The effects of Pb content on crystallographic phase, microstructure, electric-properties of PMSZT piezoelectric ceramics were studied. The crystallographic phase and microstructure of the ceramics were examined by usi...The effects of Pb content on crystallographic phase, microstructure, electric-properties of PMSZT piezoelectric ceramics were studied. The crystallographic phase and microstructure of the ceramics were examined by using X-ray diffraction (XRD) and scanning electron microscopy (SEM). The experimental result shows that the samples consist of a mixture of tetragonal and rhombohedral phases in the range of lead contents x=0.95-1.06, grains grow up homogeneously and the minimum value of Curie temperature was obtained with x-=1.02. With Pb content x〈l.02 or x〉1.02, the Curie temperature moves towards a high temperature. A well-situated electric-properties of ET33/E0 (1660), d33 (344pC/N), Kp (0.684), Qm (2350),tan 3(0.0030) were obtained when lead content x=1.02.展开更多
基金the National Natural Science Foundation of China (No.10232030)Key Laboratory for Advanced Ceramics and Machining Technology of Ministry of Education(No.x06050)
文摘The effects of Pb content on crystallographic phase, microstructure, electric-properties of PMSZT piezoelectric ceramics were studied. The crystallographic phase and microstructure of the ceramics were examined by using X-ray diffraction (XRD) and scanning electron microscopy (SEM). The experimental result shows that the samples consist of a mixture of tetragonal and rhombohedral phases in the range of lead contents x=0.95-1.06, grains grow up homogeneously and the minimum value of Curie temperature was obtained with x-=1.02. With Pb content x〈l.02 or x〉1.02, the Curie temperature moves towards a high temperature. A well-situated electric-properties of ET33/E0 (1660), d33 (344pC/N), Kp (0.684), Qm (2350),tan 3(0.0030) were obtained when lead content x=1.02.