Early Devonian Post-collisional Granitic Magmatism in the North Qilian Orogenic Belt,Western China:Insights into Lithospheric Delamination and Orogenic Collapse

Post-collisional magmatism contains important clues for understanding the reworking and growth of continental crust,as well as lithospheric delamination and orogenic collapse.Early Devonian magmatism has been identified in the North Qilian Orogenic Belt(NQOB).This paper reports an integrated study of petrology,whole-rock geochemistry,Sm-Nd isotope and zircon U-Pb dating,as well as Lu-Hf isotopic data,for two Early Devonian intrusive plutons.The Yongchang and Chijin granites yield zircon U-Pb ages of 394-407 Ma and 414 Ma,respectively.Both of them are characterized by weakly peraluminous to metaluminous without typical aluminium-rich minerals,LREE-enriched patterns with negative Eu anomalies and a negative correlation between P_(2)O_(5) and SiO_(2) contents,consistent with geochemical features of I-type granitoids.Zircons from the studied granites display negative to weak positive ε_(Hf)(t)values(−5.7 to 2.1),which agree well with those of negative ε_(Nd)(t)values(−6.4 to−2.9)for the whole-rock samples,indicating that they were derived from the partial melting of Mesoproterozoic crust.Furthermore,low Sr/Y ratios(1.13-21.28)and high zircon saturation temperatures(745℃ to 839℃,with the majority being>800℃)demonstrated a relatively shallow depth level below the garnet stability field and an additional heat source.Taken together,the Early Devonian granitic magmatism could have been produced by the partial melting of ancient crustal materials heated by mantle-derived magmas at high-temperature and low-pressure conditions during postcollisional extensional collapse.The data obtained in this study,when viewed in conjunction with previous studies,provides more information about the tectonic processes that followed the closure of the North Qilian Ocean.The tectonic transition from continental collision to post-collisional delamination could be constrained to~430 Ma,which is provided by the sudden decrease of Sr/Y and La/Yb ratios and an increase in zircon ε_(Hf)(t)values for granitoids.A two-stage tectonic evolution model from continental collision to post-collisional extensional collapse for the NQOB includes(a)continental collision and crustal thickening during ca.455-430 Ma,characterized by granulite-facies metamorphism and widespread low-Mg adakitic magmatism;(b)post-collisional delamination of thickened continental crust and extensional collapse of orogen during ca.430-390 Ma,provided by coeval high-Mg adakitic magmatism,A-type granites and I-type granitoids with low Sr-Y ratios.

Low-velocity Impact Damage Analysis of Composite Laminates Using Self-adapting Delamination Element Method

On the basis ofa 2D 4-node Mindlin shell element method, a novel self-adapting delamination finite element method is presented, which is developed to model the delamination damage of composite laminates. In the method, the sublaminate elements are generated automatically when the delamination damage occurs or extends. Thus, the complex process and state of delamination damage can be simulated practically with high efficiency for both analysis and modeling. Based on the self-adapting delamination method, linear dynamic finite element damage analysis is performed to simulate the low-velocity impact damage process of three types of mixed woven composite laminates. Taking the frictional force among sublaminations during delaminating and the transverse normal stress into account, the analytical results are consistent with those of the experimental data.

拆沉作用(delamination)及其壳—幔演化动力学意义

拆沉作用导致下地壳和岩石圈地幔下沉，相应软流圈上涌至壳—幔边界，使下地壳、岩石圈地幔和软流圈三者发生物质交换，引起岩浆作用、山脉隆升、伸展、垮塌，形成坳陷盆地，并最终使大陆地壳向长英质方向演化，产生与其它行星不同的、独一无二的中性安山质或英云闪长质成分。

Effect of bonding interface on delamination behavior of drawn Cu/Al bar clad material

Cu/Al bar clad material was fabricated by a drawing process and a subsequent heat treatment.During these processes,intermetallic compounds have been formed at the interface of Cu/Al and have affected its bonding property.Microstructures of Cu/Al interfaces were observed by OM,SEM and EDX Analyser in order to investigate the bonding properties of the material.According to the microstructure a series of diffusion layers were observed at the interface and the thicknesses of diffusion layers have increased with aging time as a result of the diffusion bonding.The interfaces were composed of 3-ply diffusion layers and their compositions were changed with aging time at 400 °C.These compositional compounds were revealed to be η2,(θ+η2),(α+θ) intermetallic phases.It is evident from V-notch impact tests that the growth of the brittle diffusion layers with the increasing aging time directly influenced delamination distance between the Cu sleeve and the Al core.It is suggested that the proper holding time at 400 °C for aging as post heat treatment of a drawn Cu/Al bar clad material would be within 1 h.

Two-dimensional analyses of delamination buckling of symmetrically cross-ply rectangular laminates

The conventional approach to analysis the buckling of rectangular laminates containing an embedded delamination subjected to the in-plane loading is to simplify the laminate as a beam-plate from which the predicted buckling load decreases as the length of the laminate increases. Two-dimensional analyses are employed in this paper by extending the one-dimensional model to take into consideration of the influence of the delamination width on the buckling performance of the laminates. The laminate is simply supported containing a through width delamination. A new parameterβ defined as the ratio of delamination length to delamination width is introduced with an emphasis on the influence of the delamination size. It is found that （i） when the ratio β is greater than one snap-through buckling prevails, the buckling load is determined by the delamination size and depth only; （ii） as the ratio β continues to increase, the buckling load will approach to a constant value. Solutions are verified with the well established results and are found in good agreement with the latter.

ANALYSIS ON BUCKLING AND POSTBUCKLING OF DELAMINATION IN 3D COMPOSITES

In this paper, the problem of axisymmetric buckling and postbuckling of a circular thin-film delamination bridged by through-thickness fiber tows in 3D composites is presented. An iterative procedure based on Taylor's series expansion is used to generate a family of nondimensionalized postbuckling solutions of the above problem by von Karman's nonlinear plate theory. Attention is focused, herein, on the effects of the bridge force of through-thickness fibers on the buckling and postbuckling behavior of the delamination. It is found that fiber bridge not only increases the ability of resisting delamination buckling and postbuckling, but also brings on the jump of the delamination deflection mode during the postbuckling phase. Consequently the behavior of the composite structure with delamination is greatly improved, such as increasing the residual strength and prolonging the service life.

Vibration of composite beams with two overlapping delaminations

Delaminations in composite laminates may de-velop from small cracks due to fabrication and impact load-ing,or from places of high stress concentration.The locationsof the delaminations are not determinate.In this research,ananalytical solution for the free vibration of a composite beamwith two overlapping delaminations is presented.The dela-minated beam is analyzed as seven interconnected beamsusing the delaminations as their boundaries.The continuityand equilibrium conditions are satisfied between the adjoin-ing regions of the beams.Classical beam theory is applied toeach of the beams.Complex vibration behaviors emerge fordifferent sizes and locations of the delaminations.Compar-ison with analytical results reported in the literature verifiesthe validity of the present solution.

Two-dimensional analysis of progressive delamination in thin film electrodes

By employing the two-dimensional analysis, i.e.,plane strain and plane stress, a semi-analytical method is developed to investigate the interfacial delamination in electrodes. The key parameters are obtained from the governing equations, and their effects on the evolution of the delamination are evaluated. The impact of constraint perpendicular to the plane is also investigated by comparing the plane strain and plane stress. It is found that the delamination in the plane strain condition occurs easier, indicating that the constraint is harmful to maintain the structure stability. According to the obtained governing equations, a formula of the dimensionless critical size for delamination is provided, which is a function of the maximum volumetric strain and the Poisson’s ratio of the active layer.

Layered double hydroxide nanosheets via solvothermal delamination

A new solvothermal post-synthesis treatment for preparing high aspect ratio magnesium aluminium layered double hydroxides(Mg Al–LDHs) has been developed. Treating laurate-intercalated Mg Al–LDHs in pure ethanol in an autoclave for 48 h at 150 °C was found to produce delaminated MgA l–LDH nanosheets with a thickness of ~2.6 nm and an aspect ratio of ~105. It is proposed that the high pressure solvothermal process promotes the insertion of ethanol molecules into the LDH interlayer space, thereby facilitating delamination. This new post-synthesis treatment provides the opportunity for a facile, large scale route to highly delaminated high aspect ratio LDHs, which might be of interest towards novel nanomaterials for energy conversion and storage.

Experimental and simulation studies on delamination strength of laminated glass composites having polyvinyl butyral and ethyl vinyl acetate inter-layers of different critical thicknesses

The laminated glasses(LGs)composites are gaining popularity as protectivestructural material. Delamination strength(DS) of(LGs) with different inter-layers and their different nominal thicknesses were compared. The effect of inter-layer thickness, delamination load, and inter-layer type on DS is clearly observed from this brief study. It is concluded that inter-layer thickness has the significant role in determining the DS of LGs. The statistical analysis confirmed the strong association of DS with inter-layer thickness and the interlayer type. It was found that the LG-PVB composite has the comparatively lower DS than LG-EVA composite and inter-layer thickness has the prominent role in the determination of DS in the LG-EVAcomposite. There is an increment in DS with an increment in critical inter-layer thickness in both LG-EVA and LG-PVBcomposites. The increment in the inter-layer thickness from 0.38 mm to 0.76 mm increases DS significantly; whereas, the further increment in the inter-layer thickness to the higher value has a lesser effect. The finite element model was constituted(without considering the effect of temperature) for determining DS of LG composite. The simulation results were in a good match with experimental results. The results of the present work can be utilized by the design engineers while selecting LG for structural applications.

The Mexican hat effect on the delamination buckling of a compressed thin film

Because of the interaction between film and substrate,the film buckling stress can vary significantly,depending on the delamination geometry,the film and substrate mechanical properties.The Mexican hat effect indicates such interaction.An analytical method is presented,and related dimensional analysis shows that a single dimensionless parameter can effectively evaluate the effect.

Delamination strength of HTS tape under transverse tensile stress and its enhancement by using different Ag layer depositing temperatures

For the application of second generation high temperature superconducting coated conductors (CCs) with layered structures, thermal mismatch between different components and electromagnetic force exerted in superconducting layer in a working magnet can cause transverse tensile stress, which would result in delamination behavior. Therefore many research groups have designed experiments to measure the delamination strength and dedicate to improving that. However, the reason of the discrete distribution of measured data has still not get quantitatively studied, besides, there are lack of investigations on the method of changing depositing conditions to improve the delamination strength except by adding an additional metal layer. In this work, we adopt an anvil test device and obtain delamination strengths as 29.6 MPa of YBa2Cu3O7-x (YBCO)/buffer and 114.6 MPa of buffer/substrate by combing energy disperse spectroscopy (EDS) detection. The reason of discretized measurement data on the delamination strength is explained. Moreover, we find that different temperatures during Ag deposition determine the bonding force of Ag and YBCO layer. The Delamination strength between Ag and YBCO layer increases from 4.4 MPa to larger than 114.6 MPa with temperature elevated from 30℃ to 100℃. Hence we present a novel method for improving the delamination strength of YBCO CCs by setting an optimal temperature of Ag deposition.

DELAMINATION FORMATION AND DELAMINATION PROPAGATION OF COMPOSITE LAMINATES UNDER COMPRESSIVE FATIGUE LOADING

Fatigue tests of the smooth composite laminates and the notched composite laminates under compressive cyclic loading have been carried out. The damage mechanism is discussed and analyzed. Damage evolution is monitored using stiffness decay. From these tests, it is found that the initial delamination occurs at the free boundary of smooth specimens, or the notch boundary of notched specimens, subjected to the compression-compression cyclic load. A point of view in relation to two-phases of compression fatigue delamination of composites is proposed, namely, compression-compression delamination consists of the delamination formation phase and the delamination propagation, and there is a 'damage transition point' to separate this two-phases. Furthermore, an empirical modulus degradation formula and its parameters fitting method are presented. According to the test data handling results, it is shown that this formula is univocal and can fit the test data conveniently. In addition, two kinds of new anti-buckling devices are designed for these tests. At last, the E-N curves, the D-N curves and the S-N curve of the smooth carbon fiber reinforced composite laminates of T300/648C are determined to predict the fatigue life of the notched composite laminate. And the E-N curve of the notched specimens at the given load ratio R = 10 and minimum load Pmin = -0.45 kN is also measured to verify the estimated result of fatigue life.

Piecemeal Delamination of Thickened Lithosphere Triggered Pulsed Magmatism and Mineralization during Late Mesozoic Intracontinental Orogeny in East Asia

The East Asia continent is characterized by a mosaic architecture with various composing blocks,such as the North and South China blocks,which had been collaged in Late Permian to Triassic in response to the break-up of Pangea.In the Late Mesozoic.

Delamination analysis of woven fabrication laminates using cohesive zone model

A new test method was proposed to evaluate the cohesive strength of composite laminates. Cohesive strength and the critical strain energy for Mode-II interlamiar fracture of E-glass/epoxy woven fabrication were determined from the single lap joint(SLJ) and end notch flexure(ENF) test, respectively. In order to verify their adequacy, a cohesive zone model simulation based on interface finite elements was performed. A closed form solution for determination of the penalty stiffness parameter was proposed. Modified form of Park-Paulino-Roesler traction-separation law was provided and conducted altogether with trapezoidal and bilinear mixed-mode damage models to simulate damage using Abaqus cohesive elements. It was observed that accurate damage prediction and numerical convergence were obtained using the proposed penalty stiffness. Comparison between three damage models reveals that good simulation of fracture process zone and delamination prediction were obtained using the modified PPR model as damage model. Cohesive zone length as a material property was determined. To ensure the sufficient dissipation of energy, it was recommended that at least 4 elements should span cohesive zone length.

DETECTION OF DELAMINATION IN A COMPOSITE PLATE BY SEM

A numerical method of integration of Green's functions of strip element method (SEM) is proposed The response of ultrasonic source generated by a transducer on the surface of a multi ply composite plate containing a delamination is analyzed by the use of SEM The numerical results show that the scanning features of the ultrasonic waves may be used to identify the delamination inside the composite plate.

Analysis and Control of Surface Delamination Defects During Milling of Orthogonal Aramid Fiber‑Reinforced Composites Laminates

The aramid fiber-reinforced composites(AFRC)can increase the durability of corresponding applications such as aerospace,automobile and other large structural parts,due to the improvement in hardness,heat build-up,wear properties and green environmental protection.However,because of its complex multiphase structure and unique heterogeneity and anisotropy,the poor compression fatigue resistance and the incident surface fibrillation are inevitable.To improve the assembly precision of AFRC,mechanical processing is necessary to meet the dimensional accuracy.This paper focuses on the influence of contour milling parameters on delamination defects during milling of AFRC laminates.A series of milling experiments are conducted and two different kinds of delamination defects including tearing delamination and uncut-off delamination are investigated.A computing method and model based on brittle fracture for the two different types of delamination are established.The results can be used for explaining the mechanism and regularity of delamination defects.The control strategy of delamination defects and evaluation method of finished surface integrity are further discussed.The results are meaningful to optimize cutting parameters,and provide a clear understanding of surface defects control.

Analysis of pre-crack kinking and delamination in terms of SLB test of honeycomb sandwich structure

The flatwise tension(FWT) and single leg bending(SLB) tests were used to investigate the fracture behavior of honeycomb sandwich specimens.In the FWT test,only the interlaminar delamination was observed.The test results show that the interfacial peel strength is higher than the interlaminar peel strength.In terms of SLB experiment,a new fracture mode was found,namely IKP(initiation of interlaminar delamination,kinking into facesheet and propagation of interlaminar delamination).The virtual crack closure technique was applied to separate the values of Mode I and Mode II components of the strain energy release rate in SLB experiment.The finite element analysis result shows that the Mode I strain energy release rate is higher than the Mode II strain energy release rate.To simulate the failure of SLB test of honeycomb sandwich specimens,a new computational model based on the Tsai-Hill failure criterion and the cohesive zone model is proposed.In comparison with experimental results,it can be concluded that the computational model can validly simulate the IKP of a honeycomb sandwich structures with reasonable accuracy.

Acoustic Response and Micro-Damage Mechanism of Fiber Composite Materials under Mode-Ⅱ Delamination

Realizing the accurate characterization for the dynamic damage process is a great challenge. Here we carry out testing simultaneously for dynamic monitoring and acoustic emission （AE） statistical analysis towards fiber composites under mode-Ⅱ delamination damage. The load curve, AE relative energy, amplitude distribution, and amplitude spectrum are obtained and the delamination damage mechanism of the composites is investigated by the microscopic observation of a fractured specimen. The results show that the micro-damage accumulation around the crack tip region has a great effect on the evolutionary process of delamination. AE characteristics and amplitude spectrum represent the damage and the physical mechanism originating from the hierarchical microstructure. Our finding provides a novel aud feasible strategy to simultaneously evaluate the dynamic response and micro-damage mechanism for fiber composites.

A Modified Cohesive Zone Model for Simulation of Delamination Behavior in Laminated Composites

Considering the promotion effect of interlaminar normal tensile stress and the inhibition effect of interlaminar normal compressive stress,two kinds of elimination initial criteria were proposed in this paper.Based on these two delamination initial criteria,a modified cohesive zone model(CZM)was established to simulate the delamination behavior in laminated composites.Numerical simulations of double cantilever beam(DCB),mixed-mode bending(MMB)and end notched flexure(ENF)tests were conducted.The results show that the proposed model can do a better job than common ones when it is used to predict laminates’delamination under interlaminar compression stress.Moreover,a factor r,named cohesive strength coefficient,was defined in this paper on account of the difference between cohesive strength and interlaminar fracture strength.With changing factor r,it shows that a moderate variation of cohesive strength will not cause significant influences on global load-displacement responses.Besides,in order to obtain a good balance between prediction accuracy and computational efficiency,there shall be two or three numerical elements within the cohesive zone.