A hot compression experiment (1073 1473 K, strain rates of 0. 001-10 s -1 ) of SAS08GR. 4N low alloy steel was performed using a Gleeble-3800 thermal-mechanical simulator, and the hot deformation behavior of the ste...A hot compression experiment (1073 1473 K, strain rates of 0. 001-10 s -1 ) of SAS08GR. 4N low alloy steel was performed using a Gleeble-3800 thermal-mechanical simulator, and the hot deformation behavior of the steel was investigated by analyzing both the true stress true strain curves and its microstructures. The thermal de formation equation and hot deformation activation energy (Q) of SA508GR. 4N steel were obtained by regression with a classic hyperbolic sine function. The hot processing map of SAS08GR. 4N steel was also established. An empirical equation for the stress peak was described for practical applications. The SA508GR. 4N steel showed a critical Zener-Hollomon parameter (lnZc) for dynamic recrystallization (DRX) of 37.44, below which full DRX may occur. The sensitivity of the SA508GR. 4N steel increased linearly with test temperature, such that higher temperatures led to enhanced workability.展开更多
The hot deformation behavior of as-cast AISI M2 high-speed steel containing mischmetal (RE) has been investigated on a Gleeble-3500 simulator in the temperature range of 1000--1 150 ℃ and strain rate range of 0.01-...The hot deformation behavior of as-cast AISI M2 high-speed steel containing mischmetal (RE) has been investigated on a Gleeble-3500 simulator in the temperature range of 1000--1 150 ℃ and strain rate range of 0.01- 10 s 1 at true strain of 1.0. The mechanical behavior has been characterized using stress-strain curve analysis, kinetic analysis, processing maps, etc. Metallographic investigation was performed to evaluate the mechanism of flow insta- bility. The results show that the deformation activation energy decreases with increasing deformation temperature; the efficiency of power dissipation increases with decreasing strain rate and increasing temperature; flow instability is observed at low-to-medium temperature and higher strain rate region when the strain is smaller, but extends to lower strain rate and high temperature regions with the increment of strain, in which it is manifested as flow localization near the grain boundary. Hot deformation equations and processing maps are obtained. The optimal processing window is suggested and the deformation mechanism is dynamic recrystallization (DRX).展开更多
Hot deformation behavior of an as-extruded duplex structured Mg-9Li-3Al-2.5Sr alloy is investigated via hot compression tests conducted at 200-350℃ with strain rate of 0.001-1 s^-1.The flow behavior of Mg-9Li-3Al-2.5...Hot deformation behavior of an as-extruded duplex structured Mg-9Li-3Al-2.5Sr alloy is investigated via hot compression tests conducted at 200-350℃ with strain rate of 0.001-1 s^-1.The flow behavior of Mg-9Li-3Al-2.5Sr alloy can be described accurately by hyperbolic sine constitutive equation and the average activation energy for deformation is calculated as 143.5 k J/mol.Based on a dynamic materials model,the processing maps of Mg-9Li-3Al-2.5Sr alloy which describe the variation of power dissipation efficiency are constructed as a function of temperature and strain rate.The processing maps exhibit an area of discontinuous dynamic recrystallization occurring at 280-300℃ with strain rate of 0.001-0.01 s^-1,which corresponds to the optimum hot working conditions.展开更多
Hot deformation behavior of a novel Ni-Cr-Mo-B heavy plate steel was studied by hot compression tests,which were conducted on a Gleeble-3800thermo-mechanical simulator corresponding to the temperature range of850-1 15...Hot deformation behavior of a novel Ni-Cr-Mo-B heavy plate steel was studied by hot compression tests,which were conducted on a Gleeble-3800thermo-mechanical simulator corresponding to the temperature range of850-1 150℃ with the strain rates of 0.01-10s-1 and the true strain of 0.8.The results suggest that the majority of flow curves exhibit a typical dynamic recrystallization(DRX)behavior with an apparent single peak stress followed by agradual fall towards a steady-state stress.Important characteristic parameters of flow behavior as critical stress/strain for initiation of DRX and peak and steady-state stress/strain were derived from curves of strain hardening rate versus stress and stress versus strain,respectively.Material constants of the investigated steel were determined based on Arrhenius-type constitutive equation,and then the peak stress was predicted by the equation with the hot deformation activation energy of 379 139J/mol,and the predicted values agree well with the experimental values.Furthermore,the effect of Zener-Hollomon parameter on the characteristic points of flow curves was studied using the power law relation,and the ratio of critical stress and strain to peak stress and strain were found to be 0.91and0.46,respectively.展开更多
The hot deformation behavior of ultra purified 17% Cr ferritic stainless steel stabilized with Nb and Ti was investigated using axisymmetric hot compression tests on a thermomechanical simulator.The deformation was ca...The hot deformation behavior of ultra purified 17% Cr ferritic stainless steel stabilized with Nb and Ti was investigated using axisymmetric hot compression tests on a thermomechanical simulator.The deformation was carried out at the temperatures ranging from 700 to 1 100℃ and strain rates from 1to 10s-1.The microstructure was investigated using electron backscattering diffraction.The effects of temperature and strain rate on deformation behavior were represented by Zener-Hollomon parameter in an exponent type equation.The effect of strain was incorporated in the constitutive equation by establishing polynomial relationship between the material constants and strain.A sixth order polynomial was suitable to represent the effect of strain.The modified constitutive equation considering the effect of strain was developed and could predict the flow stress throughout the deformation conditions except at800℃in 1s-1 and at 700℃in 5and 10s-1.Losing the reliability of the modified constitutive equation was possibly ascribed to the increase in average Taylor factor at 800℃in 1s-1 and the increase in temperature at 700℃in 5and10s-1 during hot deformation.The optimum window for improving product quality of the ferritic stainless steels was identified as hot rolling at a low finisher entry temperature of 700℃,which can be achieved in practical production.展开更多
The static recrystallization behavior of 25CrMo4 mirror plate steel has been determined by hot compression testing on a Gleeble 1500 thermal mechanical simulation tester. Compression tests were performed using double ...The static recrystallization behavior of 25CrMo4 mirror plate steel has been determined by hot compression testing on a Gleeble 1500 thermal mechanical simulation tester. Compression tests were performed using double hit schedules at temperatures of 950-- 1 150 ~C, strain rates of 0.01--0.5 s-1 , and recrystallization time of 1--100 s. Results show that the kinetics of static recrystallization and the microstructural evolution were greatly influenced by the deformation parameters (deformation temperature, strain rate and pre strain) and the initial austenite grain size. Based on the experimental results, the kinetics model of static recrystallization has been generated and the comparison between the experimental results and the predicted results has been carried out. It is shown that the predicted results were in good agreement with the experimental results.展开更多
The hot compressive deformation behavior of hot isostatically pressed Ti-47.5Al-2Cr-2Nb-0.2W-0.2B alloy using gas atomization powders was systematically investigated and the processing map was obtained in the temperat...The hot compressive deformation behavior of hot isostatically pressed Ti-47.5Al-2Cr-2Nb-0.2W-0.2B alloy using gas atomization powders was systematically investigated and the processing map was obtained in the temperature range of 1323-1473 Kand strain rate range of 0.001-0.5s^(-1).The calculated activation energy in the above variational ranges of temperature and strain rate possesses a low activation energy value of approximately 365.6kJ/mol based on the constitutive relationship models developed with the Arrhenius-type constitutive model respectively considering the strain rate and deformation temperature.The hot working flow behavior during the deformation process was analyzed combined with the microstructural evolution.Meanwhile,the processing maps during the deformation process were established based on the dynamic material model and Prasad instability criterion under different deformation conditions.Finally,the optimal hot processing window of this alloy corresponding to the wide temperature range of 1353-1453 Kand the low strain rate of 0.001-0.1s^(-1) was obtained.展开更多
The high-temperature deformation behavior of a beta Ti-3.0 Al-3.5 Cr-2.0 Fe-0.1 B alloy was investigated by a Gleeble-1500 D thermal simulator. The height reduction was 50%, corresponding to a true strain of 0.693. Th...The high-temperature deformation behavior of a beta Ti-3.0 Al-3.5 Cr-2.0 Fe-0.1 B alloy was investigated by a Gleeble-1500 D thermal simulator. The height reduction was 50%, corresponding to a true strain of 0.693. The strain rate ranging from 0.01 to 10.00 s^-1 and the deformation temperature ranging from 800 to 950 ℃ were considered.The flow stress and the apparent activation energy for deformation, along with the constitutive equation, were used to analyze the behavior of the Ti-3.0 Al-3.5 Cr-2.0 Fe-0.1 B alloy. The processing map was established. The effect of strain rate on the microstructure at 850 ℃ was evaluated.The flow stress-strain curves indicated that the peak flow stresses increased along with an increase in the strain rate and decreased as the deformation temperature increased.Based on the true stress-true strain curves, the constitutive equation was established and followed as the ε= 6.58×10-(10)[sinh(0.0113σ)]-(3.44)exp(-245481.3/RT). The processing map exhibited the "unsafe" region at the strain rate of10 s^-1 and the temperature of 850 ℃,and the rest region was "safe". The deformation microstructure demonstrated that both dynamic recovery(DRV) and dynamic recrystallization(DRX) existed during deformation. At the lower strain rate of 0.01 s^-1, the main deformation mechanism was the DRV, and the DRX was the dominant deformation mechanism at the higher strain rate of 1.00 s^-1.展开更多
The effects of squeeze casting process on microstructure and flow stress behavior of Al-17.5Si-4Cu-0.5Mg alloy were investigated and the hot-compression tests of gravity casting and squeeze casting alloy were carried ...The effects of squeeze casting process on microstructure and flow stress behavior of Al-17.5Si-4Cu-0.5Mg alloy were investigated and the hot-compression tests of gravity casting and squeeze casting alloy were carried out at 350-500°C and 0.001-5s-1.The results show that microstructures of Al-17.5Si-4Cu-0.5Mg alloys were obviously improved by squeeze casting.Due to the decrease of coarse primary Si particles,softα-Al dendrite as well as the fine microstructures appeared,and the mechanical properties of squeeze casting alloys were improved.However,when the strain rate rises or the deformation temperature decreases,the flow stress increases and it was proved that the alloy is a positive strain rate sensitive material.It was deduced that compared with the gravity casting alloy,squeeze casting alloy(solidified at 632 MPa)is more difficult to deform since the flow stress of squeeze casting alloy is higher than that of gravity casting alloy when the deformation temperature exceeds 400°C.Flow stress behavior of Al-17.5Si-4Cu-0.5Mg alloy can be described by a hyperbolic sine form with Zener-Hollomon parameter,and the average hot deformation activation energy Q of gravity casting alloy and squeeze casting alloy is 278.97 and 308.77kJ/mol,respectively.展开更多
基金Item Sponsored by National Energy Application Technology Research and Engineering Demonstrative Project of China(NY201501)
文摘A hot compression experiment (1073 1473 K, strain rates of 0. 001-10 s -1 ) of SAS08GR. 4N low alloy steel was performed using a Gleeble-3800 thermal-mechanical simulator, and the hot deformation behavior of the steel was investigated by analyzing both the true stress true strain curves and its microstructures. The thermal de formation equation and hot deformation activation energy (Q) of SA508GR. 4N steel were obtained by regression with a classic hyperbolic sine function. The hot processing map of SAS08GR. 4N steel was also established. An empirical equation for the stress peak was described for practical applications. The SA508GR. 4N steel showed a critical Zener-Hollomon parameter (lnZc) for dynamic recrystallization (DRX) of 37.44, below which full DRX may occur. The sensitivity of the SA508GR. 4N steel increased linearly with test temperature, such that higher temperatures led to enhanced workability.
基金Item Sponsored by National Natural Science Foundation of China(51101137,51171161)Science and Technology Research and Development Plan of Qinhuangdao of China(201101A100)
文摘The hot deformation behavior of as-cast AISI M2 high-speed steel containing mischmetal (RE) has been investigated on a Gleeble-3500 simulator in the temperature range of 1000--1 150 ℃ and strain rate range of 0.01- 10 s 1 at true strain of 1.0. The mechanical behavior has been characterized using stress-strain curve analysis, kinetic analysis, processing maps, etc. Metallographic investigation was performed to evaluate the mechanism of flow insta- bility. The results show that the deformation activation energy decreases with increasing deformation temperature; the efficiency of power dissipation increases with decreasing strain rate and increasing temperature; flow instability is observed at low-to-medium temperature and higher strain rate region when the strain is smaller, but extends to lower strain rate and high temperature regions with the increment of strain, in which it is manifested as flow localization near the grain boundary. Hot deformation equations and processing maps are obtained. The optimal processing window is suggested and the deformation mechanism is dynamic recrystallization (DRX).
基金the financial support from the National Natural Science Foundation(Project No.51601024)the National Key Research and Development plan(Project No.2016YFB0700403)+1 种基金the Chongqing Research Program of Basic Research and Frontier Technology(Project No.cstc2016jcyj A0418)the Fundamental Research Funds for the Central Universities(Project No.106112015CDJXY130011 and No.CDJZR14130007)
文摘Hot deformation behavior of an as-extruded duplex structured Mg-9Li-3Al-2.5Sr alloy is investigated via hot compression tests conducted at 200-350℃ with strain rate of 0.001-1 s^-1.The flow behavior of Mg-9Li-3Al-2.5Sr alloy can be described accurately by hyperbolic sine constitutive equation and the average activation energy for deformation is calculated as 143.5 k J/mol.Based on a dynamic materials model,the processing maps of Mg-9Li-3Al-2.5Sr alloy which describe the variation of power dissipation efficiency are constructed as a function of temperature and strain rate.The processing maps exhibit an area of discontinuous dynamic recrystallization occurring at 280-300℃ with strain rate of 0.001-0.01 s^-1,which corresponds to the optimum hot working conditions.
基金Sponsored by National Natural Science Foundation of China(51071019,51371030)National High Technology Research and Development Program of China(2013AA031601)National Key Technology Research and Development Program of the Ministry of Science and Technology of China(2011BAE25B01)
文摘Hot deformation behavior of a novel Ni-Cr-Mo-B heavy plate steel was studied by hot compression tests,which were conducted on a Gleeble-3800thermo-mechanical simulator corresponding to the temperature range of850-1 150℃ with the strain rates of 0.01-10s-1 and the true strain of 0.8.The results suggest that the majority of flow curves exhibit a typical dynamic recrystallization(DRX)behavior with an apparent single peak stress followed by agradual fall towards a steady-state stress.Important characteristic parameters of flow behavior as critical stress/strain for initiation of DRX and peak and steady-state stress/strain were derived from curves of strain hardening rate versus stress and stress versus strain,respectively.Material constants of the investigated steel were determined based on Arrhenius-type constitutive equation,and then the peak stress was predicted by the equation with the hot deformation activation energy of 379 139J/mol,and the predicted values agree well with the experimental values.Furthermore,the effect of Zener-Hollomon parameter on the characteristic points of flow curves was studied using the power law relation,and the ratio of critical stress and strain to peak stress and strain were found to be 0.91and0.46,respectively.
基金Sponsored by National Science and Technology Pillar Program during the Twelfth Five-year Plan Period of China(2012BAE04B02)National Natural Science Foundation of China(51271050)
文摘The hot deformation behavior of ultra purified 17% Cr ferritic stainless steel stabilized with Nb and Ti was investigated using axisymmetric hot compression tests on a thermomechanical simulator.The deformation was carried out at the temperatures ranging from 700 to 1 100℃ and strain rates from 1to 10s-1.The microstructure was investigated using electron backscattering diffraction.The effects of temperature and strain rate on deformation behavior were represented by Zener-Hollomon parameter in an exponent type equation.The effect of strain was incorporated in the constitutive equation by establishing polynomial relationship between the material constants and strain.A sixth order polynomial was suitable to represent the effect of strain.The modified constitutive equation considering the effect of strain was developed and could predict the flow stress throughout the deformation conditions except at800℃in 1s-1 and at 700℃in 5and 10s-1.Losing the reliability of the modified constitutive equation was possibly ascribed to the increase in average Taylor factor at 800℃in 1s-1 and the increase in temperature at 700℃in 5and10s-1 during hot deformation.The optimum window for improving product quality of the ferritic stainless steels was identified as hot rolling at a low finisher entry temperature of 700℃,which can be achieved in practical production.
基金sponsored by National Basic Research Program of China (2011CB012903)
文摘The static recrystallization behavior of 25CrMo4 mirror plate steel has been determined by hot compression testing on a Gleeble 1500 thermal mechanical simulation tester. Compression tests were performed using double hit schedules at temperatures of 950-- 1 150 ~C, strain rates of 0.01--0.5 s-1 , and recrystallization time of 1--100 s. Results show that the kinetics of static recrystallization and the microstructural evolution were greatly influenced by the deformation parameters (deformation temperature, strain rate and pre strain) and the initial austenite grain size. Based on the experimental results, the kinetics model of static recrystallization has been generated and the comparison between the experimental results and the predicted results has been carried out. It is shown that the predicted results were in good agreement with the experimental results.
基金the financial supports from the National Natural Science Foundation of China(Grant Nos.51301157 and 51434007)the National High Technology Research and Development Program of China 863 Program(Grant No.2013AA031103)
文摘The hot compressive deformation behavior of hot isostatically pressed Ti-47.5Al-2Cr-2Nb-0.2W-0.2B alloy using gas atomization powders was systematically investigated and the processing map was obtained in the temperature range of 1323-1473 Kand strain rate range of 0.001-0.5s^(-1).The calculated activation energy in the above variational ranges of temperature and strain rate possesses a low activation energy value of approximately 365.6kJ/mol based on the constitutive relationship models developed with the Arrhenius-type constitutive model respectively considering the strain rate and deformation temperature.The hot working flow behavior during the deformation process was analyzed combined with the microstructural evolution.Meanwhile,the processing maps during the deformation process were established based on the dynamic material model and Prasad instability criterion under different deformation conditions.Finally,the optimal hot processing window of this alloy corresponding to the wide temperature range of 1353-1453 Kand the low strain rate of 0.001-0.1s^(-1) was obtained.
基金financially supported by the.National Natural Science Foundation of China (No.51401027)the China Postdoctoral Science Foundation Funded Project (No.2016M591040)
文摘The high-temperature deformation behavior of a beta Ti-3.0 Al-3.5 Cr-2.0 Fe-0.1 B alloy was investigated by a Gleeble-1500 D thermal simulator. The height reduction was 50%, corresponding to a true strain of 0.693. The strain rate ranging from 0.01 to 10.00 s^-1 and the deformation temperature ranging from 800 to 950 ℃ were considered.The flow stress and the apparent activation energy for deformation, along with the constitutive equation, were used to analyze the behavior of the Ti-3.0 Al-3.5 Cr-2.0 Fe-0.1 B alloy. The processing map was established. The effect of strain rate on the microstructure at 850 ℃ was evaluated.The flow stress-strain curves indicated that the peak flow stresses increased along with an increase in the strain rate and decreased as the deformation temperature increased.Based on the true stress-true strain curves, the constitutive equation was established and followed as the ε= 6.58×10-(10)[sinh(0.0113σ)]-(3.44)exp(-245481.3/RT). The processing map exhibited the "unsafe" region at the strain rate of10 s^-1 and the temperature of 850 ℃,and the rest region was "safe". The deformation microstructure demonstrated that both dynamic recovery(DRV) and dynamic recrystallization(DRX) existed during deformation. At the lower strain rate of 0.01 s^-1, the main deformation mechanism was the DRV, and the DRX was the dominant deformation mechanism at the higher strain rate of 1.00 s^-1.
基金supported by National Natural Science Foundation of China(51674168)Shenyang City Application Basic Research Foundation(F14-231-1-23)
文摘The effects of squeeze casting process on microstructure and flow stress behavior of Al-17.5Si-4Cu-0.5Mg alloy were investigated and the hot-compression tests of gravity casting and squeeze casting alloy were carried out at 350-500°C and 0.001-5s-1.The results show that microstructures of Al-17.5Si-4Cu-0.5Mg alloys were obviously improved by squeeze casting.Due to the decrease of coarse primary Si particles,softα-Al dendrite as well as the fine microstructures appeared,and the mechanical properties of squeeze casting alloys were improved.However,when the strain rate rises or the deformation temperature decreases,the flow stress increases and it was proved that the alloy is a positive strain rate sensitive material.It was deduced that compared with the gravity casting alloy,squeeze casting alloy(solidified at 632 MPa)is more difficult to deform since the flow stress of squeeze casting alloy is higher than that of gravity casting alloy when the deformation temperature exceeds 400°C.Flow stress behavior of Al-17.5Si-4Cu-0.5Mg alloy can be described by a hyperbolic sine form with Zener-Hollomon parameter,and the average hot deformation activation energy Q of gravity casting alloy and squeeze casting alloy is 278.97 and 308.77kJ/mol,respectively.