The fracturing process of sandstone is inherently complex due to its loose internal structure and deformation adaptability.Liquid nitrogen pre-injection has emerged as a promising approach to damage reservoir rocks,ef...The fracturing process of sandstone is inherently complex due to its loose internal structure and deformation adaptability.Liquid nitrogen pre-injection has emerged as a promising approach to damage reservoir rocks,effectively reducing fracture pressure and establishing intricate fracture networks,thus offering a potential solution for reservoir reconstruction.To unravel the fundamental mechanisms governing sandstone fracturing behaviors following liquid nitrogen pre-injection,sandstone fracturing experiments were conducted under varying durations of liquid nitrogen injection,rock temperature,and in-situ stress conditions.The experiments showcased the evolution of injection pressure and fracture characteristics under different testing conditions,complemented by electron microscope analysis to elucidate the factors driving the complex fracture characteristics of sandstone.The findings revealed a significant decrease in fracture pressure after liquid nitrogen pre-injection,accompanied by a notable increase in the complexity of the fracture network and the roughness of the fracture surface.Moreover,prolonging the duration of liquid nitrogen injection and elevating reservoir temperature further contributed to reducing fracture pressure,consequently enhancing fracture complexity and surface roughness.Conversely,the application of confining pressure amplified fracture pressure while intensifying the degree of fracturing.Notably,the investigation highlighted the increased presence of microcracks in sandstone resulting from liquid nitrogen preinjection,facilitating fluid diffusion during fracturing and yielding lower fracture pressures,thereby enhancing the effectiveness of sandstone reservoir reformation.The research results can provide theoretical guidance for geothermal reservoir reconstruction.展开更多
To improve the defense capability of military equipment under extreme conditions,impact-resistant and high-energy-consuming materials have to be developed.The damping characteristic of entangled porous metallic wire m...To improve the defense capability of military equipment under extreme conditions,impact-resistant and high-energy-consuming materials have to be developed.The damping characteristic of entangled porous metallic wire materials(EPMWM)for vibration isolation was previously investigated.In this paper,a study focusing on the impact-resistance of EPMWM with the consideration of ambient temperature is presented.The quasi-static and low-velocity impact mechanical behavior of EPMWM under different temperatures(25℃-300℃)are systematically studied.The results of the static compression test show that the damping energy dissipation of EPMWM increases with temperature while the nonlinear damping characteristics are gradually enhanced.During the impact experiments,the impact energy loss rate of EPMWM was between 65%and 85%,while the temperatures increased from 25℃to 300℃.Moreover,under the same drop impact conditions,the overall deformation of EPMWM decreases in the temperature range of 100℃-200℃.On the other hand,the impact stiffness,energy dissipation,and impact loss factor of EPMWM significantly increase with temperature.This can be attributed to an increase in temperature,which changes the thermal expansion coefficient and contact state of the internal wire helixes.Consequently,the energy dissipation mode(dry friction,air damping,and plastic deformation)of EPMWM is also altered.Therefore,the EPMWM may act as a potential candidate material for superior energy absorption applications.展开更多
Al2O3-r2O03/NiCoCrAIYTa coatings were prepared via atmosphere plasma spraying (APS). The microstructure and phase com- position of the coatings were analyzed by X-ray diffraction (XRD), scanning electron microsco...Al2O3-r2O03/NiCoCrAIYTa coatings were prepared via atmosphere plasma spraying (APS). The microstructure and phase com- position of the coatings were analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM), laser confocal scanning microsco- py (LSCM), and transmission electron microscopy (TEM). The dry frictional wear behavior of the coatings at 500℃ in static air was inves- tigated and compared with that of 0Cr25Ni20 steel. The results show that the coatings comprise the slatted layers of oxide phases, unmelted particles, and pores. The hot abrasive resistance of the coatings is enhanced compared to that of 0Cr25Ni20, and their mass loss is approxi- mately one-fifteenth that of 0Cr25Ni20 steel. The main wear failure mechanisms of the coatings are abrasive wear, fatigue wear, and adhe- sive wear.展开更多
For the purpose of investigating the dynamic deformational behavior and failure mechanisms of magnesium under high strain rates,the Split Hopkinson Pressure Bar(SHPB)was used for investigating dynamic mechanical prope...For the purpose of investigating the dynamic deformational behavior and failure mechanisms of magnesium under high strain rates,the Split Hopkinson Pressure Bar(SHPB)was used for investigating dynamic mechanical properties of extruded Mg-Gd-Y Magnesium alloy at ambient temperature(300 K),200℃(473 K)and 300℃(573 K)temperature.The samples after compression were analyzed by scanning electron microscope(SEM)and metallographic microscope.Dynamic mechanical properties,crack performance and plastic deformation mechanism of extruded Mg-Gd-Y Magnesium alloy along the extrusion direction(ED)were discussed.The results show that,extruded Mg-Gd-Y Magnesium alloy has the largest dynamic compressive strength which is 535 MPa at ambient temperature(300 K)and strain rate of 2826 s^(−1).When temperature increases,dynamic compressive strength decreases,while ductility increases.The dynamic compression fracture mechanism of extruded Mg-Gd-Y Magnesium alloy is multi-crack propagation and intergranular quasi-cleavage fracture at both ambient temperature and high temperature.The dynamic compressive deformation mechanism of extruded Mg-Gd-Y Magnesium alloy is a combination of twinning,slipping and dynamic recrystallization at both ambient temperature and high temperature.展开更多
Based on reanalyzing test results of uniaxial compressive behavior of concrete at constant high temperatures in China, with the compressive cube strength of concrete from 20 to 80 MPa, unified formulas for uniaxial co...Based on reanalyzing test results of uniaxial compressive behavior of concrete at constant high temperatures in China, with the compressive cube strength of concrete from 20 to 80 MPa, unified formulas for uniaxial compressive strength, elastic modulus, strain at peak uniaxial compression and mathematical expression for unaxial compressive stress-strain relations for the concrete at constant high temperatures were studied. Furthermore, the axial stress-axial strain relations between laterally confined concrete under axial compression and multiaxial stress-strain relations for steel at constant high temperatures were studied. Finally, based on continuum mechanics, the mechanics model for concentric cylinders of circular steel tube with concrete core of entire section loaded at constant high temperatures was established. Applying elasto-plastic analysis method, a FORTRAN program was developed, and the concrete-filled circular steel tubular (CFST) stub colunms at constant high temperatures were analyzed. The analysis results are in agreement with the experiment ones from references.展开更多
Ni-based alloy coating on 21-4-N heat-resistant steel was prepared using CO2 laser, and the high-temperature abrasion wear was tested. The microstructure of this cladding layer and its abrasion wear behavior at high t...Ni-based alloy coating on 21-4-N heat-resistant steel was prepared using CO2 laser, and the high-temperature abrasion wear was tested. The microstructure of this cladding layer and its abrasion wear behavior at high temperature by changing compositions and temperatures were investigated by means of optical microscope and scanning electron microscope. Among the three compositions of cladding layer, i.e. Ni21+20%WC+0.5%CeO2, Ni25+20%WC+0.5%CeO2 and Ni60+20%WC+0.5%CeO2, the experimental results show that Ni21+20%WC+ 0.5%CeO2 cladding layer is made up of finer grains, and presents the best abrasion wear behavior at high temperature. The wear pattern of laser cladding layer is mainly grain abrasion at lower temperature, and it would be changed to adhesive abrasion and oxide abrasion at higher temperature.展开更多
Due to the effective precipitation strengthening effect of the β phase, Mg-Gd alloys exhibit excellent room temperature mechanical behaviors. However, when served at high temperatures, the metastable β phase will tr...Due to the effective precipitation strengthening effect of the β phase, Mg-Gd alloys exhibit excellent room temperature mechanical behaviors. However, when served at high temperatures, the metastable β phase will transform to other phases, resulting in severe performance degradation. In this study, we investigated the effect of precipitation state achieved by different heat treatments on high temperature tensile and creep behaviors of the Mg-15Gd alloy by comparing the properties of the as-cast, solid-solutioned(T4) and peak-aged(T6) alloys. The results showed that the tensile mechanical properties of the T6 alloy were always highest from room temperature to 300 ℃, in spite of an abnormal strength increase with temperature existed in the T4 alloy. For tensile creep properties, the T6 alloy exhibited the lowest steady creep rate below 235 ℃ while the T4 alloy possessed the best properties above 260 ℃. Microstructure characterization revealed that the transition was caused by the stress-promoted precipitation of β phase in the T4 alloy and rapid phase transformation in the T6 alloy at high temperatures. At 260 ℃, the calculated stress exponent n was 3.1 and 2.8 for the T4 and T6 alloys, respectively, suggesting the creep deformation mechanism was dislocation slip, which was further confirmed by the microstructure after creeping. Our findings can provide new insights into the heat treatment process of Mg-Gd alloys served at high temperatures.展开更多
Ni-W-P matrix composites containing CeO2 and SiO2 nano-particles were prepared on common carbon steel surface by means of pulse electrodeposition,and the high-temperature oxidation behavior was investigated.The result...Ni-W-P matrix composites containing CeO2 and SiO2 nano-particles were prepared on common carbon steel surface by means of pulse electrodeposition,and the high-temperature oxidation behavior was investigated.The results show that when the oxidation time is controlled in 1 h,oxidation kinetics curve between oxidation mass gain rate and oxidation temperature of CeO2-SiO2/Ni-W-P composites accords with the index increasing law.When the oxidation temperature is controlled at 300℃,the kinetics curve between oxidation mass gain rate and oxidation time accords with the linear increasing law.The composites as-deposited are in the amorphous state and turn into the crystal state at 400℃.The microstructures of oxidation film on the composites will change from the compact state to the loose state with increasing oxidation temperature to 800℃.They are still continuous and compact,and there are no crackle,strip and falling-out.CeO2 and SiO2 nano-particles co-deposited into Ni-W-P alloy can improve the high-temperature oxidation resistance.展开更多
The creep behaviors of Pt-RE alloys have been studied at 1200℃ and 1400℃.The results show that asmall amount of RE elements improves the creep behaviors of platinum greatly.The creep behaviors of PtGd0.5,PtLa0.5 and...The creep behaviors of Pt-RE alloys have been studied at 1200℃ and 1400℃.The results show that asmall amount of RE elements improves the creep behaviors of platinum greatly.The creep behaviors of PtGd0.5,PtLa0.5 and PtLa0.3 Gd0.2,are best among all the alloys studied.As far as the creep behaviors are concerned,the traditional heat-resistance alloy PtGd10 can be replaced by PtGd0.5.Particularly,the properities of PtGd0.5are near to those of PtRb10.For most of the Pt-RE alloys,long-time,static,super high-temperature treatment inair is of no advantage to the creep rupture life.The mechanisms of the effects of rare-earths on high-temperaturecreep properties of platinum are discussed.展开更多
The samples made from a SiC-C/SiC composite were pretreated in AT under creep, fatigue, creep and fatigue interaction, as well as in dry oxygen and wet oxygen under fatigue at 1300℃for 15 hours. The fracture behavior...The samples made from a SiC-C/SiC composite were pretreated in AT under creep, fatigue, creep and fatigue interaction, as well as in dry oxygen and wet oxygen under fatigue at 1300℃for 15 hours. The fracture behaviors of the pretreated samples were investigated at 1300℃. The loading-strain curves and the microstructures of the sample were compared with each other. The various of high temperature tensile behaviors was attributed to the different microstructures resulted from different high temperature pretreatments.展开更多
An aluminum-based in-situ composites reinforced with Mg2Si and Si particles were produced by centrifugal casting A1-20Si-5Mg alloy. The microstructure of the composites was examined, and the effects of temperature on ...An aluminum-based in-situ composites reinforced with Mg2Si and Si particles were produced by centrifugal casting A1-20Si-5Mg alloy. The microstructure of the composites was examined, and the effects of temperature on fracture behavior of the composite were investigated. The results show that the average fraction of primary Si and Mg2Si particles in the composites is as high as 38%, and ultimate tensile strengths (UTS) of the composites first increase then decrease with the increase of test temperature. Microstructures of broken specimens show that both the particle fracture and the interface debonding affect the fracture behavior of the composites, and the interface debonding becomes the dominant fracture mechanism with increasing test temperature. Comparative results indicate that rich particles in the composites and excellent interface strength play great roles in enhancing tensile property by preventing the movement of dislocations.展开更多
The high temperature deformation behaviors of α+β type titanium alloy TC11 (Ti-6.5Al-3.5Mo-1.5Zr-0.3Si) with coarse lamellar starting microstructure were investigated based on the hot compression tests in the tem...The high temperature deformation behaviors of α+β type titanium alloy TC11 (Ti-6.5Al-3.5Mo-1.5Zr-0.3Si) with coarse lamellar starting microstructure were investigated based on the hot compression tests in the temperature range of 950-1100 ℃ and the strain rate range of 0.001-10 s-1. The processing maps at different strains were then constructed based on the dynamic materials model, and the hot compression process parameters and deformation mechanism were optimized and analyzed, respectively. The results show that the processing maps exhibit two domains with a high efficiency of power dissipation and a flow instability domain with a less efficiency of power dissipation. The types of domains were characterized by convergence and divergence of the efficiency of power dissipation, respectively. The convergent domain in a+fl phase field is at the temperature of 950-990 ℃ and the strain rate of 0.001-0.01 s^-1, which correspond to a better hot compression process window of α+β phase field. The peak of efficiency of power dissipation in α+β phase field is at 950 ℃ and 0.001 s 1, which correspond to the best hot compression process parameters of α+β phase field. The convergent domain in β phase field is at the temperature of 1020-1080 ℃ and the strain rate of 0.001-0.1 s^-l, which correspond to a better hot compression process window of β phase field. The peak of efficiency of power dissipation in ℃ phase field occurs at 1050 ℃ over the strain rates from 0.001 s^-1 to 0.01 s^-1, which correspond to the best hot compression process parameters of ,8 phase field. The divergence domain occurs at the strain rates above 0.5 s^-1 and in all the tested temperature range, which correspond to flow instability that is manifested as flow localization and indicated by the flow softening phenomenon in stress-- strain curves. The deformation mechanisms of the optimized hot compression process windows in a+β and β phase fields are identified to be spheroidizing and dynamic recrystallizing controlled by self-diffusion mechanism, respectively. The microstructure observation of the deformed specimens in different domains matches very well with the optimized results.展开更多
Fe-Al-Ta eutectic composites with solidification rates of 6,20,30,80 and 200μm/s were obtained by a modified Bridgman directional solidification technique and alloying.Moreover,tensile property and fracture behavior ...Fe-Al-Ta eutectic composites with solidification rates of 6,20,30,80 and 200μm/s were obtained by a modified Bridgman directional solidification technique and alloying.Moreover,tensile property and fracture behavior of Fe-Al-Ta eutectic composites were studied at 600℃.The relationship between mechanical property and microstructure at high temperature was studied.Microstructure of Fe-Al-Ta eutectic is composed of Fe_(2)Ta(Al)Laves phase and Fe(Al,Ta)matrix phase.In addition,the tensile strength at high temperatures is higher than that at room temperature.The tensile strength is increased with the increase of solidification rate.Moreover,fracture morphology transforms from cleavage fracture to dimple fracture as the solidification rate is increased at high temperatures.展开更多
The oxidation behavior of the Ti-47.5Al-2.5V-1.0Cr-0.2Zr alloy at 900℃ was investigated at different oxidation times(5,20,60 and 100 h).The results show that the total weight gain of the alloy after 100 h at 900℃ ox...The oxidation behavior of the Ti-47.5Al-2.5V-1.0Cr-0.2Zr alloy at 900℃ was investigated at different oxidation times(5,20,60 and 100 h).The results show that the total weight gain of the alloy after 100 h at 900℃ oxidation is 9.1 g·m^(-2),and the oxidation rate decreases with oxidation time.The oxides on the alloy surface are mainly TiO_(2) and Al_(2)O_(3).At the beginning of oxidation(5 h),the oxide film is relatively complete,thin,and the interface between the oxide layer and the matrix is virtually flat.At the end of oxidation(100 h),the thickness of the oxide film is expanded,cracking and spalling occur,and the spalling form is intra-film spalling.At the same time,oxygen is mainly distributed in the oxide film and the oxygen content in the alloy substrate is reduced,confirming that the TiAl alloy has a certain oxidation stability at 900℃.From the outer surface of the oxide layer to the matrix,the TiO_(2) content increases and the Al_(2)O_(3) content decreases.Oxidation proceeds to completion in this system via the dissolution and diffusion of O atom.展开更多
The microstructure and its effects on the high temperature mechanical behavior of Cu-2.7%Al_2O_3 (volume fraction) dispersion strengthened copper (ADSC) alloy were investigated. The results indicate that fine alum...The microstructure and its effects on the high temperature mechanical behavior of Cu-2.7%Al_2O_3 (volume fraction) dispersion strengthened copper (ADSC) alloy were investigated. The results indicate that fine alumina particles are uniformly distributed in the copper matrix, while a few coarse ones are distributed on the grain boundaries. Tensile tests results show that Hall-Petch mechanism is the main contribution to the yield strength of ADSC alloy at room temperature. Its high temperature strength is attributed to the strong pinning effects of alumina particles on the grain and sub-grain boundaries with dislocations. The ultimate tensile strength can reach 237 MPa and the corresponding yield strength reaches 226 MPa at 700℃. Tensile fracture morphology indicates that the ADSC alloy shows brittleness at elevated temperatures. Creep tests results demonstrate that the steady state creep rates at 400 ℃ are lower than those at 700 ℃. The stress exponents at 400 ℃ and 700℃ are 7 and 5, respectively, and the creep strain rates of the ADSC alloy are controlled by dislocation core diffusion and lattice diffusion.展开更多
To maintain tight control over rheological properties of high-density water-based drilling fluids, it is essential to understand the factors influencing the theology of water-based drilling fluids. This paper examines...To maintain tight control over rheological properties of high-density water-based drilling fluids, it is essential to understand the factors influencing the theology of water-based drilling fluids. This paper examines temperature effects on the rheological properties of two types of high-density water-based drilling fluids (fresh water-based and brine-based) under high temperature and high pressure (HTHP) with a Fann 50SL rheometer. On the basis of the water-based drilling fluid systems formulated in laboratory, this paper mainly describes the influences of different types and concentration of clay, the content of a colloid stabilizer named GHJ-1 and fluid density on the rheological parameters such as viscosity and shear stress. In addition, the effects of aging temperature and aging time of the drilling fluid on these parameters were also examined. Clay content and proportions for different densities of brine-based fluids were recommended to effectively regulate the rheological properties. Four theological models, the Bingham, power law, Casson and H-B models, were employed to fit the rheological parameters. It turns out that the H-B model was the best one to describe the rheological properties of the high-density drilling fluid under HTHP conditions and power law model produced the worst fit. In addition, a new mathematical model that describes the apparent viscosity as a function of temperature and pressure was established and has been applied on site.展开更多
Coal is a common porous sedimentary rock whose microstructure and mechanical behavior are often affected by high temperature.In order to deeply investigate the effect of high temperature on the structure and mechanica...Coal is a common porous sedimentary rock whose microstructure and mechanical behavior are often affected by high temperature.In order to deeply investigate the effect of high temperature on the structure and mechanical properties of coal,six groups of coal samples with different heating temperatures were prepared.Various testing methods,including ultrasonic test,scanning electron microscopy,nuclear magnetic resonance and uniaxial compression test,were used in this study.The results showed that the physical and chemical change processes of coal samples under high temperature can be divided into two stages:the stage of drying and degassing and the stage of pyrolysis of the coal matrix.With the increase of heating temperature,the total porosity of coal samples increases,while the integrity and the deformation resistance of coal samples decrease.In addition,the elastic modulus and uniaxial compressive strength of the coal sample decrease with the increase of heating temperature.The Poisson’s ratio decreases firstly and then increases with the increase of heating temperature.展开更多
Extreme high temperature(EHT)events are among the most impact-related consequences related to climate change,especially for China,a nation with a large population that is vulnerable to the climate warming.Based on the...Extreme high temperature(EHT)events are among the most impact-related consequences related to climate change,especially for China,a nation with a large population that is vulnerable to the climate warming.Based on the latest Coupled Model Intercomparison Project Phase 6(CMIP6),this study assesses future EHT changes across China at five specific global warming thresholds(1.5℃-5℃).The results indicate that global mean temperature will increase by 1.5℃/2℃ before 2030/2050 relative to pre-industrial levels(1861-1900)under three future scenarios(SSP1-2.6,SSP2-4.5,and SSP5-8.5),and warming will occur faster under SSP5-8.5 compared to SSP1-2.6 and SSP2-4.5.Under SSP5-8.5,global warming will eventually exceed 5℃ by 2100,while under SSP1-2.6,it will stabilize around 2℃ after 2050.In China,most of the areas where warming exceeds global average levels will be located in Tibet and northern China(Northwest China,North China and Northeast China),covering 50%-70%of the country.Furthermore,about 0.19-0.44 billion people(accounting for 16%-41%of the national population)will experience warming above the global average.Compared to present-day(1995-2014),the warmest day(TXx)will increase most notably in northern China,while the number of warm days(TX90p)and warm spell duration indicator(WSDI)will increase most profoundly in southern China.For example,relative to the present-day,TXx will increase by 1℃-5℃ in northern China,and TX90p(WSDI)will increase by 25-150(10-80)days in southern China at 1.5℃-5℃ global warming.Compared to 2℃-5℃,limiting global warming to 1.5℃ will help avoid about 36%-87%of the EHT increases in China.展开更多
The AA6061-10 wt.%B4 C mono composite, AA6061-10 wt.%B4 C-Gr(Gr: graphite) hybrid composites containing 2.5, 5, and 7.5 wt.% Gr particles, and AA6061-10 wt.%B4 C-Mo S2 hybrid composites containing 2.5, 5, and 7.5 wt.%...The AA6061-10 wt.%B4 C mono composite, AA6061-10 wt.%B4 C-Gr(Gr: graphite) hybrid composites containing 2.5, 5, and 7.5 wt.% Gr particles, and AA6061-10 wt.%B4 C-Mo S2 hybrid composites containing 2.5, 5, and 7.5 wt.% Mo S2 particles were fabricated through stir casting. The dry sliding tribological behaviors of the mono composite and hybrid composites were studied as a function of temperature on high temperature pin-on-disc tribotester against EN 31 counterface. The wear rate and friction coefficient of the Gr-reinforced and Mo S2-reinforced hybrid composites decreased in the temperature range of 30-100 ℃ due to the combined lubrication offered by the wear protective layer and its solid lubricant phase. Scanning electron microscopy(SEM) observation of the worn pin surface revealed severe adhesion, delamination, and abrasion wear mechanisms at temperatures of 150, 200, and 250 ℃, respectively. At 150 ℃, transmission electron microscopy(TEM) observation of the hybrid composites revealed the formation of deformation bands due to severe plastic deformation and fine crystalline structure due to dynamic recrystallization.展开更多
The interfacial behavior of sulfur and yttrium in the yttrium modified Ni 3Al based alloy IC6 during oxidation at 1100 ℃ was analyzed by X ray line scan of electron probe microstructural analysis(EPMA). The resul...The interfacial behavior of sulfur and yttrium in the yttrium modified Ni 3Al based alloy IC6 during oxidation at 1100 ℃ was analyzed by X ray line scan of electron probe microstructural analysis(EPMA). The results show that the migration and segregation of sulfur to the interface between oxide scale and the substrate at high temperature is retarded owing to the presence of yttrium. This is attributed to the desulfurization by yttrium in the melt and the trapping of sulfur by yttrium rich phases during oxidation, which leads to improving the coherence between oxide scale and substrate. Another reason of increasing the high temperature oxidation resistance of alloy IC6 by the addition of yttrium is that yttrium migrates to the grain boundaries of oxides during oxidation and hence improve their strength. This results in the transformation of the oxide scale spallation cracks from intergranular cracks for alloy without yttrium to transgranular ones for yttrium modified alloy.展开更多
基金supported by the National Key R&D Program of China(2022YFE0128300).
文摘The fracturing process of sandstone is inherently complex due to its loose internal structure and deformation adaptability.Liquid nitrogen pre-injection has emerged as a promising approach to damage reservoir rocks,effectively reducing fracture pressure and establishing intricate fracture networks,thus offering a potential solution for reservoir reconstruction.To unravel the fundamental mechanisms governing sandstone fracturing behaviors following liquid nitrogen pre-injection,sandstone fracturing experiments were conducted under varying durations of liquid nitrogen injection,rock temperature,and in-situ stress conditions.The experiments showcased the evolution of injection pressure and fracture characteristics under different testing conditions,complemented by electron microscope analysis to elucidate the factors driving the complex fracture characteristics of sandstone.The findings revealed a significant decrease in fracture pressure after liquid nitrogen pre-injection,accompanied by a notable increase in the complexity of the fracture network and the roughness of the fracture surface.Moreover,prolonging the duration of liquid nitrogen injection and elevating reservoir temperature further contributed to reducing fracture pressure,consequently enhancing fracture complexity and surface roughness.Conversely,the application of confining pressure amplified fracture pressure while intensifying the degree of fracturing.Notably,the investigation highlighted the increased presence of microcracks in sandstone resulting from liquid nitrogen preinjection,facilitating fluid diffusion during fracturing and yielding lower fracture pressures,thereby enhancing the effectiveness of sandstone reservoir reformation.The research results can provide theoretical guidance for geothermal reservoir reconstruction.
基金supported by the National Natural Science Foundation of China(grant number 51805086)the Natural Science Foundation of Fujian Province,China(grant number 2018J01763)。
文摘To improve the defense capability of military equipment under extreme conditions,impact-resistant and high-energy-consuming materials have to be developed.The damping characteristic of entangled porous metallic wire materials(EPMWM)for vibration isolation was previously investigated.In this paper,a study focusing on the impact-resistance of EPMWM with the consideration of ambient temperature is presented.The quasi-static and low-velocity impact mechanical behavior of EPMWM under different temperatures(25℃-300℃)are systematically studied.The results of the static compression test show that the damping energy dissipation of EPMWM increases with temperature while the nonlinear damping characteristics are gradually enhanced.During the impact experiments,the impact energy loss rate of EPMWM was between 65%and 85%,while the temperatures increased from 25℃to 300℃.Moreover,under the same drop impact conditions,the overall deformation of EPMWM decreases in the temperature range of 100℃-200℃.On the other hand,the impact stiffness,energy dissipation,and impact loss factor of EPMWM significantly increase with temperature.This can be attributed to an increase in temperature,which changes the thermal expansion coefficient and contact state of the internal wire helixes.Consequently,the energy dissipation mode(dry friction,air damping,and plastic deformation)of EPMWM is also altered.Therefore,the EPMWM may act as a potential candidate material for superior energy absorption applications.
基金financially supported by the National High-tech Research and Development Program of China(No.2012AA03A513)the Fundamental Research Funds for the Central Universities(No.N140204001)the National Natural Science Foundation of China(Nos.51371044 and 51301037)
文摘Al2O3-r2O03/NiCoCrAIYTa coatings were prepared via atmosphere plasma spraying (APS). The microstructure and phase com- position of the coatings were analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM), laser confocal scanning microsco- py (LSCM), and transmission electron microscopy (TEM). The dry frictional wear behavior of the coatings at 500℃ in static air was inves- tigated and compared with that of 0Cr25Ni20 steel. The results show that the coatings comprise the slatted layers of oxide phases, unmelted particles, and pores. The hot abrasive resistance of the coatings is enhanced compared to that of 0Cr25Ni20, and their mass loss is approxi- mately one-fifteenth that of 0Cr25Ni20 steel. The main wear failure mechanisms of the coatings are abrasive wear, fatigue wear, and adhe- sive wear.
基金The authors would like to acknowledge the financial support from the National Key Basic Research Program(973 Program),Project(2013CB632205).
文摘For the purpose of investigating the dynamic deformational behavior and failure mechanisms of magnesium under high strain rates,the Split Hopkinson Pressure Bar(SHPB)was used for investigating dynamic mechanical properties of extruded Mg-Gd-Y Magnesium alloy at ambient temperature(300 K),200℃(473 K)and 300℃(573 K)temperature.The samples after compression were analyzed by scanning electron microscope(SEM)and metallographic microscope.Dynamic mechanical properties,crack performance and plastic deformation mechanism of extruded Mg-Gd-Y Magnesium alloy along the extrusion direction(ED)were discussed.The results show that,extruded Mg-Gd-Y Magnesium alloy has the largest dynamic compressive strength which is 535 MPa at ambient temperature(300 K)and strain rate of 2826 s^(−1).When temperature increases,dynamic compressive strength decreases,while ductility increases.The dynamic compression fracture mechanism of extruded Mg-Gd-Y Magnesium alloy is multi-crack propagation and intergranular quasi-cleavage fracture at both ambient temperature and high temperature.The dynamic compressive deformation mechanism of extruded Mg-Gd-Y Magnesium alloy is a combination of twinning,slipping and dynamic recrystallization at both ambient temperature and high temperature.
基金Projects(50438020 50578162) supported by the National Natural Sceince Foundation of China
文摘Based on reanalyzing test results of uniaxial compressive behavior of concrete at constant high temperatures in China, with the compressive cube strength of concrete from 20 to 80 MPa, unified formulas for uniaxial compressive strength, elastic modulus, strain at peak uniaxial compression and mathematical expression for unaxial compressive stress-strain relations for the concrete at constant high temperatures were studied. Furthermore, the axial stress-axial strain relations between laterally confined concrete under axial compression and multiaxial stress-strain relations for steel at constant high temperatures were studied. Finally, based on continuum mechanics, the mechanics model for concentric cylinders of circular steel tube with concrete core of entire section loaded at constant high temperatures was established. Applying elasto-plastic analysis method, a FORTRAN program was developed, and the concrete-filled circular steel tubular (CFST) stub colunms at constant high temperatures were analyzed. The analysis results are in agreement with the experiment ones from references.
文摘Ni-based alloy coating on 21-4-N heat-resistant steel was prepared using CO2 laser, and the high-temperature abrasion wear was tested. The microstructure of this cladding layer and its abrasion wear behavior at high temperature by changing compositions and temperatures were investigated by means of optical microscope and scanning electron microscope. Among the three compositions of cladding layer, i.e. Ni21+20%WC+0.5%CeO2, Ni25+20%WC+0.5%CeO2 and Ni60+20%WC+0.5%CeO2, the experimental results show that Ni21+20%WC+ 0.5%CeO2 cladding layer is made up of finer grains, and presents the best abrasion wear behavior at high temperature. The wear pattern of laser cladding layer is mainly grain abrasion at lower temperature, and it would be changed to adhesive abrasion and oxide abrasion at higher temperature.
基金supported by the National Natural Science Foundation of China (Grant No. 51771152)the National Key Research and Development Program of China (Grant No. 2018YFB1106800)。
文摘Due to the effective precipitation strengthening effect of the β phase, Mg-Gd alloys exhibit excellent room temperature mechanical behaviors. However, when served at high temperatures, the metastable β phase will transform to other phases, resulting in severe performance degradation. In this study, we investigated the effect of precipitation state achieved by different heat treatments on high temperature tensile and creep behaviors of the Mg-15Gd alloy by comparing the properties of the as-cast, solid-solutioned(T4) and peak-aged(T6) alloys. The results showed that the tensile mechanical properties of the T6 alloy were always highest from room temperature to 300 ℃, in spite of an abnormal strength increase with temperature existed in the T4 alloy. For tensile creep properties, the T6 alloy exhibited the lowest steady creep rate below 235 ℃ while the T4 alloy possessed the best properties above 260 ℃. Microstructure characterization revealed that the transition was caused by the stress-promoted precipitation of β phase in the T4 alloy and rapid phase transformation in the T6 alloy at high temperatures. At 260 ℃, the calculated stress exponent n was 3.1 and 2.8 for the T4 and T6 alloys, respectively, suggesting the creep deformation mechanism was dislocation slip, which was further confirmed by the microstructure after creeping. Our findings can provide new insights into the heat treatment process of Mg-Gd alloys served at high temperatures.
基金Project(20806035)supported by the National Natural Science Foundation of ChinaProject(2007E187M)supported by the Applied Basic Research Plans Program of Yunnan Province,China+2 种基金Project supported by the Foundation for Leaders of Disciplines in Science and Technology of Yunnan Province,ChinaProject(08C0025)supported by the Scientific Research Fund of Yunnan Provincial Education Department,ChinaProject supported by the Training Foundation for Talents of Kunming University of Science and Technology,China
文摘Ni-W-P matrix composites containing CeO2 and SiO2 nano-particles were prepared on common carbon steel surface by means of pulse electrodeposition,and the high-temperature oxidation behavior was investigated.The results show that when the oxidation time is controlled in 1 h,oxidation kinetics curve between oxidation mass gain rate and oxidation temperature of CeO2-SiO2/Ni-W-P composites accords with the index increasing law.When the oxidation temperature is controlled at 300℃,the kinetics curve between oxidation mass gain rate and oxidation time accords with the linear increasing law.The composites as-deposited are in the amorphous state and turn into the crystal state at 400℃.The microstructures of oxidation film on the composites will change from the compact state to the loose state with increasing oxidation temperature to 800℃.They are still continuous and compact,and there are no crackle,strip and falling-out.CeO2 and SiO2 nano-particles co-deposited into Ni-W-P alloy can improve the high-temperature oxidation resistance.
文摘The creep behaviors of Pt-RE alloys have been studied at 1200℃ and 1400℃.The results show that asmall amount of RE elements improves the creep behaviors of platinum greatly.The creep behaviors of PtGd0.5,PtLa0.5 and PtLa0.3 Gd0.2,are best among all the alloys studied.As far as the creep behaviors are concerned,the traditional heat-resistance alloy PtGd10 can be replaced by PtGd0.5.Particularly,the properities of PtGd0.5are near to those of PtRb10.For most of the Pt-RE alloys,long-time,static,super high-temperature treatment inair is of no advantage to the creep rupture life.The mechanisms of the effects of rare-earths on high-temperaturecreep properties of platinum are discussed.
基金supported by the Chinese Defence Foundation for Science(No.51303)
文摘The samples made from a SiC-C/SiC composite were pretreated in AT under creep, fatigue, creep and fatigue interaction, as well as in dry oxygen and wet oxygen under fatigue at 1300℃for 15 hours. The fracture behaviors of the pretreated samples were investigated at 1300℃. The loading-strain curves and the microstructures of the sample were compared with each other. The various of high temperature tensile behaviors was attributed to the different microstructures resulted from different high temperature pretreatments.
基金Project(51174244) supported by the National Natural Science Foundation of ChinaProject(CDJZR11130005) supported by the Fundamental Research Funds for the Central Universities,China
文摘An aluminum-based in-situ composites reinforced with Mg2Si and Si particles were produced by centrifugal casting A1-20Si-5Mg alloy. The microstructure of the composites was examined, and the effects of temperature on fracture behavior of the composite were investigated. The results show that the average fraction of primary Si and Mg2Si particles in the composites is as high as 38%, and ultimate tensile strengths (UTS) of the composites first increase then decrease with the increase of test temperature. Microstructures of broken specimens show that both the particle fracture and the interface debonding affect the fracture behavior of the composites, and the interface debonding becomes the dominant fracture mechanism with increasing test temperature. Comparative results indicate that rich particles in the composites and excellent interface strength play great roles in enhancing tensile property by preventing the movement of dislocations.
基金Project (51005112) supported by the National Natural Science Foundation of ChinaProject (2010ZF56019) supported by the Aviation Science Foundation of China+1 种基金Project (GJJ11156) supported by the Education Commission of Jiangxi Province, ChinaProject(GF200901008) supported by the Open Fund of National Defense Key Disciplines Laboratory of Light Alloy Processing Science and Technology, China
文摘The high temperature deformation behaviors of α+β type titanium alloy TC11 (Ti-6.5Al-3.5Mo-1.5Zr-0.3Si) with coarse lamellar starting microstructure were investigated based on the hot compression tests in the temperature range of 950-1100 ℃ and the strain rate range of 0.001-10 s-1. The processing maps at different strains were then constructed based on the dynamic materials model, and the hot compression process parameters and deformation mechanism were optimized and analyzed, respectively. The results show that the processing maps exhibit two domains with a high efficiency of power dissipation and a flow instability domain with a less efficiency of power dissipation. The types of domains were characterized by convergence and divergence of the efficiency of power dissipation, respectively. The convergent domain in a+fl phase field is at the temperature of 950-990 ℃ and the strain rate of 0.001-0.01 s^-1, which correspond to a better hot compression process window of α+β phase field. The peak of efficiency of power dissipation in α+β phase field is at 950 ℃ and 0.001 s 1, which correspond to the best hot compression process parameters of α+β phase field. The convergent domain in β phase field is at the temperature of 1020-1080 ℃ and the strain rate of 0.001-0.1 s^-l, which correspond to a better hot compression process window of β phase field. The peak of efficiency of power dissipation in ℃ phase field occurs at 1050 ℃ over the strain rates from 0.001 s^-1 to 0.01 s^-1, which correspond to the best hot compression process parameters of ,8 phase field. The divergence domain occurs at the strain rates above 0.5 s^-1 and in all the tested temperature range, which correspond to flow instability that is manifested as flow localization and indicated by the flow softening phenomenon in stress-- strain curves. The deformation mechanisms of the optimized hot compression process windows in a+β and β phase fields are identified to be spheroidizing and dynamic recrystallizing controlled by self-diffusion mechanism, respectively. The microstructure observation of the deformed specimens in different domains matches very well with the optimized results.
基金Funded by National Natural Science Foundation of China(No.51201121)Key Industry Innovation Chain(group)Project of Shaanxi Province(No.2019ZDLGY 04-04)+1 种基金International Cooperation Project of Key R&D Program in Shaanxi Province(No.2020KW-033)Industrialization Project of Shaanxi Provincial Department of Education(No.20JC024)
文摘Fe-Al-Ta eutectic composites with solidification rates of 6,20,30,80 and 200μm/s were obtained by a modified Bridgman directional solidification technique and alloying.Moreover,tensile property and fracture behavior of Fe-Al-Ta eutectic composites were studied at 600℃.The relationship between mechanical property and microstructure at high temperature was studied.Microstructure of Fe-Al-Ta eutectic is composed of Fe_(2)Ta(Al)Laves phase and Fe(Al,Ta)matrix phase.In addition,the tensile strength at high temperatures is higher than that at room temperature.The tensile strength is increased with the increase of solidification rate.Moreover,fracture morphology transforms from cleavage fracture to dimple fracture as the solidification rate is increased at high temperatures.
基金financially supported by the National Natural Science Foundation of China (51805335)
文摘The oxidation behavior of the Ti-47.5Al-2.5V-1.0Cr-0.2Zr alloy at 900℃ was investigated at different oxidation times(5,20,60 and 100 h).The results show that the total weight gain of the alloy after 100 h at 900℃ oxidation is 9.1 g·m^(-2),and the oxidation rate decreases with oxidation time.The oxides on the alloy surface are mainly TiO_(2) and Al_(2)O_(3).At the beginning of oxidation(5 h),the oxide film is relatively complete,thin,and the interface between the oxide layer and the matrix is virtually flat.At the end of oxidation(100 h),the thickness of the oxide film is expanded,cracking and spalling occur,and the spalling form is intra-film spalling.At the same time,oxygen is mainly distributed in the oxide film and the oxygen content in the alloy substrate is reduced,confirming that the TiAl alloy has a certain oxidation stability at 900℃.From the outer surface of the oxide layer to the matrix,the TiO_(2) content increases and the Al_(2)O_(3) content decreases.Oxidation proceeds to completion in this system via the dissolution and diffusion of O atom.
基金Project(51271203)supported by the National Natural Science Foundation of Chinathe PPP project between the CSC(China Scholarship Council)and the DAAD(German Academic Exchange Service)+2 种基金Project(11JJ2025)supported by Hunan Provincial Natural Science Foundation of ChinaProject(YSZN2013CL06)supported by the Nonferrous Metals Science Foundation of HNG-CSUProject supported by the Aid program for Science Technology Innovative Research Team in Higher Educational Institutions of Hunan Province,China
文摘The microstructure and its effects on the high temperature mechanical behavior of Cu-2.7%Al_2O_3 (volume fraction) dispersion strengthened copper (ADSC) alloy were investigated. The results indicate that fine alumina particles are uniformly distributed in the copper matrix, while a few coarse ones are distributed on the grain boundaries. Tensile tests results show that Hall-Petch mechanism is the main contribution to the yield strength of ADSC alloy at room temperature. Its high temperature strength is attributed to the strong pinning effects of alumina particles on the grain and sub-grain boundaries with dislocations. The ultimate tensile strength can reach 237 MPa and the corresponding yield strength reaches 226 MPa at 700℃. Tensile fracture morphology indicates that the ADSC alloy shows brittleness at elevated temperatures. Creep tests results demonstrate that the steady state creep rates at 400 ℃ are lower than those at 700 ℃. The stress exponents at 400 ℃ and 700℃ are 7 and 5, respectively, and the creep strain rates of the ADSC alloy are controlled by dislocation core diffusion and lattice diffusion.
文摘To maintain tight control over rheological properties of high-density water-based drilling fluids, it is essential to understand the factors influencing the theology of water-based drilling fluids. This paper examines temperature effects on the rheological properties of two types of high-density water-based drilling fluids (fresh water-based and brine-based) under high temperature and high pressure (HTHP) with a Fann 50SL rheometer. On the basis of the water-based drilling fluid systems formulated in laboratory, this paper mainly describes the influences of different types and concentration of clay, the content of a colloid stabilizer named GHJ-1 and fluid density on the rheological parameters such as viscosity and shear stress. In addition, the effects of aging temperature and aging time of the drilling fluid on these parameters were also examined. Clay content and proportions for different densities of brine-based fluids were recommended to effectively regulate the rheological properties. Four theological models, the Bingham, power law, Casson and H-B models, were employed to fit the rheological parameters. It turns out that the H-B model was the best one to describe the rheological properties of the high-density drilling fluid under HTHP conditions and power law model produced the worst fit. In addition, a new mathematical model that describes the apparent viscosity as a function of temperature and pressure was established and has been applied on site.
基金supported by the Natural Science Research Project of the Education Department of Henan Province(No.2010A44002)the National Natural Science Foundation of China(No.51904101)Open Research Fund Program of Key Laboratory of Metallogenic Prediction of Nonferrous Metals and Geological Environment Monitoring(Central South University),Ministry of Education(No.2017YSJS14).
文摘Coal is a common porous sedimentary rock whose microstructure and mechanical behavior are often affected by high temperature.In order to deeply investigate the effect of high temperature on the structure and mechanical properties of coal,six groups of coal samples with different heating temperatures were prepared.Various testing methods,including ultrasonic test,scanning electron microscopy,nuclear magnetic resonance and uniaxial compression test,were used in this study.The results showed that the physical and chemical change processes of coal samples under high temperature can be divided into two stages:the stage of drying and degassing and the stage of pyrolysis of the coal matrix.With the increase of heating temperature,the total porosity of coal samples increases,while the integrity and the deformation resistance of coal samples decrease.In addition,the elastic modulus and uniaxial compressive strength of the coal sample decrease with the increase of heating temperature.The Poisson’s ratio decreases firstly and then increases with the increase of heating temperature.
基金supported by the National Key Research and Development Program of China(2017YFA0603804)the National Natural Science Foundation of China(41831174 and 41430528)+1 种基金the Postgraduate Research&Practice Innovation Program of Jiangsu Province(KYCX19_1026)Guwei ZHANG was supported by the China Scholarship Council(NO.201908320503)。
文摘Extreme high temperature(EHT)events are among the most impact-related consequences related to climate change,especially for China,a nation with a large population that is vulnerable to the climate warming.Based on the latest Coupled Model Intercomparison Project Phase 6(CMIP6),this study assesses future EHT changes across China at five specific global warming thresholds(1.5℃-5℃).The results indicate that global mean temperature will increase by 1.5℃/2℃ before 2030/2050 relative to pre-industrial levels(1861-1900)under three future scenarios(SSP1-2.6,SSP2-4.5,and SSP5-8.5),and warming will occur faster under SSP5-8.5 compared to SSP1-2.6 and SSP2-4.5.Under SSP5-8.5,global warming will eventually exceed 5℃ by 2100,while under SSP1-2.6,it will stabilize around 2℃ after 2050.In China,most of the areas where warming exceeds global average levels will be located in Tibet and northern China(Northwest China,North China and Northeast China),covering 50%-70%of the country.Furthermore,about 0.19-0.44 billion people(accounting for 16%-41%of the national population)will experience warming above the global average.Compared to present-day(1995-2014),the warmest day(TXx)will increase most notably in northern China,while the number of warm days(TX90p)and warm spell duration indicator(WSDI)will increase most profoundly in southern China.For example,relative to the present-day,TXx will increase by 1℃-5℃ in northern China,and TX90p(WSDI)will increase by 25-150(10-80)days in southern China at 1.5℃-5℃ global warming.Compared to 2℃-5℃,limiting global warming to 1.5℃ will help avoid about 36%-87%of the EHT increases in China.
文摘The AA6061-10 wt.%B4 C mono composite, AA6061-10 wt.%B4 C-Gr(Gr: graphite) hybrid composites containing 2.5, 5, and 7.5 wt.% Gr particles, and AA6061-10 wt.%B4 C-Mo S2 hybrid composites containing 2.5, 5, and 7.5 wt.% Mo S2 particles were fabricated through stir casting. The dry sliding tribological behaviors of the mono composite and hybrid composites were studied as a function of temperature on high temperature pin-on-disc tribotester against EN 31 counterface. The wear rate and friction coefficient of the Gr-reinforced and Mo S2-reinforced hybrid composites decreased in the temperature range of 30-100 ℃ due to the combined lubrication offered by the wear protective layer and its solid lubricant phase. Scanning electron microscopy(SEM) observation of the worn pin surface revealed severe adhesion, delamination, and abrasion wear mechanisms at temperatures of 150, 200, and 250 ℃, respectively. At 150 ℃, transmission electron microscopy(TEM) observation of the hybrid composites revealed the formation of deformation bands due to severe plastic deformation and fine crystalline structure due to dynamic recrystallization.
文摘The interfacial behavior of sulfur and yttrium in the yttrium modified Ni 3Al based alloy IC6 during oxidation at 1100 ℃ was analyzed by X ray line scan of electron probe microstructural analysis(EPMA). The results show that the migration and segregation of sulfur to the interface between oxide scale and the substrate at high temperature is retarded owing to the presence of yttrium. This is attributed to the desulfurization by yttrium in the melt and the trapping of sulfur by yttrium rich phases during oxidation, which leads to improving the coherence between oxide scale and substrate. Another reason of increasing the high temperature oxidation resistance of alloy IC6 by the addition of yttrium is that yttrium migrates to the grain boundaries of oxides during oxidation and hence improve their strength. This results in the transformation of the oxide scale spallation cracks from intergranular cracks for alloy without yttrium to transgranular ones for yttrium modified alloy.