Two kinds nitride modified layers were obtained on Ti-13Nb-13 Zr surface to improve the wear property via magnetron sputtering and plasma nitriding techniques, respectively. The structures of the modified layer and th...Two kinds nitride modified layers were obtained on Ti-13Nb-13 Zr surface to improve the wear property via magnetron sputtering and plasma nitriding techniques, respectively. The structures of the modified layer and the worn surface after sliding test were characterized using X-ray diffraction(XRD) and scanning electron microscopy(SEM). The friction and wear behavior of the modified layer against alumina ball was investigated in the absence of lubricant under different loads(1 N and 2 N). The X-ray diffraction analysis reveals that nitride layer is mainly composed of TiN and Ti2N, while coating film consists of Ti N phase. Friction and wear test indicates that both modified layers can improve the wear resistance compared to untreated Ti-13Nb-13 Zr. Ti N thin film produces very hard surface, but may be easy to cause coating fracture and delamination under high normal load. However, nitride layer exhibits better wear performance. This is attributed to hard compound layer maintained its integrity with the hardened nitrogen diffusion zone during friction and wear process.展开更多
The friction and wear behavior of Fe Al intermetallics based coating produced by high velocity arc spraying technique under dry sliding at room temperature were investigated using a ball on disc tribotester. The ef...The friction and wear behavior of Fe Al intermetallics based coating produced by high velocity arc spraying technique under dry sliding at room temperature were investigated using a ball on disc tribotester. The effect of sliding speed on friction coefficient and wear of the coating was studied. The worn surface of the coating was analyzed by scanning electron microscope (SEM) to explore sliding friction and wear mechanism. The results show that the variations of friction coefficient can be divided into three distinct steps during the trail. Both the friction coefficient and the wear of the coating increase with increased sliding speed due to accelerated crack propagation rate and lamellar structure with poor ductility of the coating. The coating surface is subjected to alternately tensile stress and compression stress during sliding wear process, and the predominant wear mechanism of the coatings appears to be brittle fracture and delamination.展开更多
The objective of this research is to prepare specially designed surface texture on hard steel surface by electrochemical micromachining (EM) and to incorporate electroless plated Ag/MoS2 solid lubricant coating into t...The objective of this research is to prepare specially designed surface texture on hard steel surface by electrochemical micromachining (EM) and to incorporate electroless plated Ag/MoS2 solid lubricant coating into the dimples of EM textured steel surface to effectively reduce friction and wear of steel-steel contacts. The friction and wear behavior of the Ag/MoS2 solid lubricant coating on EM textured steel surface was evaluated in relation to the size and spacing of the dimples thereon. The microstructure of as-plated Ag/MoS2 solid lubricant coating and the morphology and elemental composition of the worn coating surface and counterface steel surface were analyzed by means of optical microscopy, scanning electron microscopy, and energy dispersive spectrometry. It is found that electroless plated Ag/MoS2 coating is able to greatly reduce the friction and wear of the EM textured steel disc coupled with GCr15 steel ring, mainly because of the formation of solid self-lubricating layer on the EM textured steel surface and of transferred lubricating film on counterface steel surface. The diameter and spacing of the dimples are suggested as 500 μm for acquiring the best wear resistance of the hard steel discs after electrochemical micromachining treatment and electroless plating of Ag/MoS2 solid lubricating coating.展开更多
Diamond-like carbon (DLC) films were synthesized by plasma immersion ion implantation and deposition (PIIID) on 9Cr18 bearing steel surface. Influences of working gas pressure and pulse width of the bias voltage on pr...Diamond-like carbon (DLC) films were synthesized by plasma immersion ion implantation and deposition (PIIID) on 9Cr18 bearing steel surface. Influences of working gas pressure and pulse width of the bias voltage on properties of the thin film were investigated. The chemical compositions of the as-deposited films were characterized by Raman spectroscopy. The micro-hardness, friction and wear behavior, corrosion resistance of the samples were evaluated, respectively. Compared with uncoated substrates, micro-hardness results reveal that the maximum is increased by 88.7%. In addition, the friction coefficient decreases to about 0.1, and the corrosion resistance of treated coupons surface are improved significantly.展开更多
Molybdenum dialkyldithiocarbamate(MoDTC)is widely used as a friction modifier in engine lubricating oil.Under MoDTC lubrication,the friction and wear behaviors of tungsten-doped diamond-like carbon(W-DLC)films anneale...Molybdenum dialkyldithiocarbamate(MoDTC)is widely used as a friction modifier in engine lubricating oil.Under MoDTC lubrication,the friction and wear behaviors of tungsten-doped diamond-like carbon(W-DLC)films annealed at 100-400℃were discussed and evaluated using scanning electron microscopy(SEM),atomic force microscopy(AFM),and Raman spectroscopy.Under(polymerized alpha olefin)PAO+MoDTC lubrication,the coefficient of friction of all samples decreased,but the wear rates of the W-DLC films annealed at 300℃increased significantly.By interacting with zinc dialkyldithiophosphate(ZDDP),the wear rates of W-DLC films annealed at different temperatures declined significantly owing to the formation of dense phosphate tribofilms on the worn surfaces.展开更多
基金Funded by the National Natural Science Foundation of China(Nos.51671140 and 51474154)the Shanxi Province Programs for Graduate Education Reform(2015JG42)
文摘Two kinds nitride modified layers were obtained on Ti-13Nb-13 Zr surface to improve the wear property via magnetron sputtering and plasma nitriding techniques, respectively. The structures of the modified layer and the worn surface after sliding test were characterized using X-ray diffraction(XRD) and scanning electron microscopy(SEM). The friction and wear behavior of the modified layer against alumina ball was investigated in the absence of lubricant under different loads(1 N and 2 N). The X-ray diffraction analysis reveals that nitride layer is mainly composed of TiN and Ti2N, while coating film consists of Ti N phase. Friction and wear test indicates that both modified layers can improve the wear resistance compared to untreated Ti-13Nb-13 Zr. Ti N thin film produces very hard surface, but may be easy to cause coating fracture and delamination under high normal load. However, nitride layer exhibits better wear performance. This is attributed to hard compound layer maintained its integrity with the hardened nitrogen diffusion zone during friction and wear process.
基金NationalNatureScienceFoundationofChina (No .5 0 0 0 5 0 2 4)
文摘The friction and wear behavior of Fe Al intermetallics based coating produced by high velocity arc spraying technique under dry sliding at room temperature were investigated using a ball on disc tribotester. The effect of sliding speed on friction coefficient and wear of the coating was studied. The worn surface of the coating was analyzed by scanning electron microscope (SEM) to explore sliding friction and wear mechanism. The results show that the variations of friction coefficient can be divided into three distinct steps during the trail. Both the friction coefficient and the wear of the coating increase with increased sliding speed due to accelerated crack propagation rate and lamellar structure with poor ductility of the coating. The coating surface is subjected to alternately tensile stress and compression stress during sliding wear process, and the predominant wear mechanism of the coatings appears to be brittle fracture and delamination.
基金supported by the the National NaturalScience Foundation of China(No.51205001)Foundation for Young Talents in College of Anhui Province(No.2012SQRL083ZD)the Talent Innovation Fund of An-hui Polytechnic University(No.S05305)
文摘The objective of this research is to prepare specially designed surface texture on hard steel surface by electrochemical micromachining (EM) and to incorporate electroless plated Ag/MoS2 solid lubricant coating into the dimples of EM textured steel surface to effectively reduce friction and wear of steel-steel contacts. The friction and wear behavior of the Ag/MoS2 solid lubricant coating on EM textured steel surface was evaluated in relation to the size and spacing of the dimples thereon. The microstructure of as-plated Ag/MoS2 solid lubricant coating and the morphology and elemental composition of the worn coating surface and counterface steel surface were analyzed by means of optical microscopy, scanning electron microscopy, and energy dispersive spectrometry. It is found that electroless plated Ag/MoS2 coating is able to greatly reduce the friction and wear of the EM textured steel disc coupled with GCr15 steel ring, mainly because of the formation of solid self-lubricating layer on the EM textured steel surface and of transferred lubricating film on counterface steel surface. The diameter and spacing of the dimples are suggested as 500 μm for acquiring the best wear resistance of the hard steel discs after electrochemical micromachining treatment and electroless plating of Ag/MoS2 solid lubricating coating.
文摘Diamond-like carbon (DLC) films were synthesized by plasma immersion ion implantation and deposition (PIIID) on 9Cr18 bearing steel surface. Influences of working gas pressure and pulse width of the bias voltage on properties of the thin film were investigated. The chemical compositions of the as-deposited films were characterized by Raman spectroscopy. The micro-hardness, friction and wear behavior, corrosion resistance of the samples were evaluated, respectively. Compared with uncoated substrates, micro-hardness results reveal that the maximum is increased by 88.7%. In addition, the friction coefficient decreases to about 0.1, and the corrosion resistance of treated coupons surface are improved significantly.
基金This research was financially supported by the National Natural Science Foundation of China(Nos.51875537 and 41872183)the Pre-Research Program in National 14th Five-Year Plan(No.61409230614)the Fundamental Research Funds for the Central University(No.2652018094).
文摘Molybdenum dialkyldithiocarbamate(MoDTC)is widely used as a friction modifier in engine lubricating oil.Under MoDTC lubrication,the friction and wear behaviors of tungsten-doped diamond-like carbon(W-DLC)films annealed at 100-400℃were discussed and evaluated using scanning electron microscopy(SEM),atomic force microscopy(AFM),and Raman spectroscopy.Under(polymerized alpha olefin)PAO+MoDTC lubrication,the coefficient of friction of all samples decreased,but the wear rates of the W-DLC films annealed at 300℃increased significantly.By interacting with zinc dialkyldithiophosphate(ZDDP),the wear rates of W-DLC films annealed at different temperatures declined significantly owing to the formation of dense phosphate tribofilms on the worn surfaces.