The 304 stainless steel with nanostructured surface layer was successfully obtained by using the high-energy shot peening (HESP) method. The internal friction and Young's modulus of this kind of surface nanocrysta...The 304 stainless steel with nanostructured surface layer was successfully obtained by using the high-energy shot peening (HESP) method. The internal friction and Young's modulus of this kind of surface nanocrystallized material were dynamically measured by means of the vibrating reed apparatus. The results implied that different treatment time could induce different microstructure and distribution characteristic of defects in this kind of materials. It is also demonstrated that there is a transition layer between the nano-layer on surface and the coarse grain region inside. The transition layer obviously has certain influence on the overall mechanical properties.展开更多
A nanostructured surface layer was fabricated on a AZ91D magnesium alloy by using a high-energy shot peening(HESP).HESP induced structure along the depth of the treated sample surface layer was characterized by means ...A nanostructured surface layer was fabricated on a AZ91D magnesium alloy by using a high-energy shot peening(HESP).HESP induced structure along the depth of the treated sample surface layer was characterized by means of X-ray diffractometer (XRD),transmission electron microscope(TEM) and high resolution transmission electron microscope(HRTEM).The experimental results show that a deformed layer of about 50 μm has formed after HESP treatment and the average grain size increases from about 40 nm in the surface layer to about 200 nm at the depth of 40 μm.The surface nanocrystallization can realize intercoordination of the dislocations slipping and dynamic recrystallization.The nanocrystalline grains have stacking faults and dislocation in their interiors.The microhardness of the top surface is about triplicate that of the coarse-grained matrix.展开更多
Isothermal and isochronal annealing was conducted to study the thermal stability of the nanocrystalline in the surface layer of Mg alloy AZ91D induced by high-energy shot peening(HESP) .Field emission scanning electro...Isothermal and isochronal annealing was conducted to study the thermal stability of the nanocrystalline in the surface layer of Mg alloy AZ91D induced by high-energy shot peening(HESP) .Field emission scanning electron microscope(FESEM) and X-ray diffractometer were used to characterize the microstructure.Results showed that nanocrystalline produced by HESP on the surface layer of the magnesium alloy AZ91D was 60-70 nm on average.The nanocrystalline could remain stable at about 100℃,and grew up slowly between 100℃ and 200℃.When the annealing temperature reached 300℃,the growth rate of the nanocrystalline increased significantly.The kinetic coefficient n of the nanocrystalline growth was calculated to be 2-3 and the grain growth activation energy Q=39.7 kJ/mol,far less than the self-diffusion activation energy of magnesium atoms in the coarse polycrystalline material.展开更多
文摘The 304 stainless steel with nanostructured surface layer was successfully obtained by using the high-energy shot peening (HESP) method. The internal friction and Young's modulus of this kind of surface nanocrystallized material were dynamically measured by means of the vibrating reed apparatus. The results implied that different treatment time could induce different microstructure and distribution characteristic of defects in this kind of materials. It is also demonstrated that there is a transition layer between the nano-layer on surface and the coarse grain region inside. The transition layer obviously has certain influence on the overall mechanical properties.
基金Projects(50471070,50644041) supported by the National Natural Science Foundation of ChinaProject(20041023) supported by Youth Science and Technology Foundation of Shanxi Province, ChinaProject(200503005) supported by Key Laboratory Opening Foundation of Shanxi Province, China
文摘A nanostructured surface layer was fabricated on a AZ91D magnesium alloy by using a high-energy shot peening(HESP).HESP induced structure along the depth of the treated sample surface layer was characterized by means of X-ray diffractometer (XRD),transmission electron microscope(TEM) and high resolution transmission electron microscope(HRTEM).The experimental results show that a deformed layer of about 50 μm has formed after HESP treatment and the average grain size increases from about 40 nm in the surface layer to about 200 nm at the depth of 40 μm.The surface nanocrystallization can realize intercoordination of the dislocations slipping and dynamic recrystallization.The nanocrystalline grains have stacking faults and dislocation in their interiors.The microhardness of the top surface is about triplicate that of the coarse-grained matrix.
文摘Isothermal and isochronal annealing was conducted to study the thermal stability of the nanocrystalline in the surface layer of Mg alloy AZ91D induced by high-energy shot peening(HESP) .Field emission scanning electron microscope(FESEM) and X-ray diffractometer were used to characterize the microstructure.Results showed that nanocrystalline produced by HESP on the surface layer of the magnesium alloy AZ91D was 60-70 nm on average.The nanocrystalline could remain stable at about 100℃,and grew up slowly between 100℃ and 200℃.When the annealing temperature reached 300℃,the growth rate of the nanocrystalline increased significantly.The kinetic coefficient n of the nanocrystalline growth was calculated to be 2-3 and the grain growth activation energy Q=39.7 kJ/mol,far less than the self-diffusion activation energy of magnesium atoms in the coarse polycrystalline material.
