Geological characteristics and exploration breakthroughs of coal rock gas in Carboniferous Benxi Formation,Ordos Basin,NW China

To explore the geological characteristics and exploration potential of the Carboniferous Benxi Formation coal rock gas in the Ordos Basin,this paper presents a systematic research on the coal rock distribution,coal rock reservoirs,coal rock quality,and coal rock gas features,resources and enrichment.Coal rock gas is a high-quality resource distinct from coalbed methane,and it has unique features in terms of burial depth,gas source,reservoir,gas content,and carbon isotopic composition.The Benxi Formation coal rocks cover an area of 16×104km^(2),with thicknesses ranging from 2 m to 25 m,primarily consisting of bright and semi-bright coals with primitive structures and low volatile and ash contents,indicating a good coal quality.The medium-to-high rank coal rocks have the total organic carbon(TOC)content ranging from 33.49%to 86.11%,averaging75.16%.They have a high degree of thermal evolution(Roof 1.2%-2.8%),and a high gas-generating capacity.They also have high stable carbon isotopic values(δ13C1of-37.6‰to-16‰;δ13C2of-21.7‰to-14.3‰).Deep coal rocks develop matrix pores such as gas bubble pores,organic pores,and inorganic mineral pores,which,together with cleats and fractures,form good reservoir spaces.The coal rock reservoirs exhibit the porosity of 0.54%-10.67%(averaging 5.42%)and the permeability of(0.001-14.600)×10^(-3)μm^(2)(averaging 2.32×10^(-3)μm^(2)).Vertically,there are five types of coal rock gas accumulation and dissipation combinations,among which the coal rock-mudstone gas accumulation combination and the coal rock-limestone gas accumulation combination are the most important,with good sealing conditions and high peak values of total hydrocarbon in gas logging.A model of coal rock gas accumulation has been constructed,which includes widespread distribution of medium-to-high rank coal rocks continually generating gas,matrix pores and cleats/fractures in coal rocks acting as large-scale reservoir spaces,tight cap rocks providing sealing,source-reservoir integration,and five types of efficient enrichment patterns(lateral pinchout complex,lenses,low-amplitude structures,nose-like structures,and lithologically self-sealing).According to the geological characteristics of coal rock gas,the Benxi Formation is divided into 8 plays,and the estimated coal rock gas resources with a buried depth of more than 2000 m are more than 12.33×10^(12)m^(3).The above understandings guide the deployment of risk exploration.Two wells drilled accordingly obtained an industrial gas flow,driving the further deployment of exploratory and appraisal wells.Substantial breakthroughs have been achieved,with the possible reserves over a trillion cubic meters and the proved reserves over a hundred billion cubic meters,which is of great significance for the reserves increase and efficient development of natural gas in China.

Damage characteristics and catastrophic failure mechanism of coal rock induced by gas adsorption under compression

To reveal the damage characteristics and catastrophic failure mechanism of coal rock caused by gas adsorption,physical tests and theoretical methods are employed.The results show that adsorption swelling can damage coal rock,which can be distinguished by fractal dimension.A fitting relationship between the adsorption damage and fractal dimension is proposed by experimental testing and theoretical analysis.High gas adsorption pressure proves to be the dominant factor that leads to coal failure softening and gas outburst disasters.Three main parameters concerning adsorption damage include the change rate of released energy density,the transition difference in the post-peak acoustic emission(AE)b value and the change rate of cumulative AE energy.Results show that all the three parameters present a step-type decreasing change with the increase in fractal dimension,and the fractal dimension shows a linear relationship within the same failure mode.Finally,a method is proposed to evaluate coal rock disaster transformation,based on the aforementioned three main parameters of adsorption damage.

Platinum and Palladium in Coal Rock and Geochemical Anomaly in Eastern Yunnan Province,Southwest China

A series of geochemical anomalies of Pt and Pd were found in 1 358 recombined samples from a geochemical stream sediment survey in eastern Yunnan （云南） Province, China. Chemical optical emission spectroscopy, X-ray fluorescence analysis, and inductively coupled plasmas atomic emission spectrometry analyses of 22 elements and chemical compositions of 21 samples from coal-bearing strata from the Late Paleozoic, Mesozoic, and Cenozoic show Pt and Pd concentrated to some extent in coal rocks, with Pd/Pt〈1. As, Pt, B, Au, Pd, V, Sb, U, Pb, and W are enriched in the Lower Carboniferous coal-bearing strata of the Wanshoushan （万寿山） Formation; B, Mo, As, Pt, U, W, Pb, Pd, and V are enriched in the Lower Permian coal-bearing strata of the Liangshan （梁山） Formation; Pt, Cu, Mo, Pd, As, V, and Ag are enriched in the Upper Permian coal-bearing strata of the Xuanwei （宣威） Formation; As, B, Pb, Pt, Pd, U, W, Sb, Mo, Zn, and Ag are enriched in the Upper Triassic coal-bearing strata of the Xujiahe （须家河） Formation; and Pt, As, and Pb are enriched in the lignite of the Pliocene Ciying （茨营） Formation. Combining analyses of the sedimentary environment and local volcanic activity reveal that the coalbearing strata in the Xuanwei Formation are possibly related to the Permian Emeishan （峨眉山） basalt.

Coal Rock Condition Detection Model Using Acoustic Emission and Light Gradient Boosting Machine

Coal rock mass instability fracture may result in serious hazards to underground coal mining.Acoustic emissions(AE)stimulated by internal structure fracture should carry lots of favorable information about health condition of rock mass.AE as a sensitive non-destructive test method is gradually utilized to detect anomaly conditions of coal rock.This paper proposes an improved multi-resolution feature to extract AE waveform at different frequency resolutions using Coilflet Wavelet Transform method(CWT).It is further adopt an efficient Light Gradient Boosting Machine(LightGBM)by several cascaded sub weak classifier models to merge AE features at different views of frequency for coal rock anomaly damage recognition.The results denote that the proposed method achieves excellent recognition performance on anomaly damage levels of coal rock.It is an effective method to detect the critical stability further to predict the rock mass bursting in time.

Effects of thermal treatment on physical and mechanical characteristics of coal rock

To study the physical and mechanical properties of coal rock after treatment at different temperatures under impact loading, dynamic compression experiments were conducted by using a split Hopkinson pressure bar(SHPB). The stress–strain curves of specimens under impact loading were obtained, and then four indexes affected by temperature were analyzed in the experiment: the longitudinal wave velocity, elastic modulus, peak stress and peak strain. Among these indexes, the elastic modulus was utilized to express the specimens' damage characteristics. The results show that the stress–strain curves under impact loading lack the stage of micro-fissure closure and the slope of the elastic deformation stage is higher than that under static loading. Due to the dynamic loading effect, the peak stress increases while peak strain decreases. The dynamic mechanical properties of coal rock show obvious temperature effects. The longitudinal wave velocity, elastic modulus and peak stress all decrease to different extents with increasing temperature, while the peak strain increases continuously. During the whole heating process, the thermal damage value continues to increase linearly, which indicates that the internal structure of coal rock is gradually damaged by high temperature.

Characteristics of acoustic emission signals in damp cracking coal rocks

A uniaxial load experiment on coal rocks at different stress rates was carried out, based on the characteristics of acoustic emission (AE) signals in cracking coal rocks, decomposition, de-noising and reconstruction for the AE signals through wavelet packet transform for solving the current problems created by the presence of noise in AE signals and the existing problems in AE signal processing. The results show that the various characteristics of AE signals in coal rocks cracking under different situations can be clearly reflected, after the AE signals are de-noised by the wavelet packet. Compared to dry coal rocks, the number of AE occurrences in damp coal rocks was significantly reduced, as well as the average amplitude. The number of AE occurrences in damp and dry coal rocks clearly increased with increases in the loading rate, but the largest amplitude of the AE signals in damp coal rocks has been reduced. There is no clear evidence of change in dry coal rocks.

Surrounding Rock Failure Mechanism and Control Technology of Gob-Side Entry with Triangle Coal Pillar at Island Longwall Panel in 15 m Extra-Thick Coal Seams

Taking the return air roadway of Tashan 8204 isolated island working face as the background, the evolution law of the stress field in the surrounding rock of the widened coal pillar area roadway during the mining period of the isolated island working face is obtained through numerical simulation. The hazardous area of strong mine pressure under different coal pillar widths is determined. Through simulation, it is known that when the width of the coal pillar is less than 20 m, there is large bearing capacity on the coal side of the roadway entity. The force on the side of the coal pillar is relatively small. When the width of the coal pillar ranges from 25 m to 45 m, the vertical stress on the roadway and surrounding areas is relatively high. Pressure relief measures need to be taken during mining to reduce surrounding rock stress. When the width of the coal pillar is greater than 45 m, the peak stress of the coal pillar is located in the deep part of the surrounding rock, but it still has a certain impact on the roadway. It is necessary to take pressure relief measures to transfer the stress to a deeper depth to ensure the stability of the triangular coal pillar during the safe mining period of the working face. This provides guidance for ensuring the stability of the triangular coal pillar during the safe mining period of the working face.

P-wave and S-wave response of coal rock containing gas-water with different saturation: an experimental perspective

The acoustic response of gas and/or water saturated coal rock is fundamental for establishing the correspondence between the physical properties of the coal reservoir and the characteristics of the well-logging response,which is the technology essential for the geophysical exploration of coalbed methane(CBM).This acoustic response depends on water(Sw)and gas(Sg)saturation among other factors.In this study,we performed acoustic tests on dry and different gas-water saturated coal samples with different degrees of metamorphism and deformation,collected from several coal mining areas in China.These tests enabled us to analyze the influence of coal type and gas-water saturation on the acoustic response of CBM formations.Our results show that the acoustic velocity of P-wave and S-wave(Vp and Vs,respectively),and the relative anisotropy of and Vs,increased with increasing vitrinite reflectance,density,Vp and Sw.WithSw increasing from 0 to 100%,the growth rate of the acoustic velocity decreased with increasing vitrinite reflectance.The Vp/Vs ratio of tectonic coal was generally higher than that of primary coal.The growth rate of the relative anisotropy in tectonic coal was markedly higher than that in primary coal.

Formation and distribution of coal measure source rocks in the Eocene Pinghu Formation in the Pinghu Slope of the Xihu Depression,East China Sea Shelf Basin

The Xihu Depression in the East China Sea Shelf Basin is a large petroliferous sedimentary depression,in which oil and gas reservoirs were mainly discovered in the Pinghu Slope and the central inversion zone.The oil-gas source correlation in the Xihu Depression was analyzed by hydrocarbon generating thermal simulation data via gold-tube pyrolysis experiments.The results indicated that the oil and gas in the Xihu Depression were mainly derived from coal measure source rocks of the Eocene Pinghu Formation.Therefore,the identification of coal seams is extremely crucial for evaluating coal measure source rocks in the Pinghu Formation in the Xihu Depression.Geochemical and petrological characterization pointed to input of terrigenous organic matter and redox conditions of the depositional environment as factors that govern the ability of the coal measure source rocks in hydrocarbon generation in the Xihu Depression.In this regard,the sedimentary organic facies in the Pinghu Formation were classified into four predominantly terrigenous and one mixed-source subfacies,which all varied in carbon and hydrogen content.The coal measure source rocks in the carbon-and hydrogen-rich tidal flat-lagoon exhibited the highest hydrocarbon generation potential,whereas the mudstone in the neritic facies was the poorest in its hydrocarbon yield.These results suggested that the coal measure source rocks in the Pinghu Formation likely developed in the Hangzhou Slope and the Tiantai Slope,both representing promising sources for oil and gas exploration.

Coal–rock interface detection on the basis of image texture features

Based on the stability and inequality of texture features between coal and rock,this study used the digital image analysis technique to propose a coal–rock interface detection method.By using gray level co-occurrence matrix,twenty-two texture features were extracted from the images of coal and rock.Data dimension of the feature space reduced to four by feature selection,which was according to a separability criterion based on inter-class mean difference and within-class scatter.The experimental results show that the optimized features were effective in improving the separability of the samples and reducing the time complexity of the algorithm.In the optimized low-dimensional feature space,the coal–rock classifer was set up using the fsher discriminant method.Using the 10-fold cross-validation technique,the performance of the classifer was evaluated,and an average recognition rate of 94.12%was obtained.The results of comparative experiments show that the identifcation performance of the proposed method was superior to the texture description method based on gray histogram and gradient histogram.

Creep characteristics of coal and rock investigated by nanoindentation

In coal mining industry,with the depth growing of coal mines,the creep behaviours of coal and rock can extensively affect the mining safety,coalbed methane recovery and geo-sequestration.To acquire a better insight into their creep characteristics,an efficient and robust researching technique,nanoindentation,was applied to investigate the creep performances of coal and rock samples obtained from two coal mines in the east of China.Creep characteristics were reflected by evaluating the curves of creep depth versus creep time of nanoindentation tests during the load-holding period at the peak load of 30 mN.These curves can be divided into two stages:transient stage and steady stage;and the time of load-holding period of 5 s,which is the dividing point between two stages,can efficiently avoid the influence of creep displacement on the unloading curves.The exponential function can perfectly fit creep curves and Kelvin model can be used to calculate the rheological parameters of coal and rock samples.Calculated results yield values for the creep modulus and viscosity terms of coal and rock.This study also settled a particular emphasis on the selection of the positions of indentations to obtain the rheological properties of mineralogical constituents in heterogonous coal and rock samples and their elastic aftereffect.

Features of infrared thermal image and radiation temperature of coal rocks loaded

Experimental study discovered that: (i) coal rocks and sandstone in the course of loading have three types of infrared thermal image features and three types of infrared radiation temperature features; (ii) infrared detection is comparable with acoustic emission detection and electrical resistance detection. Generally, the infrared forewarning of coal rocks’ failure comes later than that of acoustic and electrical resistance, but the infrared radiation temperature forewarning of coal burst comes earlier. On the basis of comprehensive study and analysis, it was suggested that stress nearby 0.79 σ c should be taken as the stress-caution-zone for rock mass failure, ground pressure and its disasters monitoring.

Experimental and theoretical investigation on mechanisms performance of the rock-coal-bolt(RCB)composite system

For coal mines,rock,coal,and rock bolt are the critical constituent materials for surrounding rock in the underground engineering.The stability of the“rock-coal-bolt”(RCB)composite system is affected by the structure and fracture of the coal-rock mass.More rock bolts installed on the rock,more complex condition of the engineering stress environment will be(tensile-shear composite stress is principal).In this paper,experimental analysis and theoretical verification were performed on the RCB composite system with different angles.The results revealed that the failure of the rock-coal(RC)composite specimen was caused by tensile and shear cracks.After anchoring,the reinforcement body formed inside the composite system limits the area where the crack could occur in the specimen.Specifically,shearing damage occurred only around the bolt,and the stress-strain curve presented a better post-peak mechanical property.The mechanical mechanism of the bolt under the combined action of tension and shear stress was analyzed.Additionally,a rock-coal-bolt tensile-shear mechanical(RCBTSM)model was established.The relationship(similar to the exponential function)between the bolt tensile-shear stress and the angle was obtained.Moreover,the influences of the dilatancy angle and bolt diameter of the RCB composite system were also considered and analyzed.Most of the bolts are subjected to the tensile-shearing action in the post-peak stage.The implications of these results for engineering practice indicated that the bolts of the RCB composite system should be prevented from entering the limit shearing state early.

Effects of water intrusion and loading rate on mechanical properties of and crack propagation in coal–rock combinations

Tackling the problems of underground water storage in collieries in arid regions requires knowledge of the effect of water intrusion and loading rate on the mechanical properties of and crack development in coal–rock combinations. Fifty-four coal–rock combinations were prepared and split equally into groups containing different moisture contents(dry, natural moisture and saturated) to conduct acoustic emission testing under uniaxial compression with loading rates ranging from 0.1 mm/min to 0.6 mm/min. The results show that the peak stress and strength-softening modulus, elastic modulus, strain-softening modulus, and post-peak modulus partly decrease with increasing moisture content and loading rate. In contrast, peak strain increases with increasing moisture content and fluctuates with rising loading rate. More significantly, the relationship between stiffness and stress, combined with accumulated counts of acoustic emission, can be used to precisely predict all phases of crack propagation. This is helpful in studying the impact of moisture content and loading rate on crack propagation and accurately calculating mechanical properties. We also determined that the stress thresholds of crack closure, crack initiation, and crack damage do not vary with changes of moisture content and loading rate, constituting 15.22%, 32.20%, and 80.98% of peak stress, respectively. These outcomes assist in developing approaches to water storage in coal mines, determining the necessary width of waterproof coal–rock pillars, and methods of supporting water-enriched roadways, while also advances understanding the mechanical properties of coal–rock combinations and laws of crack propagation.

STUDY ON THE COAL-ROCK INTERFACE RECOGNITION METHOD BASED ON MULTI-SENSOR DATA FUSION TECHNIQUE

The coal-rock interface recognition method based on multi-sensor data fusiontechnique is put forward because of the localization of single type sensor recognition method. Themeasuring theory based on multi-sensor data fusion technique is analyzed, and hereby the testplatform of recognition system is manufactured. The advantage of data fusion with the fuzzy neuralnetwork (FNN) technique has been probed. The two-level FNN is constructed and data fusion is carriedout. The experiments show that in various conditions the method can always acquire a much higherrecognition rate than normal ones.

Energy dissipation of coal and rock during damage and failure process based on EMR

The physical and mechanical change processes of coal and rock are closely related to energy transformation,and the destruction and failure of coal and rock is an instability phenomena driven by energy change.However,the energy change of large-scale coal rock in the mine site is hardly calculated accurately,making it difficult to monitor coal-rock systematic failure and collapse from the perspective of energy.By the energy dissipation EMR monitoring system,we studied the damage and failure of coal and rock with bursting liability from the energy dissipation point using the geophysical method-EMR,and explored the energy dissipation characteristics during uniaxial compression and their main influencing factors.The results show that under displacement-control loading mode,there are 2 types of energy dissipation trends for both coal and rock with bursting liability.The type Ⅰ trend is a steady increase one during the whole process,therein,the energy dissipation of rock samples is accelerated at the peak load.The type Ⅱ trend energy is a W-shaped fluctuating one containing 6 stages.Under load-control loading mode,there is one energy dissipation trend of shock downward-steady rise.Besides that,rock samples also present a trend of 4 stages.The energy dissipation characteristics of coal and rockduring loading failure process can be used as effective criteria to assess whether they are in a stable or destructive stage.The factors influencing energy dissipation in the loading failure process of coal and rock mainly include strength,homogeneity,and energy input efficiency.

The study of acoustic emission (AE) forecasting coal and rock disaster technique

Introduced the coal and rock AE propagation rule,wave guide fixing technics onAE sensors,and AE forecasting coal and rock disaster on the scene and so on,The coaland rock AE propagation rule that follows the exponent attenuation function on different AEfrequencies,different quality factors and different propagation distances were analyzedand deduced by theory,numerical simulation,and by actual experiment.Consequently,itwas deduced that the coal and rock AE propagation rule follows the exponent attenuationfunction.Based on the correlative theory of wave dynamics and AE sensor,the AE waveguide propagation mechanical model on the sensor fixing manner is found,and the relationsof displacement and speed and acceleration between the AE signal source and theAE signal receiving terminal are presented.The effect of the AE sensor fixing manners oncoal and rock surfaces,coal and rock bottoms and wave guides were studied by actualexperiment.For the results,the effect of the AE sensor fixing manner on wave guides isbetter than on coal and rock surfaces,and was equivalent to the fixing manner on coal androck bottoms.Based on the above study results,actual coal and rock dynamistic disasterswere successfully forecasted.

Deformation analysis of transversely isotropic coal-rock mass with porous and cracks

Coal-rock as a typical sedimentary rock has obvious stratification,namely it has transversely isotropic feature.Meanwhile,deformation leads to coal-rock mass having the characteristics of different porous and crack structures as well as local anisotropy.Equivalent axial and circumferential strain' formulas of the pure coal-rock mass specimen with a single crack were derived through the establishment of equivalent mechanical model of standard cylindrical coal-rock specimen,and have been widely used to a variety of media combined different structures containing multiple cracks.The complete stress strain curve of a real coal-rock specimen was obtained by the CTC test.Additionally,according to the comparison with the theoretical value,the theoretical mechanical model could well explain the deformation characteristics of coal-rock mass and verify its validity.Further,following features were analyzed:strain normalized coefficient and elastic modulus(Poisson's ratio) in vertical and parallel direction to the stratification,stratification angle,porosity,pore radius,normal and tangential stiffness of crack,and the relationship of different crack width with different tangential stiffness of crack.Through the analysis above,it substantiate this claim that the theoretical model with better reliability reflects the transversely isotropic nature of the coal-rock and the local anisotropy caused by the porous and cracks.

Correlation of electromagnetic radiation emitted from coal or rock to supporting resistance

More accurate forecasting of rock burst might be possible from observations of electromagnetic radiation emitted in the mine.We analyzed experimental observations and field data from the Muchengjian coal mine to study the relationship between electromagnetic radiation signal intensity and stress during the fracturing of coal, or rock, and samples under load.The results show that the signal intensity is positively correlated with stress.In addition, we investigated the change in the electromagnetic radiation intensity, the supporting resistance in a real coal mine environment, and the coal or rock stress in the mining area.The data analysis indicates that:1) electromagnetic radiation intensity can accurately reflect the distribution of stress in the mining area;and, 2) there is a correlation between electromagnetic radiation intensity and supporting resistance.The research has some practical guiding significance for rock burst forecasting and for the prevention of accidents in coal mines.

Similarity model tests of movement and deformation of coal-rock mass below stopes

For a study of the movement and deformation of coal-rock mass and low protected seams below a stope,as well as for fracture developments and rules of evolution of permeability,we designed a plane strain model test stand to carry out model tests of similar materials in order to improve the effect of gas drainage from low protected seams and to measure the movement and deformation of coal-rock mass using a method of non-contact close-range photogrammetry.Our results show that 1) using paraffin melting to take the place of coal seam mining can satisfy the mining conditions of a protective seam;2) coal-rock mass under goafs has an upward movement after the protective seam has been mined,causing floor heaving;3) low protected seams become swollen and deformed,providing a good pressure-relief effect and causing the coal-rock mass under both sides of coal pillars to become deformed by compression and 4) the evolution of permeability of low protected seams follows the way of initial values→a slight decrease→a great increase→stability→final decrease.Simultaneously,the coefficient of air permeability increased at a decreasing rate with an increase in interlayer spacing.