The flow behavior of a cast Ti-25Al-10Nb-3V-1Mo alloy based onTi3Al, with and without hydrogen content, was investigated under isothermal compression test at strain rates of 0.1s-1 to 0.001s -1 in the temperature rang...The flow behavior of a cast Ti-25Al-10Nb-3V-1Mo alloy based onTi3Al, with and without hydrogen content, was investigated under isothermal compression test at strain rates of 0.1s-1 to 0.001s -1 in the temperature range of 900℃ to1000 ℃. The hot compression peak stress (or the maximum flow stress) of the alloy withand without hydrogen decreases with the increasing temperature and the decreasingstrain rate. Hydrogenation makes the hot compression peak stress decrease by 37%～53%, which corresponds to lowering the deformation temperature by about 50℃.Strain rate does not change the favorable effect of hydrogenation on hot compressionflow behavior at all three deformation temperatures. The microstructure of the alloywith 0.2% H (mass %) deformed at a fixed temperature exhibits the same feature asthat of the alloys without hydrogenation deformed at higher temperatures for bothstrain rates. Hydrogenation has the same effect on microstructure as strain rate andtemperature.展开更多
Hot compression tests were carried out on a Fe-29Ni-17Co alloy in the temperature range of 900 ℃ to 1200 ℃ and at strain rates of 0.001-1 s-1. Dynamic recrystallization was found responsible for flow softening durin...Hot compression tests were carried out on a Fe-29Ni-17Co alloy in the temperature range of 900 ℃ to 1200 ℃ and at strain rates of 0.001-1 s-1. Dynamic recrystallization was found responsible for flow softening during hot compression. The flow behavior was successfully analyzed by the hyperbolic sine equation and the corresponding material constants A, n and αwere determined. The value of apparent activation energy was determined as 423 kJ/mol. The peak and steady state strains showed simple power-law dependence on the Zener-Hollomon parameter. The dynamic recrystallization kinetics was analyzed using Avrami equation and the corresponding exponent was determined to be about 2.7. This value, higher than 2 reported in the literatures, is associated with the mechanism of continuous dynamic recrystallization in the studied alloy. The flow curve up to the peak was modeled by the Cingara equation and the strain exponent, c, was determined about 0.85. The higher value of c compared with the value of 0.2 which has been reported for some stainless steels fortified the idea of extended dynamic recovery or continuous dynamic recrystallization in the studied alloy.展开更多
Aluminum silicon alloy of composition (Al-25%Si-3%Ni-1%Fe-2%Cu) was atomized using water atomization. The powders were cold compacted in a die to produce green cylinder compacts. Four consolidation processes were appl...Aluminum silicon alloy of composition (Al-25%Si-3%Ni-1%Fe-2%Cu) was atomized using water atomization. The powders were cold compacted in a die to produce green cylinder compacts. Four consolidation processes were applied, namely;conventional sintering at 500℃, sintering followed by hot forging to obtain pistons, one step hot forging into pistons, and hot pressing. The microstructure of the sintered specimens showed inter-granular pores and oxide layers on particle interfaces of 84% relative density. When the sintered specimens were hot forged, both the inter-granular pores and oxide layers on particle interfaces almost disappeared and the relative densities increased up to about 95%. The same microstructure is also obtained for the one step forged specimens, but the relative densities increased to about 97%. However, the hot pressing specimens showed the presence of oxide layers on particle surfaces as well as few isolated pores. The relative density of the hot pressed specimens was about 90%. Hardness and ultimate compression strength were measured. It is noted that the strongest bulk materials are those made by hot forging, followed by those made by hot pressing and the weakest bulk materials are those made by conventional sintering.展开更多
This paper models hot compression testing using a dilatometer in loading mode.These small-scale tests provide a high throughput at low cost,but are susceptible to inhomogeneity due to friction and temperature gradient...This paper models hot compression testing using a dilatometer in loading mode.These small-scale tests provide a high throughput at low cost,but are susceptible to inhomogeneity due to friction and temperature gradients.A novel method is presented for correcting the true stress-strain constitutive response over the full range of temperatures,strain-rates and strain.The nominal response from the tests is used to predict the offset in the stress-strain curves due to inhomogeneity,and this stress offsetΔσis applied piecewise to the data,correcting the constitutive response in one iteration.A key new feature is the smoothing and fitting of the flow stress data as a function of temperature and strain-rate,at multiple discrete strains.The corrected model then provides quantitative prediction of the spatial and temporal variation in strain-rate and strain throughout the sample,needed to correlate the local deformation conditions with the microstructure and texture evolution.The study uses a detailed series of 144 hot compression tests of a Zr-Nb alloy.While this is an important wrought nuclear alloy in its own right,it also serves here as a test case for modelling the dilatometer for hot testing of high temperature alloys,particularly those with dualα-βphase microstructures(such as titanium alloys).展开更多
文摘The flow behavior of a cast Ti-25Al-10Nb-3V-1Mo alloy based onTi3Al, with and without hydrogen content, was investigated under isothermal compression test at strain rates of 0.1s-1 to 0.001s -1 in the temperature range of 900℃ to1000 ℃. The hot compression peak stress (or the maximum flow stress) of the alloy withand without hydrogen decreases with the increasing temperature and the decreasingstrain rate. Hydrogenation makes the hot compression peak stress decrease by 37%～53%, which corresponds to lowering the deformation temperature by about 50℃.Strain rate does not change the favorable effect of hydrogenation on hot compressionflow behavior at all three deformation temperatures. The microstructure of the alloywith 0.2% H (mass %) deformed at a fixed temperature exhibits the same feature asthat of the alloys without hydrogenation deformed at higher temperatures for bothstrain rates. Hydrogenation has the same effect on microstructure as strain rate andtemperature.
文摘Hot compression tests were carried out on a Fe-29Ni-17Co alloy in the temperature range of 900 ℃ to 1200 ℃ and at strain rates of 0.001-1 s-1. Dynamic recrystallization was found responsible for flow softening during hot compression. The flow behavior was successfully analyzed by the hyperbolic sine equation and the corresponding material constants A, n and αwere determined. The value of apparent activation energy was determined as 423 kJ/mol. The peak and steady state strains showed simple power-law dependence on the Zener-Hollomon parameter. The dynamic recrystallization kinetics was analyzed using Avrami equation and the corresponding exponent was determined to be about 2.7. This value, higher than 2 reported in the literatures, is associated with the mechanism of continuous dynamic recrystallization in the studied alloy. The flow curve up to the peak was modeled by the Cingara equation and the strain exponent, c, was determined about 0.85. The higher value of c compared with the value of 0.2 which has been reported for some stainless steels fortified the idea of extended dynamic recovery or continuous dynamic recrystallization in the studied alloy.
文摘Aluminum silicon alloy of composition (Al-25%Si-3%Ni-1%Fe-2%Cu) was atomized using water atomization. The powders were cold compacted in a die to produce green cylinder compacts. Four consolidation processes were applied, namely;conventional sintering at 500℃, sintering followed by hot forging to obtain pistons, one step hot forging into pistons, and hot pressing. The microstructure of the sintered specimens showed inter-granular pores and oxide layers on particle interfaces of 84% relative density. When the sintered specimens were hot forged, both the inter-granular pores and oxide layers on particle interfaces almost disappeared and the relative densities increased up to about 95%. The same microstructure is also obtained for the one step forged specimens, but the relative densities increased to about 97%. However, the hot pressing specimens showed the presence of oxide layers on particle surfaces as well as few isolated pores. The relative density of the hot pressed specimens was about 90%. Hardness and ultimate compression strength were measured. It is noted that the strongest bulk materials are those made by hot forging, followed by those made by hot pressing and the weakest bulk materials are those made by conventional sintering.
基金Light Form,a UK Engineering and Physical Sciences Research Council(EPSRC)programme grant(EP/R001715/1)。
文摘This paper models hot compression testing using a dilatometer in loading mode.These small-scale tests provide a high throughput at low cost,but are susceptible to inhomogeneity due to friction and temperature gradients.A novel method is presented for correcting the true stress-strain constitutive response over the full range of temperatures,strain-rates and strain.The nominal response from the tests is used to predict the offset in the stress-strain curves due to inhomogeneity,and this stress offsetΔσis applied piecewise to the data,correcting the constitutive response in one iteration.A key new feature is the smoothing and fitting of the flow stress data as a function of temperature and strain-rate,at multiple discrete strains.The corrected model then provides quantitative prediction of the spatial and temporal variation in strain-rate and strain throughout the sample,needed to correlate the local deformation conditions with the microstructure and texture evolution.The study uses a detailed series of 144 hot compression tests of a Zr-Nb alloy.While this is an important wrought nuclear alloy in its own right,it also serves here as a test case for modelling the dilatometer for hot testing of high temperature alloys,particularly those with dualα-βphase microstructures(such as titanium alloys).
基金the Nation "973" Project of China (2007CB613807)the New Century Excellent Talents in University (NCET-07-0696)the fund of the State Key Laboratory of Solidification Processing in NWPU (35-TP-2009)
