Saturation Dislocation Microstructures of Double-slip-oriented Copper Single Crystal during the Corrosion Fatigue in a 0.5 mol/L NaCl Aqueous Solution

Copper single crystal specimens with the longitudinal axis parallel to the [013] double-slip-orientation were grown through Bridgman technique. The fatigue tests were performed using a symmetric tension-compression load mode at room temperature in an open-air and a 0.5 mol/L NaCl solution, respectively. The dislocation microstructures were observed with scanning electron microscopy (SEM) by the electron channeling contrast (ECC) and transmission electron microscopy (TEM). The results show that the saturation dislocation microstructures during the corrosion fatigue in the aqueous solution of 0.5 mol/L NaCI, mainly consisted of labyrinth, wall and vein dislocation structures, which differs from the dislocation structures of the walls and veins in an open-air environment.

Correlation between the Cyclic Stress Behavior and Microstructure in 316LN based on the Analysis of Hysteresis Loops

Total strain controlled cyclic test was performed on 316 LN under uniaxial loadings. Through the partitioning of hysteresis loops, the evolution of two components of cyclic flow stress, the internal and effective stresses, was reported. The former one determines the cyclic stress response. Based on the transmission electron microscopic（TEM） observation on specimens loaded with scheduled cycles, it is found that planar dislocation structures prevail during the entire cyclic process at low strain amplitude, while a remarkable dislocation rearrangement from planar structures to heterogeneous spatial distributions is companied by a cyclic softening behavior at high strain amplitude. The competition between the evolution of the intergranular and the intragranular components of the internal stress caused by the transition of slip mode induces the cyclic hardening and softening at high strain levels. The intergranular internal stress represents the most part of the internal stress at low strain level.

Deformation Behavior of Fe-36Ni Steel during Cryogenic( 123-173 K) Rolling

Microstructural evolution and mechanical properties of cryogenic rolled Fe-36Ni steel were investigated. The annealed Fe-36Ni steel was rolled at cryogenic temperature（ 123-173 K） with 20%- 90% rolling reduction in thickness.The deformation process was accompanied by twinning at cryogenic temperature,and the mean thickness of deformation twins was about 200 nm with 20% rolling reduction. When the rolling reduction was above 40%,twinning was suppressed due to the stress concentration in the tested steel. Deformation microstructure of Fe-36Ni steel consisted of both twin boundaries and dislocations by cryogenic rolling（ CR）,while it only contained dislocations after rolling at room temperature（ RT）. The tensile strength of Fe-36Ni steel was improved to 930 MPa after 90% reduction at cryogenic temperature,while the tensile strength after 90% reduction at RT was only 760 MPa. More dislocations could be produced as the nucleation sites of recrystallization during CR process.

Effect of Cyclic Stress Reduction on the Creep Characteristics of AZ91 Magnesium Alloy

The creep deformation behavior of aged AZ91 magnesium alloy under the cyclic stress reduction has been investigated in the temperature range 353–383 K. The microstructural evolution of the AZ91 magnesium alloy at different heat treatment conditions has been studied using optical microscopy and scanning electron microscopy. The minimum strain rate, e_min, was found to be higher under cyclic stress reduction condition than that under static creep condition for the same maximum stress. Cyclic creep acceleration is interpreted using the interaction of moving dislocations with the existing b-phase（Mg17Al12） precipitates. The mean value of the activation energy of secondary creep stage was found to be equal to that quoted for lattice self-diffusion of magnesium mechanism.