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A Discrete State Event Driven Simulation based Losses Analysis for Multi-terminal Megawatt Power Electronic Transformer 被引量:5
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作者 Jialin Zheng Zhengming Zhao +3 位作者 Bochen Shi Zhujun Yu Jiahe Ju Zhiqiang Fan 《CES Transactions on Electrical Machines and Systems》 CSCD 2020年第4期275-284,共10页
At present,power electronic transformers(PETs)have been widely used in power systems.With the increase of PET capacity to the megawatt level.the problem of increased losses need to be taken seriously.As an important i... At present,power electronic transformers(PETs)have been widely used in power systems.With the increase of PET capacity to the megawatt level.the problem of increased losses need to be taken seriously.As an important indicator of power electronic device designing,losses have always been the focus of attention.At present,the losses are generally measured through experiments,but it takes a lot of time and is difficult to quantitatively analyze the internal distribution of PET losses.To solve the above problems,this article first qualitatively analyzes the losses of power electronic devices and proposes a loss calculation method based on pure simulation.This method uses the Discrete State Event Driven(DSED)modeling method to solve the problem of slow simulation speed of large-capacity power electronic devices and uses a loss calculation method that considers the operating conditions of the device to improve the calculation accuracy.For the PET prototype in this article,a losses model of the PET is established.The comparison of experimental and simulation results verifies the feasibility of the losses model.Then the losses composition of PET was analyzed to provide reference opinions for actual operation.It can help pre-analyze the losses distribution of PET,thereby providing a potential method for improving system efficiency. 展开更多
关键词 Power electronic transformer(PET) losses analysis efficiency losses branch model discrete-state event-driven
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Research on power electronic transformer applied in AC/DC hybrid distribution networks 被引量:14
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作者 Yiqun Miao Jieying Song +6 位作者 Haijun Liu Zhengang Lu Shufan Chen Chun Ding Tianzhi Cao Linhai Cai Yuzhong Gong 《Global Energy Interconnection》 2018年第3期396-403,共8页
The AC/DC hybrid distribution network is one of the trends in distribution network development, which poses great challenges to the traditional distribution transformer. In this paper, a new topology suitable for AC/D... The AC/DC hybrid distribution network is one of the trends in distribution network development, which poses great challenges to the traditional distribution transformer. In this paper, a new topology suitable for AC/DC hybrid distribution network is put forward according to the demands of power grid, with advantages of accepting DG and DC loads, while clearing DC fault by blocking the clamping double sub-module(CDSM) of input stage. Then, this paper shows the typical structure of AC/DC distribution network that is hand in hand. Based on the new topology, this paper designs the control and modulation strategies of each stage, where the outer loop controller of input stage is emphasized for its twocontrol mode. At last, the rationality of new topology and the validity of control strategies are verified by the steady and dynamic state simulation. At the same time, the simulation results highlight the role of PET in energy regulation. 展开更多
关键词 AC/DC hybrid distribution network Power electronic transformer(PET) Clamping double sub-module(CDSM) Energy router
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A Critical Topology Review of Power Electronic Transformers:In View of Efficiency 被引量:5
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作者 Guidong Zhang Jie Chen +1 位作者 Bo Zhang Yun Zhang 《Chinese Journal of Electrical Engineering》 CSCD 2018年第2期90-95,共6页
Design of power electronic transformers is a hot research topic and its efficiency improvement is a critical problem all over the world.It is also the largest barrier hindering the application of power electronic tran... Design of power electronic transformers is a hot research topic and its efficiency improvement is a critical problem all over the world.It is also the largest barrier hindering the application of power electronic transformers in industry.In this paper,the state of power electronic transformers is fully presented in terms of efficiency improvements.It is followed by the efficiency modeling of several typical topologies,and their detailed analysis and comparisons.Then,the corresponding industrial application scope of these topologies is presented,providing theoretical guidance for their industrial applications. 展开更多
关键词 Power electronic transformer TOPOLOGY EFFICIENCY MODELING
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A novel low voltage ride through strategy for cascaded power electronic transformer 被引量:3
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作者 Jiexiang Han Xiangping Kong +2 位作者 Peng Li Zhe Zhang Xianggen Yin 《Protection and Control of Modern Power Systems》 2019年第1期239-250,共12页
In view of the operating characteristics for voltage sags of AC side of the power electronic transformer(PET),a low-voltage ride through(LVRT)strategy adapted to bidirectional power exchange of PET is proposed for the... In view of the operating characteristics for voltage sags of AC side of the power electronic transformer(PET),a low-voltage ride through(LVRT)strategy adapted to bidirectional power exchange of PET is proposed for the purposes of maintaining the system stability,assisting the system voltage recovery and protecting PET safety.During the asymmetric voltage sag,the negative sequence current of PET is eliminated to ensure the symmetry of the injected current.According to the degree of positive sequence voltage sag,the reactive current injection is provided to assist in voltage recovery.According to the PET active power condition before the voltage sag,the level and direction of which are maintained as far as possible without exceeding the limit,for which the disturbance to the AC and DC grids is reduced.Finally,the effectiveness of the proposed LVRT strategy is verified by simulation model. 展开更多
关键词 Power electronic transformer Low-voltage ride through Control strategy Current instruction value
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A Three-phase Integrated Power Electronic Transformer with the Capability of DC Fault Clearance 被引量:1
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作者 Yunfei Xu Guangfu Tang +2 位作者 Weiguo Li Guoliang Zhao Zhanfeng Deng 《CSEE Journal of Power and Energy Systems》 SCIE CSCD 2021年第4期785-796,共12页
This paper presents a three-phase integrated power electronic transformer(PET)topology with the capability of DC fault clearance based on the investigation of PET topology.The proposed PET has three ports of high-volt... This paper presents a three-phase integrated power electronic transformer(PET)topology with the capability of DC fault clearance based on the investigation of PET topology.The proposed PET has three ports of high-voltage AC,high-voltage DC and low-voltage DC,which can achieve the flexible access of distributed energy resources・The power unit of the PET adopts a three-phase integrated topology,and the single-phase fluctuating power in the DC-link capacitor is reduced by a 4-port DC/DC converter,thereby reducing the capacitance of the DC-link capacitor;Meanwhile,the power unit uses the clamp double sub-module(CDSM)to allow for self-clearing of the short-circuit fault on the high-voltage DC side.Finally,this paper verifies the proposed PET through an EMT simulation and experimental prototype. 展开更多
关键词 DC fault clearing experimental verification power electronic transformer three phase integration
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Dual-Timescale Control for Power Electronic Zigzag Transformer
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作者 Chunpeng Zhang Zhengming Zhao 《CES Transactions on Electrical Machines and Systems》 2017年第3期315-321,共7页
Power electronic zigzag transformer is an attractive solution for the flexible interconnection of smart distribution networks.It is constituted by slow-response and low-precision thyristor converters and fast-response... Power electronic zigzag transformer is an attractive solution for the flexible interconnection of smart distribution networks.It is constituted by slow-response and low-precision thyristor converters and fast-response and high-accuracy voltage source converters.This paper models its primary circuit and addresses its basic operation mechanism.Then a dual-timescale control scheme is investigated to realize the coordinated regulation of both types of converter.A simulation case is established in PSCAD containing interconnected mid-voltage distribution networks.Simulations with poor-and well-matched control timescales are both carried out.And accordingly,the power flow controllability under these conditions is compared.When the shorter control timescale is no more than tenth of the longer one,the power electronic zigzag transformer will operate with satisfying performances. 展开更多
关键词 Power electronic transformer thyristor converter voltage source converter dual-timescale control flexible interconnection
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Structured Microgrids (SμGs) and Flexible Electronic Large Power Transformers (FeLPTs) 被引量:3
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作者 Don Tan 《CES Transactions on Electrical Machines and Systems》 CSCD 2020年第4期255-263,共9页
Structured microgrids(SμGs)and Flexible electronic large power transformers(FeLPTs)are emerging as two essential technologies for renewable energy integration,flexible power transmission,and active control.SμGs prov... Structured microgrids(SμGs)and Flexible electronic large power transformers(FeLPTs)are emerging as two essential technologies for renewable energy integration,flexible power transmission,and active control.SμGs provide the integration of renewable energy and storage to balance the energy demand and supply as needed for a given system design.FeLPT’s flexibility for processing,control,and re-configurability offers the capability for flexible transmission for effective flow control and enable SμGs connectivity while still keeping multiscale system level control.Early adaptors for combined heat and power have demonstrated significant economic benefits while reducing environmental foot prints.They bring tremendous benefits to utility companies also.With storage and active control capabilities,a 300-percent increase in bulk transmission and distribution lines are possible without having to increase capacity.SμGs and FeLPTs will also enable the utility industry to be better prepared for the emerging large increase in base load demand from electric transportation and data centers.This is a win-win-win situation for the consumer,the utilities(grid operators),and the environment.SμGs and FeLPTs provide value in power substation,energy surety,reliability,resiliency,and security.It is also shown that the initial cost associated with SμG and FeLPTs deployment can be easily offset with reduced operating cost,which in turn reduces the total life-cycle cost by 33%to 67%. 展开更多
关键词 Terms-Structured microgrids flexible electronic large power transformers energy systems renewable integration grid modernization active control life-cycle cost
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Optical fiber-based power and data delivery system for high voltage electronic current transformer
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作者 邱红辉 段雄英 邹积岩 《Journal of Shanghai University(English Edition)》 CAS 2008年第3期268-273,共6页
This paper describes a prototype power delivery system developed for high voltage electronic current transformer (ECT) that uses laser light to transfer power to and communicates with the primary converter. The desi... This paper describes a prototype power delivery system developed for high voltage electronic current transformer (ECT) that uses laser light to transfer power to and communicates with the primary converter. The design is based on optical-to-electrical power converters, solid-state diode lasers and optical fibers. Command signals are transmitted via the same up-fiber used to send power from secondary power supply to primary converter. The upward data transmission is completed during the brief interruption of power delivery without affecting steady power-supply. A simple comparator added to the primary converter can take the command data. Experimental results show that the fibers can provide reliable up-link for data transmission at 200 kb/s from the secondary to the primary converter. Based on the delivery system, the secondary converter can control three auxiliary channels to provide additional information. These monitoring channels are used in a time-multiplexing mode to provide information about the operation temperature, voltage and current at the remote unit for monitoring the ECT. This preventive maintenance or built-in test can increase reliability by giving early warning for necessary maintenance request. 展开更多
关键词 high voltage electronic current transformer (ECT) optical power supply delivery system photovoltaic powerconverters supervisory functions
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Phase field model for electric-thermal coupled discharge breakdown of polyimide nanocomposites under high frequency electrical stress
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作者 韩智云 李庆民 +3 位作者 李俊科 王梦溪 任瀚文 邹亮 《Plasma Science and Technology》 SCIE EI CAS CSCD 2024年第2期114-124,共11页
In contrast to conventional transformers, power electronic transformers, as an integral component of new energy power system, are often subjected to high-frequency and transient electrical stresses, leading to heighte... In contrast to conventional transformers, power electronic transformers, as an integral component of new energy power system, are often subjected to high-frequency and transient electrical stresses, leading to heightened concerns regarding insulation failures. Meanwhile, the underlying mechanism behind discharge breakdown failure and nanofiller enhancement under high-frequency electrical stress remains unclear. An electric-thermal coupled discharge breakdown phase field model was constructed to study the evolution of the breakdown path in polyimide nanocomposite insulation subjected to high-frequency stress. The investigation focused on analyzing the effect of various factors, including frequency, temperature, and nanofiller shape, on the breakdown path of Polyimide(PI) composites. Additionally, it elucidated the enhancement mechanism of nano-modified composite insulation at the mesoscopic scale. The results indicated that with increasing frequency and temperature, the discharge breakdown path demonstrates accelerated development, accompanied by a gradual dominance of Joule heat energy. This enhancement is attributed to the dispersed electric field distribution and the hindering effect of the nanosheets. The research findings offer a theoretical foundation and methodological framework to inform the optimal design and performance management of new insulating materials utilized in high-frequency power equipment. 展开更多
关键词 dielectric discharge breakdown high frequency power electronic transformer polyimide nanocomposites phase field model
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Towards a (More) Electronic Transmission and Distribution (eT&D)
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作者 Don Tan Damir Novosel 《CES Transactions on Electrical Machines and Systems》 2017年第1期15-25,共11页
The challenges and the path towards a(more)electronic transmission and distribution(eT&D)is presented in this paper.The challenges are first identified together with key stakeholders in the drive for grid moderniz... The challenges and the path towards a(more)electronic transmission and distribution(eT&D)is presented in this paper.The challenges are first identified together with key stakeholders in the drive for grid modernization.A fundamental question is then asked about the investment priority.Six basic characteristics are reviewed,leading to the composition of structured microgrids as the basic functional cell of a modern grid.One example of fractal radial structure and one fractal meshed structure are presented.The likely evolution path is then proposed together with basic technology sets.Specific foundation technologies are discussed in detail,including adiabatic power conversion,3MC technology,medium voltage conversion,distribution-level electronic power transformer and FACTs hardware integration,and back-to-back converters as a universal interconnect element.The rapidly emerging on-wire sensing technology is also discussed.It is pointed out that the distribution-level large electronic power transformer will provide a key component to enable hybrid ac/dc grid flow control and ancillary support for a flexible electronic transmission and distribution(eT&D)systems. 展开更多
关键词 All things grid connected electric power systems electronic transmission&distribution(eT&D) energy solutions flexible electronic transmission systems(FETS) grid modernization large electronic power transformers 3MC converters renewable energy.
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Power flow calculation for a distribution system with multi-port PETs:an improved AC-DC decoupling iterative method 被引量:5
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作者 Hang Yin Qiang Li +3 位作者 Youbo Liu Xianglong Liu Yue Xiang Junyong Liu 《Global Energy Interconnection》 2020年第4期313-323,共11页
Recently,power electronic transformers(PETs)have received widespread attention owing to their flexible networking,diverse operating modes,and abundant control objects.In this study,we established a steady-state model ... Recently,power electronic transformers(PETs)have received widespread attention owing to their flexible networking,diverse operating modes,and abundant control objects.In this study,we established a steady-state model of PETs and applied it to the power flow calculation of AC-DC hybrid systems with PETs,considering the topology,power balance,loss,and control characteristics of multi-port PETs.To address new problems caused by the introduction of the PET port and control equations to the power flow calculation,this study proposes an iterative method of AC-DC mixed power flow decoupling based on step optimization,which can achieve AC-DC decoupling and effectively improve convergence.The results show that the proposed algorithm improves the iterative method and overcomes the overcorrection and initial value sensitivity problems of conventional iterative algorithms. 展开更多
关键词 Power electronic transformers AC-DC distribution systems AC-DC mixed power flow algorithm
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Phase Transformation and Enhancing Electron Field Emission Properties in Microcrystalline Diamond Films Induced by Cu Ion Implantation and Rapid Annealing 被引量:1
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作者 申艳艳 张一新 +5 位作者 祁婷 乔瑜 贾钰欣 黑鸿君 贺志勇 于盛旺 《Chinese Physics Letters》 SCIE CAS CSCD 2016年第8期123-126,共4页
Cu ion implantation and subsequent rapid annealing at 500℃ in N2 result in low surface resistivity of 1.611 ohm/sq with high mobility of 290 cm2 V-1S-1 for microcrystalline diamond (MCD) films. Its electrical field... Cu ion implantation and subsequent rapid annealing at 500℃ in N2 result in low surface resistivity of 1.611 ohm/sq with high mobility of 290 cm2 V-1S-1 for microcrystalline diamond (MCD) films. Its electrical field emission behavior can be turned on at Eo = 2.6 V/μm, attaining a current density of 19.5μA/cm2 at an applied field of 3.5 V/#m. Field emission scanning electron microscopy combined with Raman and x-ray photoelectron mi- croscopy reveal that the formation of Cu nanoparticles in MCD films can catalytically convert the less conducting disorder/a-C phases into graphitic phases and can provoke the formation of nanographite in the films, forming conduction channels for electron transportation. 展开更多
关键词 CU of MCD Phase Transformation and Enhancing Electron Field Emission Properties in Microcrystalline Diamond Films Induced by Cu Ion Implantation and Rapid Annealing in by
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ELECTRON MICROSCOPIC OBSERVATION OF SIMIAN SARCOMA VIRUS TRANSFORMED NIH 3T3 CELLS IN VITRO
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作者 田竟生 苏树芸 《Chinese Journal of Cancer Research》 SCIE CAS CSCD 1989年第2期16-18,共3页
For electronic microscopic observation, we found SSV-transformed NIH 3T3 cells were different from non-transformed cells. In SSV-transformed NIH 3T3 cells nuclei cytoplasma ratio was increased and in cytoplasma the ri... For electronic microscopic observation, we found SSV-transformed NIH 3T3 cells were different from non-transformed cells. In SSV-transformed NIH 3T3 cells nuclei cytoplasma ratio was increased and in cytoplasma the ribosomes (polyribosomes were attached to the swollen rough endoplasmic reticulum. It was likely that ribosomes were lined together functionally and structionally to produce specific protein (PDGF-like protein). 展开更多
关键词 NIH ELECTRON MICROSCOPIC OBSERVATION OF SIMIAN SARCOMA VIRUS TRANSFORMED NIH 3T3 CELLS IN VITRO RER
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Relativistic Reduction of the Electron-Nucleus Force in Bohr’s Hydrogen Atom and the Time of Electron Transition between the Neighbouring Quantum Energy Levels
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作者 Stanisław Olszewski 《Journal of Modern Physics》 2020年第6期944-951,共8页
The aim of the paper is to get an insight into the time interval of electron emission done between two neighbouring energy levels of the hydrogen atom. To this purpose, in the first step, the formulae of the special r... The aim of the paper is to get an insight into the time interval of electron emission done between two neighbouring energy levels of the hydrogen atom. To this purpose, in the first step, the formulae of the special relativity are applied to demonstrate the conditions which can annihilate the electrostatic force acting between the nucleus and electron in the atom. This result is obtained when a suitable electron speed entering the Lorentz transformation is combined with the strength of the magnetic field acting normally to the electron orbit in the atom. In the next step, the Maxwell equation characterizing the electromotive force is applied to calculate the time interval connected with the change of the magnetic field necessary to produce the force. It is shown that the time interval obtained from the Maxwell equation, multiplied by the energy change of two neighbouring energy levels considered in the atom, does satisfy the Joule-Lenz formula associated with the quantum electron energy emission rate between the levels. 展开更多
关键词 Hydrogen Atom The Bohr Model Lorentz Transformation Done with the Aid of the Electron Orbital Speed Maxwell Equation Applied to Calculate the Time Interval of Electron Transitions between Two Quantum Energy Levels Comparison with the Joule-Lenz Law for Energy Emission
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Influence of Repetitive Impulse Waveforms on Surface Discharge Characteristics and Insulation Life for Polyimide Film
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作者 Zhiyun Han Qingmin Li +3 位作者 Yujin Guo Tao Liu Guojing Dong Hanwen Ren 《CSEE Journal of Power and Energy Systems》 SCIE EI CSCD 2024年第2期746-755,共10页
Accelerated insulation aging problems under high frequency repetitive impulses in power electronic transformers are drawing more and more attention in modern power systems. Partial discharge (PD) characteristics inclu... Accelerated insulation aging problems under high frequency repetitive impulses in power electronic transformers are drawing more and more attention in modern power systems. Partial discharge (PD) characteristics including discharge inception voltage, phase distribution and statistical characteristics on polyimide (PI) surface under different impulse waveforms and the insulation life of PI films are studied in this paper. We carry out experiments based on PD and insulation lifetime test systems, using five different types of repetitive impulses, including three bipolar waves and two unipolar waves. The experimental results show that there is little variation in discharge inception voltage under different waveforms, but great variation in phase distribution and statistical characteristics of PD. In addition, insulation life is approximately the same under different waveforms with the same polarity, and the aging rate under bipolar waveforms is larger than that under unipolar waveforms. We explain the differences between the bipolar and unipolar waveforms on insulation life, which can be concluded that the surface charge under unipolar waveform accumulates more significnatly compared with bipolar waveform and decreases the electric filed strength in discharging the air gap and inhibits surface discharge from occurring. 展开更多
关键词 Insulation life polyimide film power electronic transformer repetitive impulse surface discharge characteristics
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An approach for parameter estimation of combined CPPM and LFM radar signal 被引量:3
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作者 Zhang Wei Xiong Ying +2 位作者 Wang Pei Wang Jun Tang Bin 《Chinese Journal of Aeronautics》 SCIE EI CAS CSCD 2013年第4期986-992,共7页
In this paper, the problem of parameter estimation of the combined radar signal adopting chaotic pulse position modulation (CPPM) and linear frequency modulation (LFM), which can be widely used in electronic count... In this paper, the problem of parameter estimation of the combined radar signal adopting chaotic pulse position modulation (CPPM) and linear frequency modulation (LFM), which can be widely used in electronic countermeasures, is addressed. An approach is proposed to estimate the initial frequency and chirp rate of the combined signal by exploiting the second-order cyclostationarity of the intra-pulse signal. In addition, under the condition of the equal pulse width, the pulse repetition interval (PRI) of the combined signal is predicted using the low-order Volterra adaptive filter. Simulations demonstrate that the proposed cyclic autocorrelation Hough transform (CHT) algorithm is theoretically tolerant to additive white Gaussian noise. When the value of signal noise to ratio (SNR) is less than 4 dB, it can still estimate the intra-pulse parameters well. When SNR = 3 dB, a good prediction of the PRI sequence can be achieved by the Volterra adaptive filter algorithm, even only 100 training samples. 展开更多
关键词 Chaotic pulse position modulation Combined radar signal Cyclic autocorrelation electronic countermeasures Hough transform Linear frequency modulation Volterra adaptive filter
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Capuli cherry-mediated green synthesis of silver nanoparticles under white solar and blue LED light 被引量:2
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作者 Brajesh Kumar Yolancla Angulo +2 位作者 Kumari Smita Luis Cumbal Alexis Debut 《Particuology》 SCIE EI CAS CSCD 2016年第1期123-128,共6页
In this article, the Capuli (Prunus serotina Ehrh. var. Capuli) cherry extract was used for the synthesis of silver nanoparticles (AgNPs) in the presence of white/visible solar and blue light-emitting diode (LED... In this article, the Capuli (Prunus serotina Ehrh. var. Capuli) cherry extract was used for the synthesis of silver nanoparticles (AgNPs) in the presence of white/visible solar and blue light-emitting diode (LED) light. For the characterization of the extract and the AgNPs, Fourier transform infrared spectroscopy and ultraviolet-visible spectroscopy were employed, along with hydrodynamic particle size analysis, trans- mission electron microscopy and X-ray diffraction. The Ag nanospheres obtained using white light were 40-100 nm in diameter and exhibited an absorption peak at λmax= 445 nm, whereas those obtained using blue LED light were 20-80 nm in diameter with an absorption peak at λmax= 425 nm. Thermal analysis revealed that the content of biomolecules surrounding the AgNPs was about 55-65%, and it was also found that blue LED light AgNPs (56.28%, 0.05 mM) had a higher antioxidant efficacy than the white solar light AgNPs (33.42%, 0.05 mM) against l,l-diphenyl-2-picrylhydrazyl. The results indicate that obtaining AgNPs using a blue LED light may prove to be a simple, cost-effective and easily reproducible method for creating future nanopharmaceuticals. 展开更多
关键词 Silver nanoparticles Capuli LED light Fourier transform infrared spectroscopy Transmission electron microscopy Antioxidant
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Opposite Relationship between Orientation Selection and Texture Memory in the Deformed Electrical Steel Sheets during α→γ→α Transformation 被引量:1
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作者 Louwen Zhang Ping Yang Weimin Mao 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2017年第12期1522-1530,共9页
The undesired {111} texture component for the magnetic properties mainly exists in the sheets of electrical steels by the conventional process, whereas the sheets with the non-{111} texture can be obtained by α→γ→... The undesired {111} texture component for the magnetic properties mainly exists in the sheets of electrical steels by the conventional process, whereas the sheets with the non-{111} texture can be obtained by α→γ→α transformation. In this paper, we mainly investigate the opposite relationship between orientation selection and texture memory in the deformed ultra-low carbon steel sheet during →→ transformation annealing. A 0.5 mm thick hot-rolled sheet is directly subjected to transformation. The result shows that the specific transformation textures are not possible to generate in the sheets without deformation. Besides, transformation annealing is conducted on the recrystallized sheets in hydrogen and vacuum, respectively. The near {100} and {110} grains have the growth advantage at the atmosphere/metal interface, and the initial ferrite textures are retained in vacuum. Cold-rolled sheets with different thicknesses are annealed for transformation in vacuum, hydrogen and nitrogen, respectively.The near {100} and {110} textures are still the preferential orientations at the atmosphere/metal interface. When the surface grains have sufficiently large growth advantage, the {111} grains developed by texture memory effect will be annexed. Otherwise, the {111} grains at the center layer of the sheets are hard to be replaced, and they are retained after α→γ→α transformation cycle. The results of deformed sheets annealed with different heating rates in hydrogen show that the growth of initial recrystallization grains has a great effect on variant selection. 展开更多
关键词 Orientation selection Texture memory Electrical steels α→γ→α transformation Electron back-scatter diffraction
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Processing of Calamine with Modern Analytical Techniques:Processed with Huanglian Decoction(黄连汤)and Sanhuang Decoction(三黄汤) 被引量:2
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作者 MENG Xiang-long MA Jun-nan +4 位作者 GUO Xiao-hui LIU Bing-chen CUI Nan-nan LI Kun ZHANG Shuo-sheng 《Chinese Journal of Integrative Medicine》 SCIE CAS CSCD 2017年第11期850-857,共8页
Objective: To determine the pyrolysis characteristics of calcined and processed calamine, qualitatively and quantitatively compare the contents of related elements, morphology and functional groups of the pyrolysis p... Objective: To determine the pyrolysis characteristics of calcined and processed calamine, qualitatively and quantitatively compare the contents of related elements, morphology and functional groups of the pyrolysis products dried at different heating temperatures and explore the critical temperature and the optimal drying temperature for the process of calamine with Huanglian Decoction(HLD, 黄连汤) and San Huang Decoction(SHD, 三黄汤). Methods: Pyrolysis products were prepared by programmable and constantly heating the calcined and processed calamine to or at different heating temperatures. Thermogravimetry(TG) was used to test their pyrolysis characteristics. Fourier transform infrared spectroscopy and scanning electron microscopeenergy dispersive spectrometer were used to determine their morphology, functional groups and element contents. Page model was used to investigate the constant drying kinetics of processed calamine. Results: The adding of HLD or SHD to calcined calamine(CC) can slow its weight loss in drying pyrolysis process. The temperature ranges where HLD and SHD can affect its weight loss were 65–150 ℃ and 74–180 ℃, respectively. The drying temperature was optimized as 90 ℃. The drying kinetic for the processed calamine fits Page model shows good linearity. Conclusions: The critical temperature and the optimal drying temperature where HLD and SHD can affect the weight loss rate in the process of calamine were explored using the theories and methods of both biophysical chemistry and processing of Chinese materia medica. This work provides a good example for the study of the process of other Chinese medicines using modern analytical techniques. 展开更多
关键词 processing of Chinese materia medica calcined calamine processed Calamine thermogravimetry fourier transformation infrared spectrometry scanning electron microscope-energy dispersive spectrometer
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Systematic study of Ce^(3+) on the structural and magnetic properties of Cu nanosized ferrites for potential applications 被引量:6
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作者 Majid Niaz Akhtar A.B.Sulong +1 位作者 M.N.Akhtar Muhammad Azhar Khan 《Journal of Rare Earths》 SCIE EI CAS CSCD 2018年第2期156-164,共9页
Ce^(3+) substituted Cu-spinel nanoferrites CuCe_xFe_(2-x)O_4(x=0.00, 0.02, 0.04, 0.06, 0.08 and 0.10) were synthesized via sol-gel self-combustion hybrid route. Single phase spinel ferrite of Cu nanoferrites we... Ce^(3+) substituted Cu-spinel nanoferrites CuCe_xFe_(2-x)O_4(x=0.00, 0.02, 0.04, 0.06, 0.08 and 0.10) were synthesized via sol-gel self-combustion hybrid route. Single phase spinel ferrite of Cu nanoferrites were examined using X-ray diffraction(XRD) analysis whereas the multiphase structure was observed as Ce contents increased from x=0.06. Field emission scanning electron microscopy(FESEM), Thermogravimetric and differential thermal analysis(TGA and DTA) and Fourier transform infrared spectroscopy(FTIR) were used to find out the morphology phase and metal stretching vibrations of Ce^(3+) substituted nanocrystalline ferrites. The crystallite size was increased and found in the range of 25-91 nm. The agglomerations in Cu ferrite samples increase as the Ce^(3+) concentration increases. The magnetic properties such as remanence, saturation magnetization, coercivity, Bohr magneton and magnetocrystalline anisotropy constant(K) were determined using M-H loops recorded from a vibrating sample magnetometer(VSM). Saturation magnetization, remanence and coercivity are increased as the Ce^(3+)contents increase in Cu nanocrystalline samples. Moreover, law of approach to saturation(LoA) was used to calculate the maximum value of saturation for Ce-doped Cu nanoferrites. The soft magnetic behaviour of the Cu nanoferrite is observed as compared to the samples substituted with the increased Ce contents in Cu nanocrystalline ferrite. Bohr magneton and magnetocrystalline anisotropy are found to increase with the substitution of rare earth Ce^(3+) contents in Cu spinel nanocrystalline ferrite. Cedoped Cu nanocrystalline ferrites with excellent properties may be suitable for potential applications in sensing, security, switching, core, multilayer chip inductor, biomedical and microwave absorption applications. 展开更多
关键词 Ce-doped Cu nanocrystalline ferrites X-ray diffraction(XRD) Scanning electron microscopy(SEM) Transmission electron microscopy(TEM) Fourier transform infrared(FTIR) Vibrating sample magnetometer(VSM)
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