The aim of this work was to study the influence of the processing route on the microstructural constituents,hardness andtribological(wear and friction)behavior of Ti6Al4V biomedical alloy.In this sense,three different...The aim of this work was to study the influence of the processing route on the microstructural constituents,hardness andtribological(wear and friction)behavior of Ti6Al4V biomedical alloy.In this sense,three different processing routes were studied:conventional casting,hot pressing and selective laser melting.A comprehensive metallurgical,mechanical and tribologicalcharacterization was performed by X-ray diffraction analysis,Vickers hardness tests and reciprocating ball-on-plate wear tests ofTi6Al4V/Al2O3sliding pairs.The results showed a great influence of the processing route on the microstructural constituents andconsequent differences on hardness and wear performance.The highest hardness and wear resistance were obtained for Ti6Al4Valloy produced by selective laser melting,due to a markedly different cooling rate that leads to significantly different microstructurewhen compared to hot pressing and casting.This study assesses and confirms that selective laser melting is potential to producecustomized Ti6Al4V implants with improved wear performance.展开更多
Aluminum silicon alloy of composition (Al-25%Si-3%Ni-1%Fe-2%Cu) was atomized using water atomization. The powders were cold compacted in a die to produce green cylinder compacts. Four consolidation processes were appl...Aluminum silicon alloy of composition (Al-25%Si-3%Ni-1%Fe-2%Cu) was atomized using water atomization. The powders were cold compacted in a die to produce green cylinder compacts. Four consolidation processes were applied, namely;conventional sintering at 500℃, sintering followed by hot forging to obtain pistons, one step hot forging into pistons, and hot pressing. The microstructure of the sintered specimens showed inter-granular pores and oxide layers on particle interfaces of 84% relative density. When the sintered specimens were hot forged, both the inter-granular pores and oxide layers on particle interfaces almost disappeared and the relative densities increased up to about 95%. The same microstructure is also obtained for the one step forged specimens, but the relative densities increased to about 97%. However, the hot pressing specimens showed the presence of oxide layers on particle surfaces as well as few isolated pores. The relative density of the hot pressed specimens was about 90%. Hardness and ultimate compression strength were measured. It is noted that the strongest bulk materials are those made by hot forging, followed by those made by hot pressing and the weakest bulk materials are those made by conventional sintering.展开更多
Gas injection is the second largest enhanced oil recovery process, next only to the thermal method used in heavy oil fields. To increase the extent of the reservoir contacted by the injected gas, the gas is generally ...Gas injection is the second largest enhanced oil recovery process, next only to the thermal method used in heavy oil fields. To increase the extent of the reservoir contacted by the injected gas, the gas is generally injected intermittently with water. This mode of injection is called water-alternating-gas (WAG). This study deals with a new immiscible water alternating gas (IWAG) EOR technique, “hot IWAG” which includes combination of thermal, solvent and sweep techniques. In the proposed method CO2 will be superheated above the reservoir temperature and instead of normal temperature water, hot water will be used. Hot CO2 and hot water will be alternatively injected into the sand packs. A laboratory test was conducted on the fractured and conventional sand packs. Slugs of water and CO2 with a low and constant rate were injected into the sand packs alternatively; slug size was 0.05 PV. Recovery from each sand pack was monitored and after that hot water and hot CO2 were injected alternatively under the same conditions and increased oil recovery from each sand pack and breakthrough were measured. Experimental results showed that the injection of hot WAG could significantly recover residual oil after WAG injection in conventional and fractured sand packs.展开更多
粉末近净成形(Powder metallurgy near net shaping,PM-NNS)技术能够制备出具有优异综合力学性能的粉末合金复杂部件。介绍了粉末热等静压(Hot isostatic pressing,HIP)近净成形技术原理及优势,综述了近年来国内外粉末近净成形在航天发...粉末近净成形(Powder metallurgy near net shaping,PM-NNS)技术能够制备出具有优异综合力学性能的粉末合金复杂部件。介绍了粉末热等静压(Hot isostatic pressing,HIP)近净成形技术原理及优势,综述了近年来国内外粉末近净成形在航天发动机领域的研究现状,从工艺路线和构件研制两方面展开,简述了构件制备过程的影响因素及缺陷控制,结合中国科学院金属研究所粉末近净成形技术在航天发动机领域的研究及应用情况,总结了粉末近净成形技术当前存在的主要问题及发展方向,以期进一步拓宽该技术的应用范围。展开更多
基金supported by FTC through the projects PTDC/EMS-TEC/5422/2014 and EXCL/EMS-TEC/ 0460/2012the grant SFRH/BPD/112111/2015+1 种基金supported by FCT with the reference project UID/EEA/04436/2013by FEDER funds through the COMPETE 2020-Programa Operacional Competitividade e Internacionalizacao (POCI) with the reference project POCI-01-0145FEDER-006941.
文摘The aim of this work was to study the influence of the processing route on the microstructural constituents,hardness andtribological(wear and friction)behavior of Ti6Al4V biomedical alloy.In this sense,three different processing routes were studied:conventional casting,hot pressing and selective laser melting.A comprehensive metallurgical,mechanical and tribologicalcharacterization was performed by X-ray diffraction analysis,Vickers hardness tests and reciprocating ball-on-plate wear tests ofTi6Al4V/Al2O3sliding pairs.The results showed a great influence of the processing route on the microstructural constituents andconsequent differences on hardness and wear performance.The highest hardness and wear resistance were obtained for Ti6Al4Valloy produced by selective laser melting,due to a markedly different cooling rate that leads to significantly different microstructurewhen compared to hot pressing and casting.This study assesses and confirms that selective laser melting is potential to producecustomized Ti6Al4V implants with improved wear performance.
文摘Aluminum silicon alloy of composition (Al-25%Si-3%Ni-1%Fe-2%Cu) was atomized using water atomization. The powders were cold compacted in a die to produce green cylinder compacts. Four consolidation processes were applied, namely;conventional sintering at 500℃, sintering followed by hot forging to obtain pistons, one step hot forging into pistons, and hot pressing. The microstructure of the sintered specimens showed inter-granular pores and oxide layers on particle interfaces of 84% relative density. When the sintered specimens were hot forged, both the inter-granular pores and oxide layers on particle interfaces almost disappeared and the relative densities increased up to about 95%. The same microstructure is also obtained for the one step forged specimens, but the relative densities increased to about 97%. However, the hot pressing specimens showed the presence of oxide layers on particle surfaces as well as few isolated pores. The relative density of the hot pressed specimens was about 90%. Hardness and ultimate compression strength were measured. It is noted that the strongest bulk materials are those made by hot forging, followed by those made by hot pressing and the weakest bulk materials are those made by conventional sintering.
文摘Gas injection is the second largest enhanced oil recovery process, next only to the thermal method used in heavy oil fields. To increase the extent of the reservoir contacted by the injected gas, the gas is generally injected intermittently with water. This mode of injection is called water-alternating-gas (WAG). This study deals with a new immiscible water alternating gas (IWAG) EOR technique, “hot IWAG” which includes combination of thermal, solvent and sweep techniques. In the proposed method CO2 will be superheated above the reservoir temperature and instead of normal temperature water, hot water will be used. Hot CO2 and hot water will be alternatively injected into the sand packs. A laboratory test was conducted on the fractured and conventional sand packs. Slugs of water and CO2 with a low and constant rate were injected into the sand packs alternatively; slug size was 0.05 PV. Recovery from each sand pack was monitored and after that hot water and hot CO2 were injected alternatively under the same conditions and increased oil recovery from each sand pack and breakthrough were measured. Experimental results showed that the injection of hot WAG could significantly recover residual oil after WAG injection in conventional and fractured sand packs.
文摘粉末近净成形(Powder metallurgy near net shaping,PM-NNS)技术能够制备出具有优异综合力学性能的粉末合金复杂部件。介绍了粉末热等静压(Hot isostatic pressing,HIP)近净成形技术原理及优势,综述了近年来国内外粉末近净成形在航天发动机领域的研究现状,从工艺路线和构件研制两方面展开,简述了构件制备过程的影响因素及缺陷控制,结合中国科学院金属研究所粉末近净成形技术在航天发动机领域的研究及应用情况,总结了粉末近净成形技术当前存在的主要问题及发展方向,以期进一步拓宽该技术的应用范围。
