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Atomic Emission Spectrometry of Inductively Coupled Plasma with Sample Introduction by Electrothermal Vaporization
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作者 Huang Min , Jiang Zucheng Zeng Yun’ e (Department of Chemistry, Wuhan University, Wuhan) Present address, Center of Material Research and Testing, Wuhan University of Technology, Wuhan. To Whom correspondence should be addressed. 《Chemical Research in Chinese Universities》 SCIE CAS CSCD 1991年第1期27-31,共5页
A system is described in which a graphite furnace electrothermal vaporization device is employed for the introduction of microlitre liquid sample into an inductively coupled argon plasma. The technique provides a pico... A system is described in which a graphite furnace electrothermal vaporization device is employed for the introduction of microlitre liquid sample into an inductively coupled argon plasma. The technique provides a picogram detection limit and an adequate precision with a relative standard deviation of 4%. Mechanism of analyte condensation in transport process is explored. As an application, the technique combined with DDTC/CCl4 extraction is used to enrich and determine non- rare earth impurities in highly pure La2O3. 展开更多
关键词 electrothermal sample introduction Inductively coupled plasma Optical emis-sion spectrometry
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