We present a coaxial detection of the backscattered electrons in SEM. The lens-aperture has been used to filter in energy and focus the backscattered electrons. This particular geometry allows us to eliminate the low ...We present a coaxial detection of the backscattered electrons in SEM. The lens-aperture has been used to filter in energy and focus the backscattered electrons. This particular geometry allows us to eliminate the low energy backscattered electrons and collect the backscattered electrons, which are backscattered close to the incident beam orientation. The main advantage of this geometry is adapted to topographic contrast attenuation and atomic number contrast enhancement. Thus this new SEM is very suitable to analyze the material composition.展开更多
A novel electromagnetic induction detector with two inductors for CE was described here.The two inductors were used as signal detection and reference,respectively.The parameters affecting the detector performance（inc...A novel electromagnetic induction detector with two inductors for CE was described here.The two inductors were used as signal detection and reference,respectively.The parameters affecting the detector performance（including coil turns,detection distance, excitation frequency,voltage,etc.） were optimized.Under the optimum condition,the feasibility of the detector was examined by analyzing inorganic ions.The fabricated detector showed good linear relationship between the response and the analytes concentrations,with a detection limit of 13μmol/L for Na~＋（S/N = 3）.A variety of advantages,such as simple construction, ease of operation,and considerably universal response,suggested this novel detector a promising application prospect in analytical area.展开更多
基金the National Natural Science Foundation of China!10045001
文摘We present a coaxial detection of the backscattered electrons in SEM. The lens-aperture has been used to filter in energy and focus the backscattered electrons. This particular geometry allows us to eliminate the low energy backscattered electrons and collect the backscattered electrons, which are backscattered close to the incident beam orientation. The main advantage of this geometry is adapted to topographic contrast attenuation and atomic number contrast enhancement. Thus this new SEM is very suitable to analyze the material composition.
基金support from the National Natural Science Foundation of China(Nos20727006 and 21075139)
文摘A novel electromagnetic induction detector with two inductors for CE was described here.The two inductors were used as signal detection and reference,respectively.The parameters affecting the detector performance（including coil turns,detection distance, excitation frequency,voltage,etc.） were optimized.Under the optimum condition,the feasibility of the detector was examined by analyzing inorganic ions.The fabricated detector showed good linear relationship between the response and the analytes concentrations,with a detection limit of 13μmol/L for Na~＋（S/N = 3）.A variety of advantages,such as simple construction, ease of operation,and considerably universal response,suggested this novel detector a promising application prospect in analytical area.
