Isothermal hot compression tests of as-cast high-Cr ultra-super-critical(USC) rotor steel with columnar grains perpendicular to the compression direction were carried out in the temperature range from 950 to 1250...Isothermal hot compression tests of as-cast high-Cr ultra-super-critical(USC) rotor steel with columnar grains perpendicular to the compression direction were carried out in the temperature range from 950 to 1250°C at strain rates ranging from 0.001 to 1 s^(-1). The softening mechanism was dynamic recovery(DRV) at 950°C and the strain rate of 1 s^(-1), whereas it was dynamic recrystallization(DRX) under the other conditions. A modified constitutive equation based on the Arrhenius model with strain compensation reasonably predicted the flow stress under various deformation conditions, and the activation energy was calculated to be 643.92 kJ ×mol^(-1). The critical stresses of dynamic recrystallization under different conditions were determined from the work-hardening rate(θ)–flow stress(σ) and-θ/σ–σ curves. The optimum processing parameters via analysis of the processing map and the softening mechanism were determined to be a deformation temperature range from 1100 to 1200°C and a strain-rate range from 0.001 to 0.08 s^(-1), with a power dissipation efficiency η greater than 31%.展开更多
The hot compressive deformation behavior of hot isostatically pressed Ti-47.5Al-2Cr-2Nb-0.2W-0.2B alloy using gas atomization powders was systematically investigated and the processing map was obtained in the temperat...The hot compressive deformation behavior of hot isostatically pressed Ti-47.5Al-2Cr-2Nb-0.2W-0.2B alloy using gas atomization powders was systematically investigated and the processing map was obtained in the temperature range of 1323-1473 Kand strain rate range of 0.001-0.5s^(-1).The calculated activation energy in the above variational ranges of temperature and strain rate possesses a low activation energy value of approximately 365.6kJ/mol based on the constitutive relationship models developed with the Arrhenius-type constitutive model respectively considering the strain rate and deformation temperature.The hot working flow behavior during the deformation process was analyzed combined with the microstructural evolution.Meanwhile,the processing maps during the deformation process were established based on the dynamic material model and Prasad instability criterion under different deformation conditions.Finally,the optimal hot processing window of this alloy corresponding to the wide temperature range of 1353-1453 Kand the low strain rate of 0.001-0.1s^(-1) was obtained.展开更多
The flow behavior of delta-processed Inconel 718 was studied in temperature range of 900-1 060℃ and strain rate range of 0.001-0.5s-1.The effects of friction and temperature on the compressive deformation behavior we...The flow behavior of delta-processed Inconel 718 was studied in temperature range of 900-1 060℃ and strain rate range of 0.001-0.5s-1.The effects of friction and temperature on the compressive deformation behavior were investigated,and the flow stress-strain error caused by friction was revised.The results showed that the effect of the friction was obvious with increasing strain rate and decreasing deformation temperature.The revised flow stress is decreased by increasing temperature and decreasing strain rate and exhibits a typical dynamic recrystallization behavior.The constitutive model has been developed through a hyperbolic-sine Arrhenius type equation to relate the flow stress,strain rate and temperature.The influence of strain has also been incorporated by considering the variation of material constants as a function of strain.The prediction accuracy of developed constitutive model has been assessed using standard statistical formulae.According to the analysis results,the proposed deformation constitutive equation gives an accurate and precise estimate of flow stress of delta-processed Inconel 718 alloy.展开更多
The high-temperature deformation behavior of a beta Ti-3.0 Al-3.5 Cr-2.0 Fe-0.1 B alloy was investigated by a Gleeble-1500 D thermal simulator. The height reduction was 50%, corresponding to a true strain of 0.693. Th...The high-temperature deformation behavior of a beta Ti-3.0 Al-3.5 Cr-2.0 Fe-0.1 B alloy was investigated by a Gleeble-1500 D thermal simulator. The height reduction was 50%, corresponding to a true strain of 0.693. The strain rate ranging from 0.01 to 10.00 s^-1 and the deformation temperature ranging from 800 to 950 ℃ were considered.The flow stress and the apparent activation energy for deformation, along with the constitutive equation, were used to analyze the behavior of the Ti-3.0 Al-3.5 Cr-2.0 Fe-0.1 B alloy. The processing map was established. The effect of strain rate on the microstructure at 850 ℃ was evaluated.The flow stress-strain curves indicated that the peak flow stresses increased along with an increase in the strain rate and decreased as the deformation temperature increased.Based on the true stress-true strain curves, the constitutive equation was established and followed as the ε= 6.58×10-(10)[sinh(0.0113σ)]-(3.44)exp(-245481.3/RT). The processing map exhibited the "unsafe" region at the strain rate of10 s^-1 and the temperature of 850 ℃,and the rest region was "safe". The deformation microstructure demonstrated that both dynamic recovery(DRV) and dynamic recrystallization(DRX) existed during deformation. At the lower strain rate of 0.01 s^-1, the main deformation mechanism was the DRV, and the DRX was the dominant deformation mechanism at the higher strain rate of 1.00 s^-1.展开更多
Hot deformation behavior of an as-extruded duplex structured Mg-9Li-3Al-2.5Sr alloy is investigated via hot compression tests conducted at 200-350℃ with strain rate of 0.001-1 s^-1.The flow behavior of Mg-9Li-3Al-2.5...Hot deformation behavior of an as-extruded duplex structured Mg-9Li-3Al-2.5Sr alloy is investigated via hot compression tests conducted at 200-350℃ with strain rate of 0.001-1 s^-1.The flow behavior of Mg-9Li-3Al-2.5Sr alloy can be described accurately by hyperbolic sine constitutive equation and the average activation energy for deformation is calculated as 143.5 k J/mol.Based on a dynamic materials model,the processing maps of Mg-9Li-3Al-2.5Sr alloy which describe the variation of power dissipation efficiency are constructed as a function of temperature and strain rate.The processing maps exhibit an area of discontinuous dynamic recrystallization occurring at 280-300℃ with strain rate of 0.001-0.01 s^-1,which corresponds to the optimum hot working conditions.展开更多
In order to optimize the deformation processing, the hot deformation behavior of Co-Cr-Mo-Cu (here- after named as Co-Cu) alloy was studied in this paper at a deformation temperature range of 950-1150 ℃ and a strai...In order to optimize the deformation processing, the hot deformation behavior of Co-Cr-Mo-Cu (here- after named as Co-Cu) alloy was studied in this paper at a deformation temperature range of 950-1150 ℃ and a strain rate range of 0.008-5 s^-1. Based on the true stress-true strain curves, a constitutive equation in hyperbolic sin function was established and a hot processing map was drawn. It was found that the flow stress of the Co-Cu alloy increased with the increase of the strain rate and decreased with the increase of the deforming temperature. The hot processing map indicated that there were two unstable regions and one well-processing region. The microstructure, the hardness distribution and the electro- chemical properties of the hot deformed sample were investigated in order to reveal the influence of the hot deformation. Microstructure observation indicated that the grain size increased with the increase of the deformation temperature but decreased with the increase of the strain rate. High temperature and low strain rate promoted the crystallization process but increased the grain size, which results in a reduction in the hardness. The hot deformation at high temperature (1100-1150 ℃) would reduce the corrosion resistance slightly. The final optimized deformation process was: a deformation temperature from 1050to 1100 ℃, and a strain rate from 0.008 to 0.2 s^-1, where a completely recrystallized and homogeneously distributed microstructure would be obtained.展开更多
Isothermal hot compression tests on the as-cast high-Cr ultra-super-critical rotor steel with columnar grains were carried out in the temperature range from 1223 to 1523Kand at strain rates from 0.001 to 1s^(-1).The...Isothermal hot compression tests on the as-cast high-Cr ultra-super-critical rotor steel with columnar grains were carried out in the temperature range from 1223 to 1523Kand at strain rates from 0.001 to 1s^(-1).The compression direction was parallel to the longitudinal direction of columnar grains.The constitutive equation based on Arrhenius model was presented,and the processing maps based on the dynamic material model were developed,correlating with microstructure observation.The main softening mechanism was dynamic recovery at 1223 Kunder strain rates from 0.1to 1s^(-1),whereas it was dynamic recrystallization under other deformation conditions.The constitutive equation modified by strain compensation reasonably predicted the flow stresses.The processing maps and microstructure evolution mechanism schematic indicated that the optimum hot working parameters lay in the zone defined by the temperature range from 1423 to 1473Kand the strain rate range from 0.001 to 1s^(-1).展开更多
MicroRNAs(miRNAs)constitute a class of small non-coding RNAs that participate in various biological processes by repressing protein translation or destabilizing target mRNAs.miRNA biogenesis begins with the transcri...MicroRNAs(miRNAs)constitute a class of small non-coding RNAs that participate in various biological processes by repressing protein translation or destabilizing target mRNAs.miRNA biogenesis begins with the transcription of primary miRNAs(pri-miRNAs)in the cell nucleus,which are then cleaved by the Drosha/DGCR complex into precursor miRNAs(pre-miRNAs).The pre-miRNAs are transported by exportin-5(XPO5)from the nucleus to the cytoplasm,展开更多
基金supported by the Major State Basic Research Development Program of China (No.2011CB012900)the National Natural Science Foundation of China (No.51374144)the Shanghai Rising-Star Program (No.14QA1402300)
文摘Isothermal hot compression tests of as-cast high-Cr ultra-super-critical(USC) rotor steel with columnar grains perpendicular to the compression direction were carried out in the temperature range from 950 to 1250°C at strain rates ranging from 0.001 to 1 s^(-1). The softening mechanism was dynamic recovery(DRV) at 950°C and the strain rate of 1 s^(-1), whereas it was dynamic recrystallization(DRX) under the other conditions. A modified constitutive equation based on the Arrhenius model with strain compensation reasonably predicted the flow stress under various deformation conditions, and the activation energy was calculated to be 643.92 kJ ×mol^(-1). The critical stresses of dynamic recrystallization under different conditions were determined from the work-hardening rate(θ)–flow stress(σ) and-θ/σ–σ curves. The optimum processing parameters via analysis of the processing map and the softening mechanism were determined to be a deformation temperature range from 1100 to 1200°C and a strain-rate range from 0.001 to 0.08 s^(-1), with a power dissipation efficiency η greater than 31%.
基金the financial supports from the National Natural Science Foundation of China(Grant Nos.51301157 and 51434007)the National High Technology Research and Development Program of China 863 Program(Grant No.2013AA031103)
文摘The hot compressive deformation behavior of hot isostatically pressed Ti-47.5Al-2Cr-2Nb-0.2W-0.2B alloy using gas atomization powders was systematically investigated and the processing map was obtained in the temperature range of 1323-1473 Kand strain rate range of 0.001-0.5s^(-1).The calculated activation energy in the above variational ranges of temperature and strain rate possesses a low activation energy value of approximately 365.6kJ/mol based on the constitutive relationship models developed with the Arrhenius-type constitutive model respectively considering the strain rate and deformation temperature.The hot working flow behavior during the deformation process was analyzed combined with the microstructural evolution.Meanwhile,the processing maps during the deformation process were established based on the dynamic material model and Prasad instability criterion under different deformation conditions.Finally,the optimal hot processing window of this alloy corresponding to the wide temperature range of 1353-1453 Kand the low strain rate of 0.001-0.1s^(-1) was obtained.
基金Sponsored by National High Technology Research and Development Program of China(2012AA03A514)Youth Scientific Research Foundation of Central South University of Forestry and Technology of China(QJ2010001A)
文摘The flow behavior of delta-processed Inconel 718 was studied in temperature range of 900-1 060℃ and strain rate range of 0.001-0.5s-1.The effects of friction and temperature on the compressive deformation behavior were investigated,and the flow stress-strain error caused by friction was revised.The results showed that the effect of the friction was obvious with increasing strain rate and decreasing deformation temperature.The revised flow stress is decreased by increasing temperature and decreasing strain rate and exhibits a typical dynamic recrystallization behavior.The constitutive model has been developed through a hyperbolic-sine Arrhenius type equation to relate the flow stress,strain rate and temperature.The influence of strain has also been incorporated by considering the variation of material constants as a function of strain.The prediction accuracy of developed constitutive model has been assessed using standard statistical formulae.According to the analysis results,the proposed deformation constitutive equation gives an accurate and precise estimate of flow stress of delta-processed Inconel 718 alloy.
基金financially supported by the.National Natural Science Foundation of China (No.51401027)the China Postdoctoral Science Foundation Funded Project (No.2016M591040)
文摘The high-temperature deformation behavior of a beta Ti-3.0 Al-3.5 Cr-2.0 Fe-0.1 B alloy was investigated by a Gleeble-1500 D thermal simulator. The height reduction was 50%, corresponding to a true strain of 0.693. The strain rate ranging from 0.01 to 10.00 s^-1 and the deformation temperature ranging from 800 to 950 ℃ were considered.The flow stress and the apparent activation energy for deformation, along with the constitutive equation, were used to analyze the behavior of the Ti-3.0 Al-3.5 Cr-2.0 Fe-0.1 B alloy. The processing map was established. The effect of strain rate on the microstructure at 850 ℃ was evaluated.The flow stress-strain curves indicated that the peak flow stresses increased along with an increase in the strain rate and decreased as the deformation temperature increased.Based on the true stress-true strain curves, the constitutive equation was established and followed as the ε= 6.58×10-(10)[sinh(0.0113σ)]-(3.44)exp(-245481.3/RT). The processing map exhibited the "unsafe" region at the strain rate of10 s^-1 and the temperature of 850 ℃,and the rest region was "safe". The deformation microstructure demonstrated that both dynamic recovery(DRV) and dynamic recrystallization(DRX) existed during deformation. At the lower strain rate of 0.01 s^-1, the main deformation mechanism was the DRV, and the DRX was the dominant deformation mechanism at the higher strain rate of 1.00 s^-1.
基金the financial support from the National Natural Science Foundation(Project No.51601024)the National Key Research and Development plan(Project No.2016YFB0700403)+1 种基金the Chongqing Research Program of Basic Research and Frontier Technology(Project No.cstc2016jcyj A0418)the Fundamental Research Funds for the Central Universities(Project No.106112015CDJXY130011 and No.CDJZR14130007)
文摘Hot deformation behavior of an as-extruded duplex structured Mg-9Li-3Al-2.5Sr alloy is investigated via hot compression tests conducted at 200-350℃ with strain rate of 0.001-1 s^-1.The flow behavior of Mg-9Li-3Al-2.5Sr alloy can be described accurately by hyperbolic sine constitutive equation and the average activation energy for deformation is calculated as 143.5 k J/mol.Based on a dynamic materials model,the processing maps of Mg-9Li-3Al-2.5Sr alloy which describe the variation of power dissipation efficiency are constructed as a function of temperature and strain rate.The processing maps exhibit an area of discontinuous dynamic recrystallization occurring at 280-300℃ with strain rate of 0.001-0.01 s^-1,which corresponds to the optimum hot working conditions.
基金financially supported by the National Natural Science Foundation of China (Nos. 81071262, 31271024 and 31470930)the Funding from Northeastern University ("985 program", Nos. N141008001 and LZ2014018), China
文摘In order to optimize the deformation processing, the hot deformation behavior of Co-Cr-Mo-Cu (here- after named as Co-Cu) alloy was studied in this paper at a deformation temperature range of 950-1150 ℃ and a strain rate range of 0.008-5 s^-1. Based on the true stress-true strain curves, a constitutive equation in hyperbolic sin function was established and a hot processing map was drawn. It was found that the flow stress of the Co-Cu alloy increased with the increase of the strain rate and decreased with the increase of the deforming temperature. The hot processing map indicated that there were two unstable regions and one well-processing region. The microstructure, the hardness distribution and the electro- chemical properties of the hot deformed sample were investigated in order to reveal the influence of the hot deformation. Microstructure observation indicated that the grain size increased with the increase of the deformation temperature but decreased with the increase of the strain rate. High temperature and low strain rate promoted the crystallization process but increased the grain size, which results in a reduction in the hardness. The hot deformation at high temperature (1100-1150 ℃) would reduce the corrosion resistance slightly. The final optimized deformation process was: a deformation temperature from 1050to 1100 ℃, and a strain rate from 0.008 to 0.2 s^-1, where a completely recrystallized and homogeneously distributed microstructure would be obtained.
基金sponsored by Major State Basic Research Development Program of China(No.2011CB012900)National Natural Science Foundation of China(No.51374144)
文摘Isothermal hot compression tests on the as-cast high-Cr ultra-super-critical rotor steel with columnar grains were carried out in the temperature range from 1223 to 1523Kand at strain rates from 0.001 to 1s^(-1).The compression direction was parallel to the longitudinal direction of columnar grains.The constitutive equation based on Arrhenius model was presented,and the processing maps based on the dynamic material model were developed,correlating with microstructure observation.The main softening mechanism was dynamic recovery at 1223 Kunder strain rates from 0.1to 1s^(-1),whereas it was dynamic recrystallization under other deformation conditions.The constitutive equation modified by strain compensation reasonably predicted the flow stresses.The processing maps and microstructure evolution mechanism schematic indicated that the optimum hot working parameters lay in the zone defined by the temperature range from 1423 to 1473Kand the strain rate range from 0.001 to 1s^(-1).
文摘MicroRNAs(miRNAs)constitute a class of small non-coding RNAs that participate in various biological processes by repressing protein translation or destabilizing target mRNAs.miRNA biogenesis begins with the transcription of primary miRNAs(pri-miRNAs)in the cell nucleus,which are then cleaved by the Drosha/DGCR complex into precursor miRNAs(pre-miRNAs).The pre-miRNAs are transported by exportin-5(XPO5)from the nucleus to the cytoplasm,