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Study on Optimization of Ethanol Reflux Extraction of Phenolic Acids from Salvia miltiorrhiza 被引量:2
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作者 Ying Gao Jinlin Wu 《Journal of Biosciences and Medicines》 CAS 2023年第1期98-105,共8页
The extraction technology of phenolic acid compounds from Salvia miltiorrhiza by ethanol reflux was studied. In this experiment, salvianolic acid B standard was used to make the standard curve. Single factor experimen... The extraction technology of phenolic acid compounds from Salvia miltiorrhiza by ethanol reflux was studied. In this experiment, salvianolic acid B standard was used to make the standard curve. Single factor experiment and orthogonal experiment were used to study the extraction of different ethanol concentrations, reflux times and material-to-liquid ratios. The OD value of salvianolic acid compounds was measured with a spectrophotometer. The extraction rate of phenolic acid compounds under different extraction conditions was calculated through a regression equation, so as to obtain the optimal conditions for the ethanol reflux extraction process of Salvia miltiorrhiza. The experimental data can provide a reference for the ethanol reflux extraction process of salvianolic acids in the industry. According to the experiment, the extraction rate of phenolic acids in Salvia miltiorrhiza was the highest when the ethanol concentration was 60%, the reflux time was 1.5 hours, and the ratio of material-to-liquid was 1:10. 展开更多
关键词 Salvia miltiorrhiza Phenolic Acid Compounds Salvianolic Acid B ethanol Reflux Orthogonal Experiment
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Cu/SiO_2:A recyclable catalyst for the synthesis of octahydroquinazolinone 被引量:2
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作者 Majid M.Heravi Narges Karimi +1 位作者 Hoda Hamidi Hossein A.Oskooie 《Chinese Chemical Letters》 SCIE CAS CSCD 2013年第2期143-144,共2页
Received 14 September 2012 Received in revised form 13 December 2012 Accepted 20 December 2012 Available online 4 February 2013
关键词 One-pot reactionOctahydroquinazolinoneCu/Si02Reflux ethanol
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