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Physical and Mathematical Modeling of the Argon-Oxygen Decarburization Refining Process of Stainless Steel 被引量:5
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作者 魏季和 《Journal of Shanghai University(English Edition)》 CAS 2002年第1期1-23,共23页
The available studies in the literature on physical and mathematical modeling of the argon oxygen decarburization (AOD) process of stainless steel have briefly been reviewed. The latest advances made by the author wi... The available studies in the literature on physical and mathematical modeling of the argon oxygen decarburization (AOD) process of stainless steel have briefly been reviewed. The latest advances made by the author with his research group have been summarized. Water modeling was used to investigate the fluid flow and mixing characteristics in the bath of an 18 t AOD vessel, as well as the 'back attack' action of gas jets and its effects on the erosion and wear of the refractory lining, with sufficiently full kinematic similarity. The non rotating and rotating gas jets blown through two annular tuyeres, respectively of straight tube and spiral flat tube type, were employed in the experiments. The geometric similarity ratio between the model and its prototype (including the straight tube type tuyeres) was 1:3. The influences of the gas flow rate, the angle included between the two tuyeres and other operating parameters, and the suitability of the spiral tuyere as a practical application, were examined. These latest studies have clearly and successfully brought to light the fluid flow and mixing characteristics in the bath and the overall features of the back attack phenomena of gas jets during the blowing, and have offered a better understanding of the refining process. Besides, mathematical modeling for the refining process of stainless steel was carried out and a new mathematical model of the process was proposed and developed. The model performs the rate calculations of the refining and the mass and heat balances of the system. Also, the effects of the operating factors, including adding the slag materials, crop ends, and scrap, and alloy agents; the non isothermal conditions; the changes in the amounts of metal and slag during the refining; and other factors were all considered. The model was used to deal with and analyze the austenitic stainless steel making (including ultra low carbon steel) and was tested on data of 32 heats obtained in producing 304 grade steel in an 18 t AOD vessel. The changes in the bath composition and temperature during the refining process with time can be accurately predicted using this model. The model can provide some very useful information and a reliable basis for optimizing the process practice of the refining of stainless steel and control of the process in real time and online. 展开更多
关键词 stainless steel argon oxygen decarburization (AOD) process fluid flow and mixing back attack phenomenon non rotating and rotating gas jets DECARBURIZATION water modeling mathematical modeling.
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分离打拿极电子倍增器性能提升技术研究
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作者 李洁 杨济世 +4 位作者 刘虎林 刘碧野 赵源 胡文波 吴胜利 《真空电子技术》 2023年第1期18-24,共7页
研究了磁控溅射法制备二次电子发射薄膜过程中氩气与氧气流量比和打拿极极间分压方式对电子倍增器增益及衰减特性的影响。研究表明,采用25∶5的氩气与氧气流量比所制备的MgO/(MgO-Au)双层结构薄膜具有最大的二次电子发射系数(SEY)和最小... 研究了磁控溅射法制备二次电子发射薄膜过程中氩气与氧气流量比和打拿极极间分压方式对电子倍增器增益及衰减特性的影响。研究表明,采用25∶5的氩气与氧气流量比所制备的MgO/(MgO-Au)双层结构薄膜具有最大的二次电子发射系数(SEY)和最小的SEY衰减率,同时利用该薄膜制作的九级打拿极电子倍增器具有最高的增益和最小的增益衰减率,这与该薄膜拥有最大的MgO晶粒尺寸和合适的导电性密切相关;采用第九打拿极与地之间的分压电阻阻值为3 MΩ且前八级打拿极极间分压电阻阻值均为6 MΩ的打拿极极间差异化分压方式制作电子倍增器能够提高器件增益,降低器件工作电压,并减缓在电子持续轰击下的增益衰减。该研究结果对高性能分离打拿极电子倍增器研制及其应用具有重要意义。 展开更多
关键词 电子倍增器 二次电子发射 氩气与氧气流量比 打拿极极间分压方式
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磁控溅射氧氩体积流量比对β-Ga_(2)O_(3)薄膜的影响
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作者 杨赉 杨发顺 +1 位作者 熊倩 马奎 《微纳电子技术》 CAS 北大核心 2023年第3期448-453,共6页
利用射频磁控溅射在c面单晶蓝宝石(Al_(2)O_(3))衬底上制备Ga_(2)O_(3)薄膜,研究了溅射过程中通入氧气与氩气的体积流量比对经过异位高温后退火处理得到的β-Ga_(2)O_(3)薄膜特性的影响。利用X射线衍射仪(XRD)和原子力显微镜(AFM)对薄... 利用射频磁控溅射在c面单晶蓝宝石(Al_(2)O_(3))衬底上制备Ga_(2)O_(3)薄膜,研究了溅射过程中通入氧气与氩气的体积流量比对经过异位高温后退火处理得到的β-Ga_(2)O_(3)薄膜特性的影响。利用X射线衍射仪(XRD)和原子力显微镜(AFM)对薄膜进行表征,结果表明β-Ga_(2)O_(3)薄膜沿着■晶面择优生长,具备较好的单一取向性。在氧氩体积流量比约为1∶20时,薄膜的结晶性能相对较好、表面晶粒分布较均匀、均方根粗糙度较小、晶粒尺寸较大。此外,吸收光谱表征结果表明,不同氧氩体积流量比下制备得到的β-Ga_(2)O_(3)薄膜的带隙变化范围为4.53~4.64 eV,在较低氧氩体积流量比下制备的β-Ga_(2)O_(3)薄膜表现出较优的光学性质,在波长200~300 nm内具有较好的吸收特性,表现出良好的深紫外光学特性。 展开更多
关键词 β-Ga_(2)O_(3) 蓝宝石(Al_(2)O_(3))衬底 射频磁控溅射 氧氩体积流量比 结晶性能 光学特性
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直流脉冲磁控反应溅射技术制备掺铝氧化锌薄膜的研究 被引量:3
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作者 陈超 冀勇 +4 位作者 郜小勇 赵孟珂 马姣民 张增院 卢景霄 《物理学报》 SCIE EI CAS CSCD 北大核心 2012年第3期338-343,共6页
采用直流脉冲磁控反应溅射技术,在不同氧氩比(GFR)条件下玻璃衬底上制备了一系列掺铝氧化锌(AZO)薄膜,并利用X射线衍射、扫描电子显微镜和分光光度计从宏观应力和微观晶格畸变的角度研究了GFR对薄膜结构、表面形貌和光学特性的影响.制... 采用直流脉冲磁控反应溅射技术,在不同氧氩比(GFR)条件下玻璃衬底上制备了一系列掺铝氧化锌(AZO)薄膜,并利用X射线衍射、扫描电子显微镜和分光光度计从宏观应力和微观晶格畸变的角度研究了GFR对薄膜结构、表面形貌和光学特性的影响.制备的多晶AZO薄膜呈现了明显的ZnO-(103)择优取向,这归结于3 h薄膜沉积过程中伴随的退火引起的薄膜晶面能转变.随着GFR的增大,AZO薄膜内宏观拉应力先增大到最大值,随后宏观压应力随着GFR的继续增大而增大.薄膜中的宏观应力明显随着GFR从拉应力向压应力转变.这与晶格微观畸变诱导的微观应力的研究结果趋势恰恰相反.随着GFR的增加,薄膜在可见光区的平均透射率先增加后减小,薄膜晶粒尺寸诱导的晶界散射是影响薄膜透射率的主导机制. 展开更多
关键词 掺铝氧化锌薄膜 直流脉冲磁控反应溅射 光学性质 氧氩比
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