Interfacial Bonding Strength of TiN Film Coated on Si_3N_4 Ceramic Substrate

The fraction of TiN/Si3N4 in the cross section was observed with scanning electric microscope （SEM）, and residual stresses of TiN coated on the surface of Si3N4 ceramic were measured with X-ray diffraction （XRD）.The hardness of TiN film was measured, and bonding strength of TiN film coated on Si3N4 substrate was measured by scratching method. The formed mechanism of residual stress and the failure mechanism of the bonding interface in the film were analyzed, and the adhesion mechanism of TiN film was investigated preliminarily. The results show that residual stresses of TiN film are all behaved as compressive stress, and TiN film is represented smoothly with brittle fracture, which is closely bonded with Si3N4 substrate. TiN film has high hardness and bonding strength of about 500 MPa, which could satisfy usage requests of the surface of cutting Si3N4 ceramic.

Crack patterns corresponding to the residual strength plateau of ceramics subjected to thermal shock

The formation strength plateau of ceramics is addressed. A set of of 99A1203 are conducted, mechanism of the residual subjected to thermal shock thermal shock experiments where the thin specimens of 1 mm× 10 mm×50 mm exhibit parallel through edge cracks, and thus permit quantitative measurements of the crack patterns. The cracks evolve with the severity of ther- mal shock. It is found that there is a correlation between the length and density of the thermal shock cracks. The increase of crack length weakens the residual strength, whereas the increase of crack density improves it. In a considerably wide temperature range, the two contrary effects just counteract each other; consequently a plateau appears in the variation curve of the residual strength. A comparison between the numerical and experimental results of the residual strength is made, and they are found in good agreement. This work is helpful to a deep understanding of the thermal shock failure of ceramics.

Detection technology of micro residual core in small inner cavity of complex castings

A new technology for detecting a tiny residual core in the small inner cavity of complex castings is proposed. The residual core is identified by using image recognition technology. Tracer processing and image signal processing are combined to enhance the image contrast. The relationships between the concentration of tracer, the size of the residual core, the wall thickness of the castings and the contrast were obtained. Based on the experimental data, the minimum detectable amount of residual core under different conditions was obtained. The results show that the minimum detectable amount decreases from 4.398 mg to 0.438 mg for the 1.0 mm wall thickness casting when the concentration of tracer increases from 0% to 20%. The signal-to-noise ratio(SNR) of the detection results increases by 27.010 by means of average filtering and linear point operation. The subtraction of image and image background was performed, and then the boundary extraction was carried out to obtain a clear and reliable result. The experimental results show that the non-traced residual core cannot be detected for a blade with a thickness less than 5 mm. The residual core of 1 mm thickness can be barely identified by artificial recognition after tracer processing and image processing, while the residual core of 0.6 mm thickness can be detected clearly using image recognition technology.