Nanometer TiO 2 powders were obtained from TiOSO 4 and studied by XRD, TEM and BET. The result indicated that pH and heat treatment temperature have great effects on their grain size and crystal phase structu...Nanometer TiO 2 powders were obtained from TiOSO 4 and studied by XRD, TEM and BET. The result indicated that pH and heat treatment temperature have great effects on their grain size and crystal phase structure. Annealed at 500 ℃, nanometer TiO 2 with a specific surface area of 101.39 m 2 ·g -1 and a grain size about 10 nm were obtained(pH=5); and with a specific surface area of 95.48 m 2 ·g -1 and a grain size about 30 nm were obtained(pH=10). The research indicated that crystal phase transformation of rutile at 750 ℃made great promotion in grain size growth.展开更多
Nanometer TiO 2 powders were obtained from TiOSO 4 and studied by XRD, TEM and BET. The result indicated that pH and heat treatment temperature have great effects on their grain size and crystal phase structu...Nanometer TiO 2 powders were obtained from TiOSO 4 and studied by XRD, TEM and BET. The result indicated that pH and heat treatment temperature have great effects on their grain size and crystal phase structure. Annealed at 500 ℃, nanometer TiO 2 with a specific surface area of 101.39 m 2 ·g -1 and a grain size about 10 nm were obtained(pH=5); and with a specific surface area of 95.48 m 2 ·g -1 and a grain size about 30 nm were obtained(pH=10). The research indicated that crystal phase transformation of rutile at 750 ℃made great promotion in grain size growth.展开更多
The electrical resistivity of NZ30K-Mg alloy was measured at different heating rates during continuous heating to stud the precipitation kinetics.Two kinds of metastable phases,β＂ and β＇,formed during the heating....The electrical resistivity of NZ30K-Mg alloy was measured at different heating rates during continuous heating to stud the precipitation kinetics.Two kinds of metastable phases,β＂ and β＇,formed during the heating.Kissinger method and differentia isoconversional method were employed to assess the precipitation kinetic parameters of NZ30K-Mg alloy,activation energy Eα an pre-exponential factor A＇α.The fraction of transformation（α） and the precipitation sequence in NZ30K-Mg alloy were determinec Continuous heating transformation（CHT） and isothermal heating transformation（IHT） diagrams were further obtained for guidin the aging of NZ30K-Mg alloy.The analysis shows that the precipitation kinetic parameters of NZ30K-Mg alloy can be obtaine accurately using isoconversional method.展开更多
In this study, Zanjan from Iran has been chosen from among all the semi-arid regions of world, which has Synoptic station and statistical data since 1955. Spring and monthly precipitations are also provided in the per...In this study, Zanjan from Iran has been chosen from among all the semi-arid regions of world, which has Synoptic station and statistical data since 1955. Spring and monthly precipitations are also provided in the period of 1956-2005. First, all data has been controlled by double mass method with the help of adjacent stations, and then it was normalized by the box-cox transformations method. The global SPI index was calculated for all months and spring, also drought and wet periods were determined and finally compared. In the drought category view, spring months have represented the great similarities. The moving averages are represented all months and spring’s precipitations such as three years, five years, seven years and nine years are shown. Statistical period was observed and analyzed based on five periods of ten years, and results precipitation with more than 5mm and 10mm has gradually decreased on April. However the number of days with precipitation has increased. The calculated spring precipitations and all of the atmospheric factors represented the dependence of this model to maximum average of spring temperature and relative humidity of spring and winter by the use of multi variable regression method. The predicted precipitation of spring also showed the gradual decline of precipitation in the next 30 years by the arima model.展开更多
The particle sizes of ultrafine powders are between cluster and fine powders, with theparticle diameters generally in the range of 1--100nm. When compared with commonmaterials consisting of bigger particles, materials...The particle sizes of ultrafine powders are between cluster and fine powders, with theparticle diameters generally in the range of 1--100nm. When compared with commonmaterials consisting of bigger particles, materials consisting of nanometer-size particleshave many special properties. These include small-sized effect, surface and interface展开更多
文摘Nanometer TiO 2 powders were obtained from TiOSO 4 and studied by XRD, TEM and BET. The result indicated that pH and heat treatment temperature have great effects on their grain size and crystal phase structure. Annealed at 500 ℃, nanometer TiO 2 with a specific surface area of 101.39 m 2 ·g -1 and a grain size about 10 nm were obtained(pH=5); and with a specific surface area of 95.48 m 2 ·g -1 and a grain size about 30 nm were obtained(pH=10). The research indicated that crystal phase transformation of rutile at 750 ℃made great promotion in grain size growth.
文摘Nanometer TiO 2 powders were obtained from TiOSO 4 and studied by XRD, TEM and BET. The result indicated that pH and heat treatment temperature have great effects on their grain size and crystal phase structure. Annealed at 500 ℃, nanometer TiO 2 with a specific surface area of 101.39 m 2 ·g -1 and a grain size about 10 nm were obtained(pH=5); and with a specific surface area of 95.48 m 2 ·g -1 and a grain size about 30 nm were obtained(pH=10). The research indicated that crystal phase transformation of rutile at 750 ℃made great promotion in grain size growth.
基金Project (2011ZX04014-052,2012ZX04012011) supported by CNC Machine Tools and Basic Manufacturing Equipment Technology Comments
文摘The electrical resistivity of NZ30K-Mg alloy was measured at different heating rates during continuous heating to stud the precipitation kinetics.Two kinds of metastable phases,β＂ and β＇,formed during the heating.Kissinger method and differentia isoconversional method were employed to assess the precipitation kinetic parameters of NZ30K-Mg alloy,activation energy Eα an pre-exponential factor A＇α.The fraction of transformation（α） and the precipitation sequence in NZ30K-Mg alloy were determinec Continuous heating transformation（CHT） and isothermal heating transformation（IHT） diagrams were further obtained for guidin the aging of NZ30K-Mg alloy.The analysis shows that the precipitation kinetic parameters of NZ30K-Mg alloy can be obtaine accurately using isoconversional method.
文摘In this study, Zanjan from Iran has been chosen from among all the semi-arid regions of world, which has Synoptic station and statistical data since 1955. Spring and monthly precipitations are also provided in the period of 1956-2005. First, all data has been controlled by double mass method with the help of adjacent stations, and then it was normalized by the box-cox transformations method. The global SPI index was calculated for all months and spring, also drought and wet periods were determined and finally compared. In the drought category view, spring months have represented the great similarities. The moving averages are represented all months and spring’s precipitations such as three years, five years, seven years and nine years are shown. Statistical period was observed and analyzed based on five periods of ten years, and results precipitation with more than 5mm and 10mm has gradually decreased on April. However the number of days with precipitation has increased. The calculated spring precipitations and all of the atmospheric factors represented the dependence of this model to maximum average of spring temperature and relative humidity of spring and winter by the use of multi variable regression method. The predicted precipitation of spring also showed the gradual decline of precipitation in the next 30 years by the arima model.
基金National Natural Science Foundaion of ChinaChinese Academy of Sciences
文摘The particle sizes of ultrafine powders are between cluster and fine powders, with theparticle diameters generally in the range of 1--100nm. When compared with commonmaterials consisting of bigger particles, materials consisting of nanometer-size particleshave many special properties. These include small-sized effect, surface and interface
