3,3,4,4-Biphenyltetracarboxylic dianhydride/pyromellitic dianhydride/4,4-oxydianiline（BPDA/PMDA/ODA） polyimide copolymer fibers with different draw ratios were prepared from the imidization of polyacrylic acid（PAA...3,3,4,4-Biphenyltetracarboxylic dianhydride/pyromellitic dianhydride/4,4-oxydianiline（BPDA/PMDA/ODA） polyimide copolymer fibers with different draw ratios were prepared from the imidization of polyacrylic acid（PAA） fibers via a dry-jet wet-spinning process.Their morphologies,microcrystal orientations,thermal stabilities,and mechanical properties were investigated via scanning electron microscopy（SEM）,wide angle X-ray diffraction（WAXD）,thermogravimetric analysis（TGA）,and tensile experiments.In order to acquire fibers with better mechanical performance,we aimed at obtaining the optimal draw ratio.Drawing during thermal imidization resulted in a decreased diameter of fiber from 25.8 μm to 16.9 μm corresponding to draw ratio from 1 to 3.5.WAXD results show that the degree of the orientation of the undrawn sample is 64.1％,whereas that of the drawn sample is up to 82％.The as-spun fiber and those with different draw ratios all exhibit high thermal stabilities,i.e.,the temperature at a mass loss of 5％ can reach as high as 570 ℃.The tensile strengths and tensile modulus of the fibers increase with the draw ratios,and the maximum tensile strength and modulus are 0.90 and 12.61 GPa,respectively.展开更多
The liner of a CNG pressure vessel is manufactured by a DDI(deep drawing and ironing)process for the cylinder part,which is a continuous process that includes a drawing process to reduce the diameter of the billet and...The liner of a CNG pressure vessel is manufactured by a DDI(deep drawing and ironing)process for the cylinder part,which is a continuous process that includes a drawing process to reduce the diameter of the billet and a subsequent ironing process to reduce the thickness of the billet.A tractrix die used in the 1^(st) deep drawing allows the blank to flow smoothly by decreasing the punch load and radial tensile stress occurring in the workpiece.It also increases the draw ratio compared to conventional dies,but it causes forming defects.In this study,a shape coefficient(S_(c))is proposed for the tractrix die using the blank diameter(D_(0)),inflow diameter of the workpiece(d_(i)),and inflow angle of the workpiece(θ)for design of the tractrix die.The effects of the thickness and inflow angle of the workpiece on wrinkling and folding were investigated through FEA.Also,a discriminant is proposed for the relative radial stress(σ)generated during the deep drawing process using the tractirx die and used to predict fracture.Based on the results,the blank thickness,the draw ratio,and the inflow of the workpiece angle in the 1^(st) deep drawing process are suggested,and the number of operations in the DDI process was reduced from 6 to 4.This improves the productivity and reduces the manufacturing cost.展开更多
Prandtl-Reuss flow rule and Hill’s yield criterion were adopted and combined with the concept of finite deformation theory, updated Lagrangian formulation, and a three-dimensional finite element analytical model was ...Prandtl-Reuss flow rule and Hill’s yield criterion were adopted and combined with the concept of finite deformation theory, updated Lagrangian formulation, and a three-dimensional finite element analytical model was established by application of quadrilateral four-node degenerated shell elements coupling into a rigid matrix to deal with the sheet metal forming problems. The fractured thickness of a specimen obtained from a simple tension test was used to be the fracture criterion for the numerical analysis to explore the relationship between punch load and stroke, the thickness distribution, the deformation history and the forming limit of work-piece in the elliptical cup drawing process. The numerical analysis and experiment results show that the punch load increases with the increase of punch stroke, and when the load reaches its maximum, the blank continues to deform with the increase of the punch stroke, resulting in a reduced load until the extension is completed. The minimum thickness of the work-piece concentrates in the contact region of the work-piece and long axis of the punch due to the smaller radius of the curvature of the long axis than the short axis. So the blanks bore the maximum tensile stress in the long axis. Through the limit drawing ratio defined by perimeter of the elliptical punch, the limit drawing ratio of this elliptical cup drawing is defined to be 2.136.展开更多
To investigate how the popular magnesium alloy AZ31 sheet(aluminum 3%,zinc 1%)behaves in cold working,deep drawing experiments at room temperature,along with finite element(FE)simulation,were performed on the cold for...To investigate how the popular magnesium alloy AZ31 sheet(aluminum 3%,zinc 1%)behaves in cold working,deep drawing experiments at room temperature,along with finite element(FE)simulation,were performed on the cold forming sheet of the AZ31 alloy after being annealed under various conditions.The activities were focused on the fracture pattern,limit drawing ratio(LDR),deformation load,thickness distribution,anisotropic effect,as well as the influences of the annealing conditions and tool configuration on them.The results display that punch shoulder radius instead of die clearance,has much influence on the thickness distribution.The anisotropy is remarkable in cold working,which adversely impacts the LDR.The fracture often happens on the side wall at an angle to axis of the deformed specimen.The results also imply that the LDR for the material under present experimental conditions is 1.72,and annealing the material at 450 ℃ for 1 h may be preferable for the cold deep drawing.展开更多
Large cutting height fully mechanized top-coal caving is a new mining method that improves recovery ratio and single-pass production. It also allows safe and efficient mining. A rational cutting height is one key para...Large cutting height fully mechanized top-coal caving is a new mining method that improves recovery ratio and single-pass production. It also allows safe and efficient mining. A rational cutting height is one key parameter of this technique. Numerical simulation and a granular-media model experiment were used to analyze the effect of cutting height on the rock pressure of a fully mechanized top-coal caving work face. The recovery ratio was also studied. As the cutting height increases the top-coal thickness is reduced. Changing the ratio of cutting to drawing height intensifies the face pressure and the top-coal shattering. A maximum cutting height exists under a given set of conditions due to issues with surrounding rock-mass control. An increase in cutting height makes the top-coal cave better and the recovery ratio when drawing top-coal is then improved. A method of adjusting the face rock pressure is presented. Changing the cutting to drawing height ratio is the technique used to control face rock pressure. The recovery ratio when cutting coal exceeds that when caving top-coal so the face recovery ratio may be improved by over sizing the cutting height and increasing the top-coal drawing ratio. An optimum ratio of cutting to drawing height exists that maximizes the face recovery ratio. A rational cutting height is determined by comprehensively considering the surrounding rock-mass control and the recovery ratio. At the same time increasing the cutting height can improve single pass mining during fully mechanized top-coal caving.展开更多
By adopting a homemade extension apparatus and wide-angle X-ray diffraction(WAXD)technique,the structural evolutions of the extracted ultra-high molecular weight polyethylene(UHMWPE)fibers with different spinning draw...By adopting a homemade extension apparatus and wide-angle X-ray diffraction(WAXD)technique,the structural evolutions of the extracted ultra-high molecular weight polyethylene(UHMWPE)fibers with different spinning draw ratios were investigated during the poststretching process.Molecular chains oriented along the axis quickly at the early stage of drawing,which is quite different from the situation of drawing with solvents.The crystal regions,which have not melted at higher temperature,show stronger rigidity in the absence of solvents.Rigid characteristics show faster response to the external field.Also,the surface morphologies of fibers after poststretching are characterized by scanning electron microscopy(SEM).The lamellae stack disordered before stretching,but arranged in order along the draw direction when the draw ratios were larger than 1.展开更多
基金Supported by the National Natural Science Foundation of China（No.51173178）, the National Basic Research Program of China（No.2014CB643600）, the Project of the Science and Technology Bureau of Changchun City, China（No.llGH03）, the De- velopment Project of Jilin Province Science and Technology, China（No.20130413048GH） and the International Cooperative Project of Science and Technology Bureau of Changchun City, China（No.2010064）.
文摘3,3,4,4-Biphenyltetracarboxylic dianhydride/pyromellitic dianhydride/4,4-oxydianiline（BPDA/PMDA/ODA） polyimide copolymer fibers with different draw ratios were prepared from the imidization of polyacrylic acid（PAA） fibers via a dry-jet wet-spinning process.Their morphologies,microcrystal orientations,thermal stabilities,and mechanical properties were investigated via scanning electron microscopy（SEM）,wide angle X-ray diffraction（WAXD）,thermogravimetric analysis（TGA）,and tensile experiments.In order to acquire fibers with better mechanical performance,we aimed at obtaining the optimal draw ratio.Drawing during thermal imidization resulted in a decreased diameter of fiber from 25.8 μm to 16.9 μm corresponding to draw ratio from 1 to 3.5.WAXD results show that the degree of the orientation of the undrawn sample is 64.1％,whereas that of the drawn sample is up to 82％.The as-spun fiber and those with different draw ratios all exhibit high thermal stabilities,i.e.,the temperature at a mass loss of 5％ can reach as high as 570 ℃.The tensile strengths and tensile modulus of the fibers increase with the draw ratios,and the maximum tensile strength and modulus are 0.90 and 12.61 GPa,respectively.
基金Supported by a 2-Year Research Grant of Pusan National University,Korea。
文摘The liner of a CNG pressure vessel is manufactured by a DDI(deep drawing and ironing)process for the cylinder part,which is a continuous process that includes a drawing process to reduce the diameter of the billet and a subsequent ironing process to reduce the thickness of the billet.A tractrix die used in the 1^(st) deep drawing allows the blank to flow smoothly by decreasing the punch load and radial tensile stress occurring in the workpiece.It also increases the draw ratio compared to conventional dies,but it causes forming defects.In this study,a shape coefficient(S_(c))is proposed for the tractrix die using the blank diameter(D_(0)),inflow diameter of the workpiece(d_(i)),and inflow angle of the workpiece(θ)for design of the tractrix die.The effects of the thickness and inflow angle of the workpiece on wrinkling and folding were investigated through FEA.Also,a discriminant is proposed for the relative radial stress(σ)generated during the deep drawing process using the tractirx die and used to predict fracture.Based on the results,the blank thickness,the draw ratio,and the inflow of the workpiece angle in the 1^(st) deep drawing process are suggested,and the number of operations in the DDI process was reduced from 6 to 4.This improves the productivity and reduces the manufacturing cost.
基金funded by research projects (NSC97-2221-E-129-003) of the National Science Council
文摘Prandtl-Reuss flow rule and Hill’s yield criterion were adopted and combined with the concept of finite deformation theory, updated Lagrangian formulation, and a three-dimensional finite element analytical model was established by application of quadrilateral four-node degenerated shell elements coupling into a rigid matrix to deal with the sheet metal forming problems. The fractured thickness of a specimen obtained from a simple tension test was used to be the fracture criterion for the numerical analysis to explore the relationship between punch load and stroke, the thickness distribution, the deformation history and the forming limit of work-piece in the elliptical cup drawing process. The numerical analysis and experiment results show that the punch load increases with the increase of punch stroke, and when the load reaches its maximum, the blank continues to deform with the increase of the punch stroke, resulting in a reduced load until the extension is completed. The minimum thickness of the work-piece concentrates in the contact region of the work-piece and long axis of the punch due to the smaller radius of the curvature of the long axis than the short axis. So the blanks bore the maximum tensile stress in the long axis. Through the limit drawing ratio defined by perimeter of the elliptical punch, the limit drawing ratio of this elliptical cup drawing is defined to be 2.136.
文摘To investigate how the popular magnesium alloy AZ31 sheet(aluminum 3%,zinc 1%)behaves in cold working,deep drawing experiments at room temperature,along with finite element(FE)simulation,were performed on the cold forming sheet of the AZ31 alloy after being annealed under various conditions.The activities were focused on the fracture pattern,limit drawing ratio(LDR),deformation load,thickness distribution,anisotropic effect,as well as the influences of the annealing conditions and tool configuration on them.The results display that punch shoulder radius instead of die clearance,has much influence on the thickness distribution.The anisotropy is remarkable in cold working,which adversely impacts the LDR.The fracture often happens on the side wall at an angle to axis of the deformed specimen.The results also imply that the LDR for the material under present experimental conditions is 1.72,and annealing the material at 450 ℃ for 1 h may be preferable for the cold deep drawing.
基金Financial support for this work, provided by the National Basic Research Program of China (No.2007CB209400)the National Natural Science Foundation of China (No.51004104)
文摘Large cutting height fully mechanized top-coal caving is a new mining method that improves recovery ratio and single-pass production. It also allows safe and efficient mining. A rational cutting height is one key parameter of this technique. Numerical simulation and a granular-media model experiment were used to analyze the effect of cutting height on the rock pressure of a fully mechanized top-coal caving work face. The recovery ratio was also studied. As the cutting height increases the top-coal thickness is reduced. Changing the ratio of cutting to drawing height intensifies the face pressure and the top-coal shattering. A maximum cutting height exists under a given set of conditions due to issues with surrounding rock-mass control. An increase in cutting height makes the top-coal cave better and the recovery ratio when drawing top-coal is then improved. A method of adjusting the face rock pressure is presented. Changing the cutting to drawing height ratio is the technique used to control face rock pressure. The recovery ratio when cutting coal exceeds that when caving top-coal so the face recovery ratio may be improved by over sizing the cutting height and increasing the top-coal drawing ratio. An optimum ratio of cutting to drawing height exists that maximizes the face recovery ratio. A rational cutting height is determined by comprehensively considering the surrounding rock-mass control and the recovery ratio. At the same time increasing the cutting height can improve single pass mining during fully mechanized top-coal caving.
基金Founded by the PhD Foundation of Anhui Jianzhu University (2018QD59)the Natural Science Foundation of Anhui Ed ucation Department (Nos.KJ2021A0624,KJ2019JD18,and KJ2019A0774)+1 种基金the National Natural Science Foundation of China (Nos.51903002,51703218,and 51633009)the Anhui Provincial Science and Technology Major Projects (Nos.17030901101 and 201903a05020027)。
文摘By adopting a homemade extension apparatus and wide-angle X-ray diffraction(WAXD)technique,the structural evolutions of the extracted ultra-high molecular weight polyethylene(UHMWPE)fibers with different spinning draw ratios were investigated during the poststretching process.Molecular chains oriented along the axis quickly at the early stage of drawing,which is quite different from the situation of drawing with solvents.The crystal regions,which have not melted at higher temperature,show stronger rigidity in the absence of solvents.Rigid characteristics show faster response to the external field.Also,the surface morphologies of fibers after poststretching are characterized by scanning electron microscopy(SEM).The lamellae stack disordered before stretching,but arranged in order along the draw direction when the draw ratios were larger than 1.
