Geological radar probing technology finds wide application in engineering projects. The high-precision characteristics of geologic radar should be studied in connection with fine processing and interpretation. This ar...Geological radar probing technology finds wide application in engineering projects. The high-precision characteristics of geologic radar should be studied in connection with fine processing and interpretation. This article discusses such issues as (1) geologic radar noise source and (2) fine processing and interpretation of radar data. It is focused on how to achieve fine processing and interpretation.展开更多
Ultra-fine CeO_2-ZrO_2 mixed oxide was successfully synthesized by wet-solid phase mechanochemical processing, Ce_2(CO_3)_3·8H_2O, ZrOCl_2·xH_2O and ammonia were used as reactants. It is found that the cryst...Ultra-fine CeO_2-ZrO_2 mixed oxide was successfully synthesized by wet-solid phase mechanochemical processing, Ce_2(CO_3)_3·8H_2O, ZrOCl_2·xH_2O and ammonia were used as reactants. It is found that the crystalline Ce_2(CO_3)_3·8H_2O and ZrOCl_2·xH_2O are changed to amorphous cerium and zirconium hydroxide precursor after milling with ammonia, and Ce_(0.15)Zr_(0.85)O_2 mixed oxide with pure tetragonal phase structure and medium particle size(D_(50))less than 1μm is formed by calcining precursor over 673 K. The XRD patterns indicate that the crystal unite size increases with rising calcining temperature due to crystal growth. However, the particle size and BET surface area of the Ce(Zr)O_2 mixed oxide decreases with rising calcining temperature, which may be attributed to the contract of particles and the vanish of holes inside grains.展开更多
Strontium bismuth tantalum (SBT) fine power was prepared by Sol-Gel method. Pentaethoxy tantalum, strontium acetate and bismuth subnitrate were used as raw materials, and were dissolved in proper order in ethylene gl...Strontium bismuth tantalum (SBT) fine power was prepared by Sol-Gel method. Pentaethoxy tantalum, strontium acetate and bismuth subnitrate were used as raw materials, and were dissolved in proper order in ethylene glycol to form transparent sol. The mixed precursor was dried at 80℃ and annealed at 800℃ for 1 h. Crystallized nanometer sized SBT fine powder was obtained and characterized by XRD.展开更多
Fine-grained BaTiO3-based X7R ceramic materials were prepared and the effects of milling process on the core-shell structures and dielectric properties were investigated using scanning electron microscope, transmissio...Fine-grained BaTiO3-based X7R ceramic materials were prepared and the effects of milling process on the core-shell structures and dielectric properties were investigated using scanning electron microscope, transmission electron microscope, and energy dispersive spectroscopy (EDS). As the milling time extends, the dielectric constant of the ceramics increases, whereas the temperature coefficient of capacitance at 125℃ drops quickly. The changes in dielectric properties are considered relevant to the microstructure evolution caused by the milling process. Defects on the surface of BaTiO3 particles increase because of the effects of milling process, which will make it easier for additives to diffuse into the interior grains. As the milling time increases, the shell region gets thicker and the core region gets smaller; however, EDS results show that the chemical inhomogeneity between grain core and grain shell becomes weaker.展开更多
Compacting process of fine powder is greatly affected by the aggregate structure of particles. According to the experiment in which several kinds of silicon nitrides in different partical shape and size were compacted...Compacting process of fine powder is greatly affected by the aggregate structure of particles. According to the experiment in which several kinds of silicon nitrides in different partical shape and size were compacted in uniaxialorientation, it is found that the volume compacting rate offorming body differs with the pressure. The aggregatestructure of each sample A, B or C was estimated by applying Cooper's equation to the analysis of the compacting process of each sample展开更多
Fault fracture zones and water-bearing bodies in front of the driving head are the main disasters in mine laneways,thus it is important to perform their advanced detection and prediction in advance in order to provide...Fault fracture zones and water-bearing bodies in front of the driving head are the main disasters in mine laneways,thus it is important to perform their advanced detection and prediction in advance in order to provide reliable technical support for the excavation.Based on the electromagnetic induction theory,we analyzed the characteristics of primary and secondary fields with a positive and negative wave form of current,proposed the fine processing of the advanced detection with variation rate of apparent resistivity and introduced in detail the computational formulae and procedures.The result of physical simulation experiments illustrate that the tectonic interface of modules can be judged by first-order rate of apparent resistivity with a boundary error of 5%,and the position of water body determined by the fine analysis method agrees well with the result of borehole drilling.This shows that in terms of distinguishing structure and aqueous anomalies,the first-order rate of apparent resistivity is more sensitive than the secondorder rate of apparent resistivity.However,some remaining problems are suggested for future solutions.展开更多
The liquid phase behavior of the fine-grained 5083 AI alloy obtained through thermomechanical process was investigated during the tensile tests in a temperature range of 380-570℃ and strain rate range of 4.17× 1...The liquid phase behavior of the fine-grained 5083 AI alloy obtained through thermomechanical process was investigated during the tensile tests in a temperature range of 380-570℃ and strain rate range of 4.17× 10^-4- 1.0× 10^-2 s^-1. The maximum elongation 530% of the fine-grained 5083 AI alloy was obtained at 550℃ and 4.17× 10^-4 s^-1. Fracture analysis by scanning electron microscopy (SEM) indicated that the formation of filament (formed by liquid phase) was greatly affected by the tensile temperature and strain rate. The results also showed that the optimum morphology of formed filament was obtained at 550℃ and a strain rate of 4.17× 10^-4 s^-1. The effect of liquid phase on superplastic deformation of the alloy was further discussed.展开更多
A super-high temperature furnace was developed to fabricate spheroidal cast tungsten carbide powder with excellent flowability and fine feathery structure in a large scale. Optical microscope and scanning electron mic...A super-high temperature furnace was developed to fabricate spheroidal cast tungsten carbide powder with excellent flowability and fine feathery structure in a large scale. Optical microscope and scanning electron microscope were taken to characterize the morphology and microstructure of cast tungsten carbide powder. X-ray diffractometry was used to analyze the phase composition of powders involved. It is found that the carbon potential in the furnace and feeding speed play an important role on the microstructure, morphology and properties of the spheroidal cast tungsten carbide powder. As carbon potential is between 0.3% and 0.9% in the furnace, cast tungsten carbide powder with hardness over 2800(HV0.5), flowability over 7.1 s/50 g and tap density over 10.3 g/cm3 is obtained.展开更多
Suitable methods for enhancing the volume stability of steel slag utilized as fine aggregate were determined. The effects of steam treatment at 100 ℃ and autoclave treatment under 2.0 MPa on the soundness of steel sl...Suitable methods for enhancing the volume stability of steel slag utilized as fine aggregate were determined. The effects of steam treatment at 100 ℃ and autoclave treatment under 2.0 MPa on the soundness of steel slag sand were investigated by means of powder ratio, linear expansion, compressive and flexural strength. DTA, EDX, XRD and ethylene glycol methods were employed to analyze both the treated slags and susceptible expansion grains. Experimental results indicate that powder ratio, content of free lime and rate of linear expansion can express the improvement in volume stability of different treated methods. Steam treatment process cannot ultimately prevent specimens from cracking and decrease of strength, but mortar made from autoclave treated slag keeps integration subjected to hot water of 80℃ until 28 d and its strength do not show significant decrement. The hydration of over-burn free lime and periclase phase are the main cause for the disintegration or crack of untreated and steam treated steel slag's specimens. Autoclave treatment process is more effective than steam treatment process on enhancement of volume stability of steel slag.展开更多
In order to provide certain references for further deepening the development of processing industry of agricultural products,this paper analyzed and elaborated the basic principles,construction priorities and safeguar...In order to provide certain references for further deepening the development of processing industry of agricultural products,this paper analyzed and elaborated the basic principles,construction priorities and safeguard measures of the development of deep processing industry of agricultural products in Nanchong City of Sichuan Province. Besides,it made a scientific planning for accelerating the deep processing of agricultural products in Nanchong City in 2018-2020,to ensure the full implementation of fine and deep processing of agricultural products.展开更多
A study on alkaline sulfite anthraquinone pulping of wheat straw indicated that the addition of formaldehyde could improve fine pulp yield effectively, enhance brightness of unbleached pulp, and decrease kappa number....A study on alkaline sulfite anthraquinone pulping of wheat straw indicated that the addition of formaldehyde could improve fine pulp yield effectively, enhance brightness of unbleached pulp, and decrease kappa number. Finally, the optimum conditions of this process were formed.展开更多
As a part of the green process for manufacturing chromium compounds, two steps are involved in the synthesis of ultra-fine Cr2O3 powders: the first is the hydrogen reduction of K2CrO4 into intermediate trivalent (C...As a part of the green process for manufacturing chromium compounds, two steps are involved in the synthesis of ultra-fine Cr2O3 powders: the first is the hydrogen reduction of K2CrO4 into intermediate trivalent (Cr^3+) or tetravalent (Cr^4+) chromium compounds; the second is the decomposing of the intermediate into Cr2O3 by heat treating. The intermediate is well characterized by means of SEM, XRD, and XPS. The possible reaction mechanism of the process is analyzed.展开更多
基金This project is sponsored by The Special Fund of Scientific Instruments of National Natural Science Foundation of China(50127402) and The Geophysical Responses to The High-resolution Exploration for Coal-methane of 973 Program(2002CB211707).
文摘Geological radar probing technology finds wide application in engineering projects. The high-precision characteristics of geologic radar should be studied in connection with fine processing and interpretation. This article discusses such issues as (1) geologic radar noise source and (2) fine processing and interpretation of radar data. It is focused on how to achieve fine processing and interpretation.
文摘Ultra-fine CeO_2-ZrO_2 mixed oxide was successfully synthesized by wet-solid phase mechanochemical processing, Ce_2(CO_3)_3·8H_2O, ZrOCl_2·xH_2O and ammonia were used as reactants. It is found that the crystalline Ce_2(CO_3)_3·8H_2O and ZrOCl_2·xH_2O are changed to amorphous cerium and zirconium hydroxide precursor after milling with ammonia, and Ce_(0.15)Zr_(0.85)O_2 mixed oxide with pure tetragonal phase structure and medium particle size(D_(50))less than 1μm is formed by calcining precursor over 673 K. The XRD patterns indicate that the crystal unite size increases with rising calcining temperature due to crystal growth. However, the particle size and BET surface area of the Ce(Zr)O_2 mixed oxide decreases with rising calcining temperature, which may be attributed to the contract of particles and the vanish of holes inside grains.
文摘Strontium bismuth tantalum (SBT) fine power was prepared by Sol-Gel method. Pentaethoxy tantalum, strontium acetate and bismuth subnitrate were used as raw materials, and were dissolved in proper order in ethylene glycol to form transparent sol. The mixed precursor was dried at 80℃ and annealed at 800℃ for 1 h. Crystallized nanometer sized SBT fine powder was obtained and characterized by XRD.
基金supported by the National Science fund for Distinguished Young Scholars (No.50625204)the National Natural Science Foundation of China (Science Fund for Creative Research Groups)(No.50621201)+1 种基金the Major State Basic Research Development Program of China (No.2009CB623301)the National High-Tech Research and Development Program of China (No.2006AA03Z0428), and Samsung Electro-Mechanics Co., Ltd.
文摘Fine-grained BaTiO3-based X7R ceramic materials were prepared and the effects of milling process on the core-shell structures and dielectric properties were investigated using scanning electron microscope, transmission electron microscope, and energy dispersive spectroscopy (EDS). As the milling time extends, the dielectric constant of the ceramics increases, whereas the temperature coefficient of capacitance at 125℃ drops quickly. The changes in dielectric properties are considered relevant to the microstructure evolution caused by the milling process. Defects on the surface of BaTiO3 particles increase because of the effects of milling process, which will make it easier for additives to diffuse into the interior grains. As the milling time increases, the shell region gets thicker and the core region gets smaller; however, EDS results show that the chemical inhomogeneity between grain core and grain shell becomes weaker.
文摘Compacting process of fine powder is greatly affected by the aggregate structure of particles. According to the experiment in which several kinds of silicon nitrides in different partical shape and size were compacted in uniaxialorientation, it is found that the volume compacting rate offorming body differs with the pressure. The aggregatestructure of each sample A, B or C was estimated by applying Cooper's equation to the analysis of the compacting process of each sample
基金supports for this work,provided by the Natural Science Foundation of Jiangsu Province (No. BK2009095)the National Natural Science Foundation of China (No. 51004102)+1 种基金the National Science & Technology Support Project of the 11th Five-Year Plan of China (No. 2007Bak24B03)the State Basic Research and Development Program of China (No. 2007CB209400)
文摘Fault fracture zones and water-bearing bodies in front of the driving head are the main disasters in mine laneways,thus it is important to perform their advanced detection and prediction in advance in order to provide reliable technical support for the excavation.Based on the electromagnetic induction theory,we analyzed the characteristics of primary and secondary fields with a positive and negative wave form of current,proposed the fine processing of the advanced detection with variation rate of apparent resistivity and introduced in detail the computational formulae and procedures.The result of physical simulation experiments illustrate that the tectonic interface of modules can be judged by first-order rate of apparent resistivity with a boundary error of 5%,and the position of water body determined by the fine analysis method agrees well with the result of borehole drilling.This shows that in terms of distinguishing structure and aqueous anomalies,the first-order rate of apparent resistivity is more sensitive than the secondorder rate of apparent resistivity.However,some remaining problems are suggested for future solutions.
文摘The liquid phase behavior of the fine-grained 5083 AI alloy obtained through thermomechanical process was investigated during the tensile tests in a temperature range of 380-570℃ and strain rate range of 4.17× 10^-4- 1.0× 10^-2 s^-1. The maximum elongation 530% of the fine-grained 5083 AI alloy was obtained at 550℃ and 4.17× 10^-4 s^-1. Fracture analysis by scanning electron microscopy (SEM) indicated that the formation of filament (formed by liquid phase) was greatly affected by the tensile temperature and strain rate. The results also showed that the optimum morphology of formed filament was obtained at 550℃ and a strain rate of 4.17× 10^-4 s^-1. The effect of liquid phase on superplastic deformation of the alloy was further discussed.
文摘A super-high temperature furnace was developed to fabricate spheroidal cast tungsten carbide powder with excellent flowability and fine feathery structure in a large scale. Optical microscope and scanning electron microscope were taken to characterize the morphology and microstructure of cast tungsten carbide powder. X-ray diffractometry was used to analyze the phase composition of powders involved. It is found that the carbon potential in the furnace and feeding speed play an important role on the microstructure, morphology and properties of the spheroidal cast tungsten carbide powder. As carbon potential is between 0.3% and 0.9% in the furnace, cast tungsten carbide powder with hardness over 2800(HV0.5), flowability over 7.1 s/50 g and tap density over 10.3 g/cm3 is obtained.
基金the National Natural Science Foundation of China (No.50678139)
文摘Suitable methods for enhancing the volume stability of steel slag utilized as fine aggregate were determined. The effects of steam treatment at 100 ℃ and autoclave treatment under 2.0 MPa on the soundness of steel slag sand were investigated by means of powder ratio, linear expansion, compressive and flexural strength. DTA, EDX, XRD and ethylene glycol methods were employed to analyze both the treated slags and susceptible expansion grains. Experimental results indicate that powder ratio, content of free lime and rate of linear expansion can express the improvement in volume stability of different treated methods. Steam treatment process cannot ultimately prevent specimens from cracking and decrease of strength, but mortar made from autoclave treated slag keeps integration subjected to hot water of 80℃ until 28 d and its strength do not show significant decrement. The hydration of over-burn free lime and periclase phase are the main cause for the disintegration or crack of untreated and steam treated steel slag's specimens. Autoclave treatment process is more effective than steam treatment process on enhancement of volume stability of steel slag.
基金Supported by the Project of National Modern Agriculture Demonstration Area of the Ministry of Agriculture "Nanchong City National Modern Agriculture Demonstration Area"[Nong Ji Fa(2010)22]Project of Nanchong City National Modern Agriculture Demonstration Area Agricultural Reform and Construction Pilot Demonstration Area of the Ministry of Agriculture and Ministry of Finance[Nong Cai Fa(2013)13]Project of Nanchong City Nanchong National Agricultural Science and Technology Park of Ministry of Science and Technology(Guo Ke Ban Nong(2015)9]
文摘In order to provide certain references for further deepening the development of processing industry of agricultural products,this paper analyzed and elaborated the basic principles,construction priorities and safeguard measures of the development of deep processing industry of agricultural products in Nanchong City of Sichuan Province. Besides,it made a scientific planning for accelerating the deep processing of agricultural products in Nanchong City in 2018-2020,to ensure the full implementation of fine and deep processing of agricultural products.
文摘A study on alkaline sulfite anthraquinone pulping of wheat straw indicated that the addition of formaldehyde could improve fine pulp yield effectively, enhance brightness of unbleached pulp, and decrease kappa number. Finally, the optimum conditions of this process were formed.
基金the Knowledge Innovation Program of the Chinese Academy of Sciences(No.082813)the Key Program of National Natural Science Foundation of China(No.50234040)+1 种基金the National Science & Technology Pillar Program in the Eleventh Five-year Plan Period(No.2006BAC02A05)the National Basic Research Program(973 Program)of China(No.2007CB613500)
文摘As a part of the green process for manufacturing chromium compounds, two steps are involved in the synthesis of ultra-fine Cr2O3 powders: the first is the hydrogen reduction of K2CrO4 into intermediate trivalent (Cr^3+) or tetravalent (Cr^4+) chromium compounds; the second is the decomposing of the intermediate into Cr2O3 by heat treating. The intermediate is well characterized by means of SEM, XRD, and XPS. The possible reaction mechanism of the process is analyzed.