Blind tip reconstruction(BTR) method is one of the favorable methods to estimate the atomic force microscopy(AFM) probe shape. The exact shape of the characterizer is not required for BTR, while the geometry of the sa...Blind tip reconstruction(BTR) method is one of the favorable methods to estimate the atomic force microscopy(AFM) probe shape. The exact shape of the characterizer is not required for BTR, while the geometry of the sample may affect the reconstruction significantly. A cone-shaped array sample was chosen as a characterizer to be evaluated. The target AFM probe to be reconstructed was a diamond triangular pyramid probe with two feature angles, namely front angle(FA) and back angle(BA). Four conical structures with different semi-angles were dilated by the pyramid probe. Simulation of scanning process demonstrates that it is easy to judge from the images of the isolated rotary structure, cone-shaped, the suitability of the sample to be a tip characterizer for a pyramid probe. The cone-shaped array sample was repeatedly scanned 50 times by the diamond probe using an AFM. The series of scanning images shrank gradually and more information of the probe was exhibited in the images, indicating that the characterizer has been more suitable for BTR. The feature angle FA of the characterizer increasingly reduces during the scanning process. A self-adaptive grinding between the probe and the characterizer contributes to BTR of the diamond pyramid probe.展开更多
The scratch test is used for quality control mostly in phenomenological ways,and whether fracture toughness can be obtained from this test is still a matter of debate requiring further elucidation.In this paper,values...The scratch test is used for quality control mostly in phenomenological ways,and whether fracture toughness can be obtained from this test is still a matter of debate requiring further elucidation.In this paper,values of the fracture toughness of copper obtained by different scratch-based approaches are compared in order to examine the applicability of scratch-based methodologies to characterize the fracture toughness of soft metals.The scratch response of copper to a Rockwell C diamond indenter is studied under a constant normal load condition.The variations of penetration depth,residual depth,and residual scratch width with applied normal load are quantified from spherical to sphero-conical contact regimes by piecewise functions.A newly proposed size effect law is found to be the most suitable for scratch-based approaches to characterizing the fracture toughness of soft metallic materials with significant plasticity.A simple expression relating the nominal stress to the penetration depth is proposed for the spherical contact regime and gives almost the same value of fracture toughness.The residual scratch width provides useful information on pile-up of material and on the spherical tip radius of the indenter.It is found that the values of the fracture toughness obtained from the microscratch test are influenced by the data range for analysis.展开更多
In order to deposit good films, we need to study the uniformity of plasma density and the plasma density under different gas pressures and powers. The plasma density was diagnosed by a Langmuir probe. The optical emis...In order to deposit good films, we need to study the uniformity of plasma density and the plasma density under different gas pressures and powers. The plasma density was diagnosed by a Langmuir probe. The optical emission spectroscopy （OES） of CH4 and H2 discharge was obtained with raster spectroscopy, with characteristic peaks of H and CH achieved. Diamond-like carbon films were achieved based on the study of plasma density and OES and characterized by atomic force microscope （AFM）, X-ray diffraction instrument （XRD）, Raman spectroscope and profiler.展开更多
提出了一种基于非对称V型槽加载的探针馈电圆极化单层钻石形微带贴片天线。通过调节V型槽的槽宽、槽长、开槽倾角及馈电点位置可实现微带贴片天线的圆极化辐射。研究了V型槽尺寸对微带贴片天线性能的影响。结果表明:介质厚度为0.051λ_0...提出了一种基于非对称V型槽加载的探针馈电圆极化单层钻石形微带贴片天线。通过调节V型槽的槽宽、槽长、开槽倾角及馈电点位置可实现微带贴片天线的圆极化辐射。研究了V型槽尺寸对微带贴片天线性能的影响。结果表明:介质厚度为0.051λ_0(λ_0为中心工作波长)时,天线的阻抗带宽大于9%(VSWR≤2),圆极化带宽为3%(AR≤3),最大增益可达6.29 d Bi,最小轴比小于0.5 d B。展开更多
To resolve inflation of inertial confinement fusion (ICF) target and encapsulation of micro inflation hole with adhesive, a scanning probe microscope (SPM) diamond microprobe was used as the cutting tool with SPM in c...To resolve inflation of inertial confinement fusion (ICF) target and encapsulation of micro inflation hole with adhesive, a scanning probe microscope (SPM) diamond microprobe was used as the cutting tool with SPM in contact mode. Some parameters influencing the quality of micro inflation hole, such as the scanning direction of the diamond tip, the scanning rate and the contact force are discussed. Accurate taper hole was achieved whose climension and precision could meet the requirements of inflation and encapsulation technique of micro hole. The experimental results show that using SPM diamond microprobe as the cutting tool and with special processing technique, the precision machining of target capsule's taper inflation hole can be realized. A novel operative technology for filling high Z gas to target is provided.展开更多
基金supported by the National Natural Science Foundation of China(Grant No.51305298,No.51675379)Tianjin Research Program of Application Foundation and Advanced Technology(Grant No.13JCQNJC04700)
文摘Blind tip reconstruction(BTR) method is one of the favorable methods to estimate the atomic force microscopy(AFM) probe shape. The exact shape of the characterizer is not required for BTR, while the geometry of the sample may affect the reconstruction significantly. A cone-shaped array sample was chosen as a characterizer to be evaluated. The target AFM probe to be reconstructed was a diamond triangular pyramid probe with two feature angles, namely front angle(FA) and back angle(BA). Four conical structures with different semi-angles were dilated by the pyramid probe. Simulation of scanning process demonstrates that it is easy to judge from the images of the isolated rotary structure, cone-shaped, the suitability of the sample to be a tip characterizer for a pyramid probe. The cone-shaped array sample was repeatedly scanned 50 times by the diamond probe using an AFM. The series of scanning images shrank gradually and more information of the probe was exhibited in the images, indicating that the characterizer has been more suitable for BTR. The feature angle FA of the characterizer increasingly reduces during the scanning process. A self-adaptive grinding between the probe and the characterizer contributes to BTR of the diamond pyramid probe.
基金This work was supported by the National Natural Science Foundation of China(No.51705082)the Engineering Research Center for CAD/CAM of Fujian Provincial Colleges and Universities(No.K201705)+1 种基金the Development Center of Scientific and Educational Park of Fuzhou University in the City of Jinjiang(No.2019-JJFDKY-11)Fuzhou University Testing Fund of Precious Apparatus(No.2020T017).
文摘The scratch test is used for quality control mostly in phenomenological ways,and whether fracture toughness can be obtained from this test is still a matter of debate requiring further elucidation.In this paper,values of the fracture toughness of copper obtained by different scratch-based approaches are compared in order to examine the applicability of scratch-based methodologies to characterize the fracture toughness of soft metals.The scratch response of copper to a Rockwell C diamond indenter is studied under a constant normal load condition.The variations of penetration depth,residual depth,and residual scratch width with applied normal load are quantified from spherical to sphero-conical contact regimes by piecewise functions.A newly proposed size effect law is found to be the most suitable for scratch-based approaches to characterizing the fracture toughness of soft metallic materials with significant plasticity.A simple expression relating the nominal stress to the penetration depth is proposed for the spherical contact regime and gives almost the same value of fracture toughness.The residual scratch width provides useful information on pile-up of material and on the spherical tip radius of the indenter.It is found that the values of the fracture toughness obtained from the microscratch test are influenced by the data range for analysis.
基金supported in part by the National Natural Science Foundation of China （10575039） the Chinese Specialized Research Fund for the Doctoral Programme of Higher Education （2004057408）+1 种基金the Key Project of Science Research Fund of Guangdong （China） （05100534）the Science Project Foundation of Guangzhou City （China） （2005Z3-D2031）.
文摘In order to deposit good films, we need to study the uniformity of plasma density and the plasma density under different gas pressures and powers. The plasma density was diagnosed by a Langmuir probe. The optical emission spectroscopy （OES） of CH4 and H2 discharge was obtained with raster spectroscopy, with characteristic peaks of H and CH achieved. Diamond-like carbon films were achieved based on the study of plasma density and OES and characterized by atomic force microscope （AFM）, X-ray diffraction instrument （XRD）, Raman spectroscope and profiler.
文摘提出了一种基于非对称V型槽加载的探针馈电圆极化单层钻石形微带贴片天线。通过调节V型槽的槽宽、槽长、开槽倾角及馈电点位置可实现微带贴片天线的圆极化辐射。研究了V型槽尺寸对微带贴片天线性能的影响。结果表明:介质厚度为0.051λ_0(λ_0为中心工作波长)时,天线的阻抗带宽大于9%(VSWR≤2),圆极化带宽为3%(AR≤3),最大增益可达6.29 d Bi,最小轴比小于0.5 d B。
基金This work was supported by the National Natural Science Foundation of China(Grant No.50275039)the Scientific Research Foundation of Harbin Institute of Technology(HIT2002.23).
文摘To resolve inflation of inertial confinement fusion (ICF) target and encapsulation of micro inflation hole with adhesive, a scanning probe microscope (SPM) diamond microprobe was used as the cutting tool with SPM in contact mode. Some parameters influencing the quality of micro inflation hole, such as the scanning direction of the diamond tip, the scanning rate and the contact force are discussed. Accurate taper hole was achieved whose climension and precision could meet the requirements of inflation and encapsulation technique of micro hole. The experimental results show that using SPM diamond microprobe as the cutting tool and with special processing technique, the precision machining of target capsule's taper inflation hole can be realized. A novel operative technology for filling high Z gas to target is provided.
