An energy consumption analysis based on the heating characteristic of a building with central heat exchanger in a university of Tianjin was done,and the feasibility of intermittent heating with variable speed pumps wa...An energy consumption analysis based on the heating characteristic of a building with central heat exchanger in a university of Tianjin was done,and the feasibility of intermittent heating with variable speed pumps was discussed. By comparing various methods of energy consumption analysis,a modified Bin method based on the weather data in Tianjin was adopted. The heat consumption of the buildings under intermittent heating mode was calculated and compared with continuous heating mode,the result shows that intermittent heating can reduce energy consumption for 1 941 759 kW·h,save standard coal for 341 t,and reduce pump power consumption for 72 679 kW·h annually. Intermittent operation by means of varying the pump frequency not only leads to savings in fuel consumption and reduction in pollutant emissions,but also reduces operating costs significantly and it is an ideal energy-saving method. By analyzing the results,the recommendations of heating operation regulation and the transformation of pipe network were proposed separately to different kinds of buildings in colleges,such as laboratory building,teaching building.展开更多
Primary and secondary networks are treated as a whole in indirect heating systems, and an advanced new temperature-flow regulation method is presented whose flow ratio is greater than 60% in a secondary network and 30...Primary and secondary networks are treated as a whole in indirect heating systems, and an advanced new temperature-flow regulation method is presented whose flow ratio is greater than 60% in a secondary network and 30% in a primary network when under a partial load. Through deducing and optimizing an exponential function flow regulation rule, the formulae of flow regulation and the supply and return water temperatures are obtained, and their relevant curves are plotted. After comparison, it is found that this control method has a huge energy conservation space, and it should therefore be generalized soon.展开更多
Accurate insight into the heat generation rate(HGR) of lithium-ion batteries(LIBs) is one of key issues for battery management systems to formulate thermal safety warning strategies in advance.For this reason,this pap...Accurate insight into the heat generation rate(HGR) of lithium-ion batteries(LIBs) is one of key issues for battery management systems to formulate thermal safety warning strategies in advance.For this reason,this paper proposes a novel physics-informed neural network(PINN) approach for HGR estimation of LIBs under various driving conditions.Specifically,a single particle model with thermodynamics(SPMT) is first constructed for extracting the critical physical knowledge related with battery HGR.Subsequently,the surface concentrations of positive and negative electrodes in battery SPMT model are integrated into the bidirectional long short-term memory(BiLSTM) networks as physical information.And combined with other feature variables,a novel PINN approach to achieve HGR estimation of LIBs with higher accuracy is constituted.Additionally,some critical hyperparameters of BiLSTM used in PINN approach are determined through Bayesian optimization algorithm(BOA) and the results of BOA-based BiLSTM are compared with other traditional BiLSTM/LSTM networks.Eventually,combined with the HGR data generated from the validated virtual battery,it is proved that the proposed approach can well predict the battery HGR under the dynamic stress test(DST) and worldwide light vehicles test procedure(WLTP),the mean absolute error under DST is 0.542 kW/m^(3),and the root mean square error under WLTP is1.428 kW/m^(3)at 25℃.Lastly,the investigation results of this paper also show a new perspective in the application of the PINN approach in battery HGR estimation.展开更多
The relationship among heating rate, mechanical properties, microstructure and texture of Al-Mg-Si-Cu alloy during solution treatment was investigated through tensile test, scanning electron microscope, X-ray diffract...The relationship among heating rate, mechanical properties, microstructure and texture of Al-Mg-Si-Cu alloy during solution treatment was investigated through tensile test, scanning electron microscope, X-ray diffractometer and EBSD technology. The experimental results reveal that there is a non-monotonic relationship among solution heating rate, mechanical properties, microstructure and texture. As the solution heating rate increases, the strength variations are dependent on the tensile direction;work hardening exponent n decreases first, and then increases;plastic strain ratio r increases first, and then decreases, and finally increases. The final microstructure and texture are also affected by heating rate. As heating rate increases, the microstructure transforms from elongated grain structure to equiaxed grain structure, and the average grain size decreases first, and then increases, and decreases finally. Although the texture components including CubeND{001}<310> and P{011}<122> orientations almost have no change with the increase of heating rate, the texture intensity and volume fraction decrease first, and then increase, and finally decrease. Both microstructure and texture evolutions are weakly affected by heating rate. Improving heating rate is not always favorable for the development of fine equiaxed grain structure, weak texture and high average r value, which may be related to the recrystallization behavior.展开更多
This study introduces a novel method of electric field sintering for preparing NdFeB magnets. NdFeB alloy compacts were all sintered by electric fields for 8 min at 1000~C with different preset heating rates. The char...This study introduces a novel method of electric field sintering for preparing NdFeB magnets. NdFeB alloy compacts were all sintered by electric fields for 8 min at 1000~C with different preset heating rates. The characteristics of electric field sintering and the effects of heating rate on the sintering densification of NdFeB alloys were also studied. It is found that electric field sintering is a new non-pressure rapid sintering method for preparing NdFeB magnets with fine grains at a relatively lower sintering temperature and in a shorter sintering time. Using this method, the sintering temperature and process of the compacts can be controlled accurately. When the preset heating rate in- creasing from 5 to 2000~C/s the densification of NdFeB sintered compacts gradHally improves. As the preset heating rate is 2000C/s, Nd-rich phases are small, dispersed and uniformly distributed in the sintered compact, and the magnet has a better microstructure than that made by conventional vacuum sintering. Also, the maximum energy product of the sintered magnet reaches 95% of conventionally vacuum sintered magnets.展开更多
Oxide scale formation on a C-steel surface has been investigated using linear heating rates ranging from 0.1℃/min to 10℃/min at high temperatures. The studies on the oxide scale formation at high temperature (650℃)...Oxide scale formation on a C-steel surface has been investigated using linear heating rates ranging from 0.1℃/min to 10℃/min at high temperatures. The studies on the oxide scale formation at high temperature (650℃) at slower heating rate (0.1℃/min) shows that the kinetic regime is linear. X-ray diffraction measurements revealed that the scale constituents are significantly influenced by the heating rate. The adherence of the scale was improved by using slower heating rate (0.1℃/min-≤650℃), while above such degree the scale was susceptible to cracking and flaking out of the alloy surface. In fact, the development of oxide growth stresses can cause considerable scale cracking. As well, variation of the crystallite sizes under the aforementioned conditions might affect the scale stacking to the alloy surface. The secondary electron detector images of the oxide scale shows that the scale was imperfectly smooth and there were a number of voids and defects in the scale skin, especially at fast heating rate. This observation could be attributed to defects of the as-received alloy. In general, slower heating rate reduced the defects of the scale and improved its adherence.展开更多
Indium tin oxide (ITO) films were prepared on polyester, Si and glass substrate with relatively high deposition rate of above 0.9 nm/s by DC reactive magnetron sputtering technique at the sputtering pressure of 0.06 P...Indium tin oxide (ITO) films were prepared on polyester, Si and glass substrate with relatively high deposition rate of above 0.9 nm/s by DC reactive magnetron sputtering technique at the sputtering pressure of 0.06 Pa system, respectively. The dependence of resistivity on deposition parameters, such as deposition rate, target-to-substrate distance (TSD), oxygen flow rate and sputtering time (thickness), has been investigated, together with the structural and the optical properties. It was revealed that all ITO films exhibited lattice expansion. The resistivity of ITO thin films shows significant substrate effect: much lower resistivity and broader process window have been reproducibly achieved for the deposition of ITO films onto polyester rather than those prepared on both Si and glass substrates. The films with resistivity of as low as 4.23 x 10^-4 Ω.cm and average transmittance of ~78% at wavelength of 400~700 nm have been achieved for the films on polyester at room temperature.展开更多
The influence of heating rate on double reversible transformation in CuZnAlMnNi shape memory alloy was investigated by differential scanning calorimetry. It was found that rapid heating inhibits X -->M transformati...The influence of heating rate on double reversible transformation in CuZnAlMnNi shape memory alloy was investigated by differential scanning calorimetry. It was found that rapid heating inhibits X -->M transformation but is favorable to the reverse martensite transformation, giving rise to the approach of the two transformation peaks. With the decrease of heating rate, the two transformation peaks separate gradually.展开更多
Effects of temperature and heating rate on the mechanical properties of the tensile specimens of magnesium alloy AZ31 were experimentally investigated using a Gleeble-1500 thermo-mechanical material testing system.The...Effects of temperature and heating rate on the mechanical properties of the tensile specimens of magnesium alloy AZ31 were experimentally investigated using a Gleeble-1500 thermo-mechanical material testing system.The metallurgraphs of the fracture section of the specimens were also experimentally observed and analyzed for exploring their failure mechanism under different temperatures and heating rates.The results show that the higher the temperature,the lower the ultimate strength of the specimens.And the higher the heating rate,the higher the ultimate strength of the specimens.The high temperatures and high heating rates will induce microvoids in the specimens which make the specimens failure under relatively low loads.展开更多
We investigated the effects of heating rate on the process parameters of superplastic forming for Zr55Cu30Al10Ni5 by differential scanning calorimetry. The continuous heating and isothermal annealing analyses suggeste...We investigated the effects of heating rate on the process parameters of superplastic forming for Zr55Cu30Al10Ni5 by differential scanning calorimetry. The continuous heating and isothermal annealing analyses suggested that the temperatures of glass transition and onset crystallization are heating rate-dependent in the supercooled liquid region. Then, the time-temperature-transformation diagram under different heating rates indicates that increasing the heating rate can lead to an increase of the incubation time at the same anneal temperature in the supercooled liquid region. Based on the Arrhenius relationship, we discovered that the incubation time increases by 1.08-1.11 times with double increase of the heating rate at the same anneal temperature, and then verified it by the data of literatures and the experimental results. The obtained curve of the max available incubation time reveals that the incubation time at a certain anneal temperature in the supercooled liquid region is not infinite, and will increase with increasing heating rate until this temperature shifts out of the supercooled liquid region because of exceeding critical heating rate. It is concluded that heating rate must be an important processing parameter of superplastic forming for Zr55Cu30Al10Ni5.展开更多
The latitude-altitude distributions of radiative fluxes and heating rates are investigated by utilizing CloudSat satellite data over China during summer. The Tibetan Plateau causes the downward shortwave fluxes of the...The latitude-altitude distributions of radiative fluxes and heating rates are investigated by utilizing CloudSat satellite data over China during summer. The Tibetan Plateau causes the downward shortwave fluxes of the lower atmosphere over central China to be smaller than the fluxes over southern and northern China by generating more clouds. The existence of a larger quantity of clouds over central China reflects a greater amount of solar radiation back into space. The vertical gradients of upward shortwave radiative fluxes in the atmosphere below 8 km are greater than those above 8 km. The latitudinal-altitude distributions of downward longwave radiative fluxes show a slantwise decreasing trend from low latitudes to high latitudes that gradually weaken in the downward direction. The upward longwave radiative fluxes also weaken in the upward direction but with larger gradients. The maximum heating rates by solar radiation and cooling rates by longwave infrared radiation are located over 28 40°N at 7 8 km mean sea level (MSL), and they are larger than the rates in the northern and southern regions. The heating and cooling rates match well both vertically and geographically.展开更多
The effect of the heating rate on the nucleation of metallic glass in a rapid heating process starting from the glass transition temperature is investigated. The critical nucleus radius increases with the increase of ...The effect of the heating rate on the nucleation of metallic glass in a rapid heating process starting from the glass transition temperature is investigated. The critical nucleus radius increases with the increase of the temperature of the undercooling liquid. If the increment rate of the critical nucleus radius, owing to the heating process, is higher than the growth rate of the nuclei, the nuclei generated at the low temperature will become the embryos at the high temperature. This means that the high heating rate can make no nucleation happen in the heating process. In consideration of the interfacial energy, the growth rate of the nuclei increases with the increase of their size and the growth rate of the critical nucleus is zero. Thus, the lower heating rate can also make the nuclei decline partially. Finally, this theory is used to analyze the nucleation process during laser remelting metallic glass.展开更多
The effects of heating rate on the aggregate behavior of poly(ethylene oxide)-b-poly(N-isopropylacrylamide) in aqueous solutions were investigated in detail by laser light scattering and TEM. By employing two sepa...The effects of heating rate on the aggregate behavior of poly(ethylene oxide)-b-poly(N-isopropylacrylamide) in aqueous solutions were investigated in detail by laser light scattering and TEM. By employing two separate heating protocols, step-by-step heating at 〈 5 K/step and one-step jump, to heat the sample from 15℃ to the selected temperature, we found that the heating rate only showed significant effect on the aggregates above the cloud point. The aggregate formed by step-by-step heating exhibited a much larger size and a broader size distribution than those formed by one-step jump heating. Moreover, neither of the aggregates were ideal micellar structures as indicated by the size and the Rg/Rh values. On the contrary, at temperatures below the cloud point where the block copolymer formed core-shelled micelles, the heating rate showed negligible effect on the size and size distribution of the micelles. Since the system underwent a phase separation above the cloud point, the heating rate effect could be reasonably explained by the phase separation mechanisms: the nucleation-and-growth mechanism in the metastable region and the spinodal decomposition mechanism in the unstable region.展开更多
In the framework of the finite element method (FEM), a prediction method for the heating rate and the skin friction on a body surface is presented by using the energy and momentum conservation equations respectively. ...In the framework of the finite element method (FEM), a prediction method for the heating rate and the skin friction on a body surface is presented by using the energy and momentum conservation equations respectively. Meanwhile, a brief analysis is made of the role the weighted functions play in the present work.展开更多
AlxOy films by DC reactive magnetron sputtering were annealed in air ambient at 500 ℃for 1 h with different heating rates of 5,15,and 25 ℃/min.Then heat treatments at 900 ℃ were carried out on these 500 ℃-annealed...AlxOy films by DC reactive magnetron sputtering were annealed in air ambient at 500 ℃for 1 h with different heating rates of 5,15,and 25 ℃/min.Then heat treatments at 900 ℃ were carried out on these 500 ℃-annealed films to simulate the high-temperature application environment.Effects of the annealing heating rate on structure and properties of both 500 ℃-annealed and 900 ℃-heated films were investigated systematically.It was found that distinct γ-Al2O3 crystallization was observed in the 900 ℃-heated films only when the annealing heating rates are 15 and 25 ℃/min.The 500 ℃-annealed film possessed the most compact surface morphology in the case of 25 ℃/min.The highest microhardness of both 500 ℃-annealed and 900℃-heated films were obtained when the annealing heating rate was 15 ℃/min.展开更多
A rapid-heating method in the absence of electric/magnetic field was achieved by introducing a self-propagating-combustion (SHS) as heating source. The effect of heating rate on the alumina grain growth was explored...A rapid-heating method in the absence of electric/magnetic field was achieved by introducing a self-propagating-combustion (SHS) as heating source. The effect of heating rate on the alumina grain growth was explored based on this rapid-heating method. Comparing with the alumina prepared by two different heating ratios (greater than 1 000 ℃/min in SItS and about 50 ℃/min in common pressureless sintering furnace), it was revealed that the rapid heating could promote the grain growth greatly without pressure during sintering. However, if a pressure was applied simultaneously, the grain growth would be almost completely restrained. Since these observations are quite different from the expectation, a new grain growth model was proposed.展开更多
The relation between the melting point of Portland cement raw meal and its heating rate have been studied. The raw meal was burnt at different heating rate ranging from 10 similar to 900 degrees C/min Dy the following...The relation between the melting point of Portland cement raw meal and its heating rate have been studied. The raw meal was burnt at different heating rate ranging from 10 similar to 900 degrees C/min Dy the following methods: (A) in electric resistance furnace; (B) in DTA-TG analyzer with infrared ray focused heating; (C) in high temperature microscope with electron stream heating. Based on thermal analysis theory and melt theory and the tests above, it is found that melting point T-m of cement raw meal decreases with the increased heating rate Phi during burning in the following relation: T-m=1280-0.107 empty set.展开更多
In the present work,the microstructure,texture,and mechanical properties of a cold-rolled Ti-IF steel,after annealing at different heating rates,have been investigated.The results reveal that the mean grain size is gr...In the present work,the microstructure,texture,and mechanical properties of a cold-rolled Ti-IF steel,after annealing at different heating rates,have been investigated.The results reveal that the mean grain size is gradually refined from 19.2 to 16.3 μ m as the heating rate increases from 4 to 50 ℃/s,but refined only slightly at heating rates of over 50 ℃/s.The recrystallization microstructure has a strong texture,which is a result of the sharpening of the favorable { 111 }//ND (normal direction) texture components or γ-fiber.With increasing heating rates,the peak value off(g) of γ-fiber decreases from 17 to 9.The yield and tensile strengths increase gradually as the heating rate increases from 4 to 50 ℃/s,but remain almost unchanged at heating rates of more than 50 ℃/s.The total elongation and uniform elongation increase gradually as the heating rate increases from 4 to 100 ℃/s,but decreases slowly for heating rates higher than 100 ℃/s.As the heating rate increases from 4 to 100 ℃/s,the plastic strain ratio of the steel decreases from 2.8 to 2.2; however,it increases to 2.9 for heating rates above 100 ℃/s.The strain hardening exponent remains unchanged at 0.27 in all annealing cycles.展开更多
The common problem of cold strip continuous annealing furnaces is high exhaust gas temperature and great energy consumption. Taking the cold-strip continuous annealing furnaces of Baosteel No. 4 cold mill plant as an ...The common problem of cold strip continuous annealing furnaces is high exhaust gas temperature and great energy consumption. Taking the cold-strip continuous annealing furnaces of Baosteel No. 4 cold mill plant as an example, several waste heat recovery systems in the annealing furnaces are compared and their advantages and disadvantages are analyzed through different energy-saving technologies.展开更多
The response and failure of magnesium alloy AZ31 specimens subjected to different pre-loaded-stress levels and heating rates were investigated with a Gleeble-1500 thermo-mechanical material testing system.It is found ...The response and failure of magnesium alloy AZ31 specimens subjected to different pre-loaded-stress levels and heating rates were investigated with a Gleeble-1500 thermo-mechanical material testing system.It is found that the increases of either pre-loaded stresses or heating-rates decrease the failure temperatures of the specimens.The metallographs of the tested specimens were also observed.It is shown that the high heating-rate may cause stronger local thermal inconsistency,which remarkably increases the microdefects and reduces the macroscopic mechanical properties of the material.展开更多
文摘An energy consumption analysis based on the heating characteristic of a building with central heat exchanger in a university of Tianjin was done,and the feasibility of intermittent heating with variable speed pumps was discussed. By comparing various methods of energy consumption analysis,a modified Bin method based on the weather data in Tianjin was adopted. The heat consumption of the buildings under intermittent heating mode was calculated and compared with continuous heating mode,the result shows that intermittent heating can reduce energy consumption for 1 941 759 kW·h,save standard coal for 341 t,and reduce pump power consumption for 72 679 kW·h annually. Intermittent operation by means of varying the pump frequency not only leads to savings in fuel consumption and reduction in pollutant emissions,but also reduces operating costs significantly and it is an ideal energy-saving method. By analyzing the results,the recommendations of heating operation regulation and the transformation of pipe network were proposed separately to different kinds of buildings in colleges,such as laboratory building,teaching building.
文摘Primary and secondary networks are treated as a whole in indirect heating systems, and an advanced new temperature-flow regulation method is presented whose flow ratio is greater than 60% in a secondary network and 30% in a primary network when under a partial load. Through deducing and optimizing an exponential function flow regulation rule, the formulae of flow regulation and the supply and return water temperatures are obtained, and their relevant curves are plotted. After comparison, it is found that this control method has a huge energy conservation space, and it should therefore be generalized soon.
基金funded by the Artificial Intelligence Technology Project of Xi’an Science and Technology Bureau in China(No.21RGZN0014)。
文摘Accurate insight into the heat generation rate(HGR) of lithium-ion batteries(LIBs) is one of key issues for battery management systems to formulate thermal safety warning strategies in advance.For this reason,this paper proposes a novel physics-informed neural network(PINN) approach for HGR estimation of LIBs under various driving conditions.Specifically,a single particle model with thermodynamics(SPMT) is first constructed for extracting the critical physical knowledge related with battery HGR.Subsequently,the surface concentrations of positive and negative electrodes in battery SPMT model are integrated into the bidirectional long short-term memory(BiLSTM) networks as physical information.And combined with other feature variables,a novel PINN approach to achieve HGR estimation of LIBs with higher accuracy is constituted.Additionally,some critical hyperparameters of BiLSTM used in PINN approach are determined through Bayesian optimization algorithm(BOA) and the results of BOA-based BiLSTM are compared with other traditional BiLSTM/LSTM networks.Eventually,combined with the HGR data generated from the validated virtual battery,it is proved that the proposed approach can well predict the battery HGR under the dynamic stress test(DST) and worldwide light vehicles test procedure(WLTP),the mean absolute error under DST is 0.542 kW/m^(3),and the root mean square error under WLTP is1.428 kW/m^(3)at 25℃.Lastly,the investigation results of this paper also show a new perspective in the application of the PINN approach in battery HGR estimation.
基金The authors are grateful for the financial supports from the Science Challenge Project(TZ2018001)the State Key Laboratory of Advanced Metals and Materials University of Science and Technology Beijing,China(2019-Z02)+3 种基金the National Natural Science Foundation of China(52075272)the Key Laboratory of Impact and Safety Engineering,Ministry of Education,Ningbo University,China(CJ201912)the Ningbo Natural Science Foundation,China(2018A610174)the K.C.Wong Magna Fund from Ningbo University,China.
文摘The relationship among heating rate, mechanical properties, microstructure and texture of Al-Mg-Si-Cu alloy during solution treatment was investigated through tensile test, scanning electron microscope, X-ray diffractometer and EBSD technology. The experimental results reveal that there is a non-monotonic relationship among solution heating rate, mechanical properties, microstructure and texture. As the solution heating rate increases, the strength variations are dependent on the tensile direction;work hardening exponent n decreases first, and then increases;plastic strain ratio r increases first, and then decreases, and finally increases. The final microstructure and texture are also affected by heating rate. As heating rate increases, the microstructure transforms from elongated grain structure to equiaxed grain structure, and the average grain size decreases first, and then increases, and decreases finally. Although the texture components including CubeND{001}<310> and P{011}<122> orientations almost have no change with the increase of heating rate, the texture intensity and volume fraction decrease first, and then increase, and finally decrease. Both microstructure and texture evolutions are weakly affected by heating rate. Improving heating rate is not always favorable for the development of fine equiaxed grain structure, weak texture and high average r value, which may be related to the recrystallization behavior.
基金the National Natural Science Foundation of China(No.50945018)
文摘This study introduces a novel method of electric field sintering for preparing NdFeB magnets. NdFeB alloy compacts were all sintered by electric fields for 8 min at 1000~C with different preset heating rates. The characteristics of electric field sintering and the effects of heating rate on the sintering densification of NdFeB alloys were also studied. It is found that electric field sintering is a new non-pressure rapid sintering method for preparing NdFeB magnets with fine grains at a relatively lower sintering temperature and in a shorter sintering time. Using this method, the sintering temperature and process of the compacts can be controlled accurately. When the preset heating rate in- creasing from 5 to 2000~C/s the densification of NdFeB sintered compacts gradHally improves. As the preset heating rate is 2000C/s, Nd-rich phases are small, dispersed and uniformly distributed in the sintered compact, and the magnet has a better microstructure than that made by conventional vacuum sintering. Also, the maximum energy product of the sintered magnet reaches 95% of conventionally vacuum sintered magnets.
文摘Oxide scale formation on a C-steel surface has been investigated using linear heating rates ranging from 0.1℃/min to 10℃/min at high temperatures. The studies on the oxide scale formation at high temperature (650℃) at slower heating rate (0.1℃/min) shows that the kinetic regime is linear. X-ray diffraction measurements revealed that the scale constituents are significantly influenced by the heating rate. The adherence of the scale was improved by using slower heating rate (0.1℃/min-≤650℃), while above such degree the scale was susceptible to cracking and flaking out of the alloy surface. In fact, the development of oxide growth stresses can cause considerable scale cracking. As well, variation of the crystallite sizes under the aforementioned conditions might affect the scale stacking to the alloy surface. The secondary electron detector images of the oxide scale shows that the scale was imperfectly smooth and there were a number of voids and defects in the scale skin, especially at fast heating rate. This observation could be attributed to defects of the as-received alloy. In general, slower heating rate reduced the defects of the scale and improved its adherence.
文摘Indium tin oxide (ITO) films were prepared on polyester, Si and glass substrate with relatively high deposition rate of above 0.9 nm/s by DC reactive magnetron sputtering technique at the sputtering pressure of 0.06 Pa system, respectively. The dependence of resistivity on deposition parameters, such as deposition rate, target-to-substrate distance (TSD), oxygen flow rate and sputtering time (thickness), has been investigated, together with the structural and the optical properties. It was revealed that all ITO films exhibited lattice expansion. The resistivity of ITO thin films shows significant substrate effect: much lower resistivity and broader process window have been reproducibly achieved for the deposition of ITO films onto polyester rather than those prepared on both Si and glass substrates. The films with resistivity of as low as 4.23 x 10^-4 Ω.cm and average transmittance of ~78% at wavelength of 400~700 nm have been achieved for the films on polyester at room temperature.
文摘The influence of heating rate on double reversible transformation in CuZnAlMnNi shape memory alloy was investigated by differential scanning calorimetry. It was found that rapid heating inhibits X -->M transformation but is favorable to the reverse martensite transformation, giving rise to the approach of the two transformation peaks. With the decrease of heating rate, the two transformation peaks separate gradually.
基金Projects(10872221,50621403)supported by the National Natural Science Foundation of China
文摘Effects of temperature and heating rate on the mechanical properties of the tensile specimens of magnesium alloy AZ31 were experimentally investigated using a Gleeble-1500 thermo-mechanical material testing system.The metallurgraphs of the fracture section of the specimens were also experimentally observed and analyzed for exploring their failure mechanism under different temperatures and heating rates.The results show that the higher the temperature,the lower the ultimate strength of the specimens.And the higher the heating rate,the higher the ultimate strength of the specimens.The high temperatures and high heating rates will induce microvoids in the specimens which make the specimens failure under relatively low loads.
基金Funded by the National Natural Science Foundation of China(Nos.51175210 and 51175211)
文摘We investigated the effects of heating rate on the process parameters of superplastic forming for Zr55Cu30Al10Ni5 by differential scanning calorimetry. The continuous heating and isothermal annealing analyses suggested that the temperatures of glass transition and onset crystallization are heating rate-dependent in the supercooled liquid region. Then, the time-temperature-transformation diagram under different heating rates indicates that increasing the heating rate can lead to an increase of the incubation time at the same anneal temperature in the supercooled liquid region. Based on the Arrhenius relationship, we discovered that the incubation time increases by 1.08-1.11 times with double increase of the heating rate at the same anneal temperature, and then verified it by the data of literatures and the experimental results. The obtained curve of the max available incubation time reveals that the incubation time at a certain anneal temperature in the supercooled liquid region is not infinite, and will increase with increasing heating rate until this temperature shifts out of the supercooled liquid region because of exceeding critical heating rate. It is concluded that heating rate must be an important processing parameter of superplastic forming for Zr55Cu30Al10Ni5.
基金supported by the National Natural Science Foundation of China(Grant Nos.40875084and40705012)the National Key Technologies R&D Program of China(Grant No.2008BAC40B00)
文摘The latitude-altitude distributions of radiative fluxes and heating rates are investigated by utilizing CloudSat satellite data over China during summer. The Tibetan Plateau causes the downward shortwave fluxes of the lower atmosphere over central China to be smaller than the fluxes over southern and northern China by generating more clouds. The existence of a larger quantity of clouds over central China reflects a greater amount of solar radiation back into space. The vertical gradients of upward shortwave radiative fluxes in the atmosphere below 8 km are greater than those above 8 km. The latitudinal-altitude distributions of downward longwave radiative fluxes show a slantwise decreasing trend from low latitudes to high latitudes that gradually weaken in the downward direction. The upward longwave radiative fluxes also weaken in the upward direction but with larger gradients. The maximum heating rates by solar radiation and cooling rates by longwave infrared radiation are located over 28 40°N at 7 8 km mean sea level (MSL), and they are larger than the rates in the northern and southern regions. The heating and cooling rates match well both vertically and geographically.
基金Project supported by the National Natural Science Foundation of China(Grant No.50971102)the Specialized Research Fund for the Doctoral Program of Higher Education of China(Grant No.20116102110016)+1 种基金the National Basic Research Program of China(Grant No.2011CB610402)the Fund of the State Key Laboratory of Solidification Processing in Northwestern Polytechnical University,China(Grant No.SKLSP201306)
文摘The effect of the heating rate on the nucleation of metallic glass in a rapid heating process starting from the glass transition temperature is investigated. The critical nucleus radius increases with the increase of the temperature of the undercooling liquid. If the increment rate of the critical nucleus radius, owing to the heating process, is higher than the growth rate of the nuclei, the nuclei generated at the low temperature will become the embryos at the high temperature. This means that the high heating rate can make no nucleation happen in the heating process. In consideration of the interfacial energy, the growth rate of the nuclei increases with the increase of their size and the growth rate of the critical nucleus is zero. Thus, the lower heating rate can also make the nuclei decline partially. Finally, this theory is used to analyze the nucleation process during laser remelting metallic glass.
基金supported by the National Natural Science Foundation of China(No.20504001)
文摘The effects of heating rate on the aggregate behavior of poly(ethylene oxide)-b-poly(N-isopropylacrylamide) in aqueous solutions were investigated in detail by laser light scattering and TEM. By employing two separate heating protocols, step-by-step heating at 〈 5 K/step and one-step jump, to heat the sample from 15℃ to the selected temperature, we found that the heating rate only showed significant effect on the aggregates above the cloud point. The aggregate formed by step-by-step heating exhibited a much larger size and a broader size distribution than those formed by one-step jump heating. Moreover, neither of the aggregates were ideal micellar structures as indicated by the size and the Rg/Rh values. On the contrary, at temperatures below the cloud point where the block copolymer formed core-shelled micelles, the heating rate showed negligible effect on the size and size distribution of the micelles. Since the system underwent a phase separation above the cloud point, the heating rate effect could be reasonably explained by the phase separation mechanisms: the nucleation-and-growth mechanism in the metastable region and the spinodal decomposition mechanism in the unstable region.
基金The project supported by the National Natural Science Foundation of China (19889210)
文摘In the framework of the finite element method (FEM), a prediction method for the heating rate and the skin friction on a body surface is presented by using the energy and momentum conservation equations respectively. Meanwhile, a brief analysis is made of the role the weighted functions play in the present work.
文摘AlxOy films by DC reactive magnetron sputtering were annealed in air ambient at 500 ℃for 1 h with different heating rates of 5,15,and 25 ℃/min.Then heat treatments at 900 ℃ were carried out on these 500 ℃-annealed films to simulate the high-temperature application environment.Effects of the annealing heating rate on structure and properties of both 500 ℃-annealed and 900 ℃-heated films were investigated systematically.It was found that distinct γ-Al2O3 crystallization was observed in the 900 ℃-heated films only when the annealing heating rates are 15 and 25 ℃/min.The 500 ℃-annealed film possessed the most compact surface morphology in the case of 25 ℃/min.The highest microhardness of both 500 ℃-annealed and 900℃-heated films were obtained when the annealing heating rate was 15 ℃/min.
基金Funded by the National Natural Science Foundation of China(No.U12301013)the State Ministry of Science and Technology Innovation Fund(No.0102010DFA52240)
文摘A rapid-heating method in the absence of electric/magnetic field was achieved by introducing a self-propagating-combustion (SHS) as heating source. The effect of heating rate on the alumina grain growth was explored based on this rapid-heating method. Comparing with the alumina prepared by two different heating ratios (greater than 1 000 ℃/min in SItS and about 50 ℃/min in common pressureless sintering furnace), it was revealed that the rapid heating could promote the grain growth greatly without pressure during sintering. However, if a pressure was applied simultaneously, the grain growth would be almost completely restrained. Since these observations are quite different from the expectation, a new grain growth model was proposed.
文摘The relation between the melting point of Portland cement raw meal and its heating rate have been studied. The raw meal was burnt at different heating rate ranging from 10 similar to 900 degrees C/min Dy the following methods: (A) in electric resistance furnace; (B) in DTA-TG analyzer with infrared ray focused heating; (C) in high temperature microscope with electron stream heating. Based on thermal analysis theory and melt theory and the tests above, it is found that melting point T-m of cement raw meal decreases with the increased heating rate Phi during burning in the following relation: T-m=1280-0.107 empty set.
文摘In the present work,the microstructure,texture,and mechanical properties of a cold-rolled Ti-IF steel,after annealing at different heating rates,have been investigated.The results reveal that the mean grain size is gradually refined from 19.2 to 16.3 μ m as the heating rate increases from 4 to 50 ℃/s,but refined only slightly at heating rates of over 50 ℃/s.The recrystallization microstructure has a strong texture,which is a result of the sharpening of the favorable { 111 }//ND (normal direction) texture components or γ-fiber.With increasing heating rates,the peak value off(g) of γ-fiber decreases from 17 to 9.The yield and tensile strengths increase gradually as the heating rate increases from 4 to 50 ℃/s,but remain almost unchanged at heating rates of more than 50 ℃/s.The total elongation and uniform elongation increase gradually as the heating rate increases from 4 to 100 ℃/s,but decreases slowly for heating rates higher than 100 ℃/s.As the heating rate increases from 4 to 100 ℃/s,the plastic strain ratio of the steel decreases from 2.8 to 2.2; however,it increases to 2.9 for heating rates above 100 ℃/s.The strain hardening exponent remains unchanged at 0.27 in all annealing cycles.
文摘The common problem of cold strip continuous annealing furnaces is high exhaust gas temperature and great energy consumption. Taking the cold-strip continuous annealing furnaces of Baosteel No. 4 cold mill plant as an example, several waste heat recovery systems in the annealing furnaces are compared and their advantages and disadvantages are analyzed through different energy-saving technologies.
基金Projects(10872221,50621403)supported by the National Natural Science Foundation of China
文摘The response and failure of magnesium alloy AZ31 specimens subjected to different pre-loaded-stress levels and heating rates were investigated with a Gleeble-1500 thermo-mechanical material testing system.It is found that the increases of either pre-loaded stresses or heating-rates decrease the failure temperatures of the specimens.The metallographs of the tested specimens were also observed.It is shown that the high heating-rate may cause stronger local thermal inconsistency,which remarkably increases the microdefects and reduces the macroscopic mechanical properties of the material.