Effect of two-stage sintering parameters such as heating rate, top sintering temperature and holding time, sintering temperature and holding time at the second stage on relative density, transverse rupture strength(TR...Effect of two-stage sintering parameters such as heating rate, top sintering temperature and holding time, sintering temperature and holding time at the second stage on relative density, transverse rupture strength(TRS) and microstructures of powder injection molded Ti(C, N)-based cermets were investigated, by means of Archimedes’s method, three-point bending test and micrographic analysis. The results show that the optimum sintering cycle for powder injection molded Ti(C, N)-based cermets comprises rapid heating (10℃/min) at low temperatures, slow heating (5℃/min) at intermediate temperatures, holding at the highest sintering temperature (1420℃) for a short time (10min), and holding at the second stage (1360℃) for a longer time (6h) to avoid grain coarsening, and that its TRS reaches 624MPa, and there are little pores in their microstructures.展开更多
In this work,the small lateral-compression testing based on energy equivalent(SLTEE)method is put forward to determine the stress-strain curves of materials utilizing small disk specimens.Numerical simulations of smal...In this work,the small lateral-compression testing based on energy equivalent(SLTEE)method is put forward to determine the stress-strain curves of materials utilizing small disk specimens.Numerical simulations of small lateral-compression testing with imaginary materials are conducted to examine the validity of the SLT-EE method.The results demonstrate that the stress-strain curves determined by the SLT-EE method coincide with the curves input by finite element analysis.In order to predict the stress-strain curves of materials with different dimensions,a modified SLT-EE method is successfully proposed by introducing a correction factor/.Finally,the small disk compression experiments of Q345B,304,7075 and 6061 are performed.The stress-strain curves of the four materials predicted by the SLT-EE method show agreement with the tension results.Furthermore,the mechanical properties of in-service hollow components are also determined utilizing the same method successfully.展开更多
文摘Effect of two-stage sintering parameters such as heating rate, top sintering temperature and holding time, sintering temperature and holding time at the second stage on relative density, transverse rupture strength(TRS) and microstructures of powder injection molded Ti(C, N)-based cermets were investigated, by means of Archimedes’s method, three-point bending test and micrographic analysis. The results show that the optimum sintering cycle for powder injection molded Ti(C, N)-based cermets comprises rapid heating (10℃/min) at low temperatures, slow heating (5℃/min) at intermediate temperatures, holding at the highest sintering temperature (1420℃) for a short time (10min), and holding at the second stage (1360℃) for a longer time (6h) to avoid grain coarsening, and that its TRS reaches 624MPa, and there are little pores in their microstructures.
基金the financial support from the key projects of the National Natural Science Foundation of China(Grant No.11632001)the innovative development foundation of Chinese Academy of Engineering Physics(Grant No.PY20200046).
文摘In this work,the small lateral-compression testing based on energy equivalent(SLTEE)method is put forward to determine the stress-strain curves of materials utilizing small disk specimens.Numerical simulations of small lateral-compression testing with imaginary materials are conducted to examine the validity of the SLT-EE method.The results demonstrate that the stress-strain curves determined by the SLT-EE method coincide with the curves input by finite element analysis.In order to predict the stress-strain curves of materials with different dimensions,a modified SLT-EE method is successfully proposed by introducing a correction factor/.Finally,the small disk compression experiments of Q345B,304,7075 and 6061 are performed.The stress-strain curves of the four materials predicted by the SLT-EE method show agreement with the tension results.Furthermore,the mechanical properties of in-service hollow components are also determined utilizing the same method successfully.
基金Supported by the National Natural Science Foundation of China under Grant Nos.10571112, 60673105(国家自然科学基金)the Teaching and Research Award Program for Outstanding Young Teachers in Higher Education Institutions of MOE, China(高等学校优秀 青年教师教学科研奖励计划)the National Basic Research Program of China under Grant No.2002CB312200(国家重点基础研究发展 计划(973))