eutectic Si particles uniformly distributed in the α-Al matrix.展开更多
This paper reports some results obtained in an investigation to see how increasing the corundum dispersoid content from o% to 7% in a matrix of hiduminium alloy affects the tensile and compressive strengths, the hardn...This paper reports some results obtained in an investigation to see how increasing the corundum dispersoid content from o% to 7% in a matrix of hiduminium alloy affects the tensile and compressive strengths, the hardness and the casting characteristics of the composite. The results show that as the corundum content is increased, ultimate tensile strength (UTS)- compressive strength and hardness increase remarkably, whereas fluidity of the molten composite during casting drops significantly. It was found that just a minute amount of corundum is sufficient to cause a fairly large change in the mechanical properties and the fluidity of the molten material.This drop in castability is one of the reasons why adding corundum beyond 7 percent is not recommended. If other factors are kept constant, the fluidity is seen to slightly improve if the pouring temperature of the molten metal were increased from 670 to 710℃展开更多
The research and development status of casting magnesium alloys including the commercial casting alloys and the new types casting alloys are reviewed,with more attention to microstructure and mechanical properties of ...The research and development status of casting magnesium alloys including the commercial casting alloys and the new types casting alloys are reviewed,with more attention to microstructure and mechanical properties of modified-AZ91,AM60 and WE43 alloys with various additions,and new types of low cost casting alloys and high strength casting alloys.The modification and/or refinement of Mg2 Si phase in Mg-Al-Si based casting alloys by various additions are discussed and new purifying technologies for casting magnesium alloys are introduced to improve the performance.The modified AZ81 alloy with reduced impurities is found to have the tensile strength of 280 ± 6 MPa and elongation of 16% ± 0.7%.The fatigue strength of AZ91 D alloy could be obviously improved by addition of Ce and Nd.The Mg-16Gd-2Ag-0.3Zr alloy exhibits very high tensile and yield strengths(UTS:423 MPa and YS:328 MPa);however,its elongation still needs to be improved.展开更多
A novel processing route involving strip casting, pre-annealing treatment, cold rolling and recrystallization annealing was applied to a Fe-2.6%Si steel to improve the magnetic properties. The impact of as-cast strip ...A novel processing route involving strip casting, pre-annealing treatment, cold rolling and recrystallization annealing was applied to a Fe-2.6%Si steel to improve the magnetic properties. The impact of as-cast strip pre-annealing on the microstructure, texture, precipitation and magnetic properties were investigated by electron probe micro-analysis, transmission electron microscopy, and X-ray diffraction analysis,etc. It was found that the precipitation of second-phase particles during strip casting was restrained by rapid solidification. The absence of pre-annealing led to the occurrence of a large amount of 20-50 nm Mn S precipitates in the final annealed sheets, which is responsible for fine grains and high core loss(4.01 W/kg) due to grain boundary pinning effect. Although the microstructure and texture of 900-1000?C pre-annealed samples were similar to those of as-cast strip, significant grain coarsening together with the strengthening of-fiber texture was observed in the 1100?C pre-annealed strips. In comparison with the case of as-cast strip, a higher amount of large-sized precipitates consisting of manganese sulfide and/or aluminum nitride occurred in matrix after pre-annealing. Correspondingly, in the final annealed sheets, the number density of precipitates with sizes smaller than 100 nm was substantially reduced, and100-200 nm and 200-500 nm sized particles became more dominant in samples subjected to 30-min and 120-min pre-annealing treatments respectively. In addition, the average grain size of final annealed sheets increased with the pre-annealing temperature and time because of the weakened pining effect of coarsen precipitates. Ultimately, the magnetic induction of samples subjected to pre-annealing was slightly increased and ranged from 1.73 T to 1.75 T owing to the enhancement of {100} recrystallization texture, and simultaneously the core loss significantly decreased until a minimum of 3.26 W/kg was reached. Nevertheless, large number of 200-500 nm particles presented during pre-annealing for 120 min could weaken the improvement in core loss which is likely associated with the pinning effect on magnetic domain wall.展开更多
基金This work was financiallysupported by the Fund of BeijingJiaotong University(No.2004SZ006).
文摘Poor casting properties restrict the application of high strength casting Al-5.0%Cu alloy. The addition of element can improve the casting properties of this alloy. Effect of Si on the casting properties of Al-5.0%Cu alloy was studied. It has been found that the addition of Si can improve the casting properties of Al-5.0%Cu alloy obviously. With the increase of Si content, the hot cracking tendency of the alloy decreases significantly, and the fluidity of the alloy increases firstly and then decreases slowly. When the content of Si element is higher than 2wt.%, the fluidity of the alloy increases greatly with the increasing of Si content.
基金financially supported by Jiangsu Industrial Support Project (Nos. BE2014007-2, BE2014007-3, and BE2014007-4)the financial support from Jiangsu Development and Reform Commission (No. [2013]2027)Jiangsu Postgraduates Innovating Scientific Research Project (No. KYLX15-1061)
文摘The preparation procedure of DD5 single crystal castings was optimized. The microstructure characteristics of DD5 single crystal superalloy were investigated by microstructure observation and segregation behavior examination. The results show that the grain orientation is optimized by constraining the spiral crystallizer in [001] orientation and spatial scale. Also, the γ' phase of inter-dendrites is larger and more irregular than that in dendrite arms. High temperature tensile tests of DD5 single crystal castings exhibit that the peak stress increases with increasing temperature, while the area reduction shows an opposite trend, when the temperature is below 800℃; meanwhile, when the temperature is between 800℃ and 1000℃, the fracture stress of the alloy is the same as the peak stress. The fracture mode changes from shear to ductile with increasing temperature from 600℃ and 1000℃.
基金Funded by the National Natural Science Foundation of China(No.51174244)the Foundational and Cutting-edge Research Plan of Chongqing,China(No.csts2013jcyj A50014)the Fundamental Research Funds for Central University,China(No.CDJZR12240056)
文摘Centrifugal casting was applied to produce cylindrical castings using SiCp/Al composite slurry,which contained 20%SiC particles.The castings comprised a particle free zone and a particle rich zone.The amount of SiC particles had a dramatic transformation from the particle rich zone to the particle free zone,and the maximum content of SiC particles in the particle rich zone reached up to 40 vol%.The ultimate tensile strength(UTS) of the as-cast SiCp / Al composites in the particle rich zone was 143 MPa,and the fracture was caused by the desorption of SiC particles from matrix alloy.The coefficient of thermal expansion(CTE) of the SiC_p / Al composites in the range of 20 and 100 ℃ was determined as 16.67×10^(-6) s^(-1),and the experimental CTE was lower than the predicted data based on the Kerner's model.The results show that the decrease in CTE in the case of the composites at high temperature stage can be attributed to the solute concentration of Si in Al and the plastic deformation of the matrix alloy in the composites with void architecture.
基金the DST–Fly Ash unit, New Delhi, India for their financial support (Grant Ref No.FAU/DST/600(52)/2012-13)Advance Analytical laboratory, Andhra University, India for the support in SEM–EDS studies
文摘The microstructure and mechanical properties of as-cast A356(Al–Si) alloy castings were investigated. A356 alloy was cast into three different molds composed of sand, ferrochrome(Fe–Cr) slag, and a mixture of sand and Fe–Cr. A sodium silicate–CO_2 process was used to make the necessary molds. Cylindrical-shaped castings were prepared. Cast products with no porosity and a good surface finish were achieved in all of the molds. These castings were evaluated for their metallography, secondary dendrite arm spacing(SDAS), and mechanical properties, including hardness, compression, tensile, and impact properties. Furthermore, the tensile and impact samples were analyzed by fractography. The results show that faster heat transfer in the Fe–Cr slag molds than in either the silica sand or mixed molds led to lower SDAS values with a refined microstructure in the products cast in Fe–Cr slag molds. Consistent and enhanced mechanical properties were observed in the slag mold products than in the castings obtained from either sand or mixed molds. The fracture surface of the slag mold castings shows a dimple fracture morphology with a transgranular fracture nature. However, the fracture surfaces of the sand mold castings display brittle fracture. In conclusion, products cast in Fe–Cr slag molds exhibit an improved surface finish and enhanced mechanical properties compared to those of products cast in sand and mixed molds.
基金Funded by the Program for New Century Excellent Talents in University(NCET-12-1040)the National Natural Science Foundation of China(Nos.50901048 and 51174143)+2 种基金the Key Project of Chinese Ministry of Education(No.2012017)the Program Foundation of Ministry of Education of China(No.20101402110008)Natural Science Foundation of Shanxi(No.2010021022-5)
文摘Mg matrix composites with SiC particles ranging from 5vol%-25vol% were prepared using stirring casting method. Die casting, squeezing casting, and extrusion were applied for inhibiting or eliminating the defects such as gas porosity and shrinkage void. Through die casting and squeezing casting, most of the defects in Mg matrix composites could be eliminated, but the mechanical properties were improved limitedly. On the other hand, after hot extrusion, not only most of the defects of as-cast composites ingots were eliminated, but also the mechanical properties were improved markedly. With the addition of SiC, the tensile strength, yield strength and elastic modulus of as extrusion SiCp/AZ61 composites increased remarkably, and the elongation decreased obviously.
基金financially supported by the Jiangsu province transformation of scientific and technological achievements program(BA2015041)the Jiangsu key laboratory for advanced metallic materials(BM2007204)
文摘The purpose of this study was to prepare high-quality Al-Si-Mg-Mn alloy with a good combination of strength and ductility employing the vacuum-assisted high-pressure die cast process. An orthogonal study of heat treatments was conducted to design an optimized T6 heat treatment process for both Al-10%Si-0.3%Mg-Mn and Al-11%Si-0.6%Mg-Mn alloys. The results demonstrate that no obvious blisters and warpage were observed in these two alloys with solid solution treatment. After the optimal T6 heat treatment of 530°C×3 h + 165°C×6 h, Al-11%Si-0.6%Mg-Mn alloy has better mechanical properties, of which tensile strength, yield strength and elongation reached 377.3 MPa, 307.8 MPa and 9%, respectively. The improvement of mechanical properties can be attributed to the high density of needle-like β″(Mg_5Si_6) precipitation after aging treatment and the fine and spherical eutectic Si particles uniformly distributed in the α-Al matrix.
文摘This paper reports some results obtained in an investigation to see how increasing the corundum dispersoid content from o% to 7% in a matrix of hiduminium alloy affects the tensile and compressive strengths, the hardness and the casting characteristics of the composite. The results show that as the corundum content is increased, ultimate tensile strength (UTS)- compressive strength and hardness increase remarkably, whereas fluidity of the molten composite during casting drops significantly. It was found that just a minute amount of corundum is sufficient to cause a fairly large change in the mechanical properties and the fluidity of the molten material.This drop in castability is one of the reasons why adding corundum beyond 7 percent is not recommended. If other factors are kept constant, the fluidity is seen to slightly improve if the pouring temperature of the molten metal were increased from 670 to 710℃
基金supported by the National Natural Science Foundation of China(Grant Nos.51531002,51474043 and 51571043)the Ministry of Education of China(SRFDR 20130191110018)+1 种基金Chongqing Municipal Government(CSTC2013JCYJC60001,CEC project,Two River Scholar Project and The Chief Scientist Studio Project)Fundamental Research Funds for the Central Universities(No.106112015CDJZR135515)
文摘The research and development status of casting magnesium alloys including the commercial casting alloys and the new types casting alloys are reviewed,with more attention to microstructure and mechanical properties of modified-AZ91,AM60 and WE43 alloys with various additions,and new types of low cost casting alloys and high strength casting alloys.The modification and/or refinement of Mg2 Si phase in Mg-Al-Si based casting alloys by various additions are discussed and new purifying technologies for casting magnesium alloys are introduced to improve the performance.The modified AZ81 alloy with reduced impurities is found to have the tensile strength of 280 ± 6 MPa and elongation of 16% ± 0.7%.The fatigue strength of AZ91 D alloy could be obviously improved by addition of Ce and Nd.The Mg-16Gd-2Ag-0.3Zr alloy exhibits very high tensile and yield strengths(UTS:423 MPa and YS:328 MPa);however,its elongation still needs to be improved.
基金financially supported by the National Natural Science Foundation of China(Nos.51674080,51404155 and U1260204)the Program for New Century Excellent Talents in University(No.NCET-13-0111)+1 种基金the Program for Liaoning Excellent Talents in University(No.LR2014007)support from the University of Texas at El Paso
文摘A novel processing route involving strip casting, pre-annealing treatment, cold rolling and recrystallization annealing was applied to a Fe-2.6%Si steel to improve the magnetic properties. The impact of as-cast strip pre-annealing on the microstructure, texture, precipitation and magnetic properties were investigated by electron probe micro-analysis, transmission electron microscopy, and X-ray diffraction analysis,etc. It was found that the precipitation of second-phase particles during strip casting was restrained by rapid solidification. The absence of pre-annealing led to the occurrence of a large amount of 20-50 nm Mn S precipitates in the final annealed sheets, which is responsible for fine grains and high core loss(4.01 W/kg) due to grain boundary pinning effect. Although the microstructure and texture of 900-1000?C pre-annealed samples were similar to those of as-cast strip, significant grain coarsening together with the strengthening of-fiber texture was observed in the 1100?C pre-annealed strips. In comparison with the case of as-cast strip, a higher amount of large-sized precipitates consisting of manganese sulfide and/or aluminum nitride occurred in matrix after pre-annealing. Correspondingly, in the final annealed sheets, the number density of precipitates with sizes smaller than 100 nm was substantially reduced, and100-200 nm and 200-500 nm sized particles became more dominant in samples subjected to 30-min and 120-min pre-annealing treatments respectively. In addition, the average grain size of final annealed sheets increased with the pre-annealing temperature and time because of the weakened pining effect of coarsen precipitates. Ultimately, the magnetic induction of samples subjected to pre-annealing was slightly increased and ranged from 1.73 T to 1.75 T owing to the enhancement of {100} recrystallization texture, and simultaneously the core loss significantly decreased until a minimum of 3.26 W/kg was reached. Nevertheless, large number of 200-500 nm particles presented during pre-annealing for 120 min could weaken the improvement in core loss which is likely associated with the pinning effect on magnetic domain wall.