Microstructure evolution and strengthening mechanism of high -performance powder metallurgy TA15 titanium alloy by hot rolling

Hot deformation of sintered billets by powder metallurgy(PM)is an effective preparation technique for titanium alloys,which is more significant for high-alloying alloys.In this study,Ti–6.5Al–2Zr–Mo–V(TA15)titanium alloy plates were prepared by cold press-ing sintering combined with high-temperature hot rolling.The microstructure and mechanical properties under different process paramet-ers were investigated.Optical microscope,electron backscatter diffraction,and others were applied to characterize the microstructure evolution and mechanical properties strengthening mechanism.The results showed that the chemical compositions were uniformly dif-fused without segregation during sintering,and the closing of the matrix craters was accelerated by increasing the sintering temperature.The block was hot rolled at 1200℃ with an 80%reduction under only two passes without annealing.The strength and elongation of the plate at 20–25℃ after solution and aging were 1247 MPa and 14.0%,respectively,which were increased by 24.5%and 40.0%,respect-ively,compared with the as-sintered alloy at 1300℃.The microstructure was significantly refined by continuous dynamic recrystalliza-tion,which was completed by the rotation and dislocation absorption of the substructure surrounded by low-angle grain boundaries.After hot rolling combined with heat treatment,the strength and plasticity of PM-TA15 were significantly improved,which resulted from the dense,uniform,and fine recrystallization structure and the synergistic effect of multiple slip systems.

Design,preparation,microstructure and mechanical property of the lightweight radiation-shielding Mg-Ta-Al composites basing differential temperature hot rolling

A novel lightweight,radiation-shielding Mg-Ta-Al layered metal-matrix composite(LMC)was successful designed by doping the extremely refractory metal(Ta)into Mg sheets.These Mg-based LMCs sheets shows excellent radiation-dose shield effect,about 145 krad·a^(−1),which is about 17 times of traditional Mg alloy,while its surface density is only about 0.9 g·cm^(−2),reducing by 60%than that of pure Ta.The quantitate relationship between radiation-dose and the materials’thickness was also confirmed to the logistic function when the surface density is in the range of 0.6-1.5 g·cm^(−2).Meantime,the rolling parameters,interface microstructure and mechanical properties in both as-rolled and annealing treated samples were evaluated.The sheets possess a special dissimilar atoms diffusion transitional zone containing an obvious inter-diffusion Mg-Al interface and the unique micro-corrugated Ta-Al interface,as well as a thin Al film with a thickness of about 10μm.The special zone could reduce the stress concentration and enhance the strength of Mg-Ta-Al LMCs.The interface bonding strength reaches up to 54-76 MPa.The ultimate tensile strength(UTS)and yield strength(TYS)of the Mg-Ta-Al sheet were high to 413 MPa and 263 MPa,respectively,along with an elongation of 5.8%.The molecular dynamics(MD)analysis results show that the two interfaces exhibit different formation mechanism,the Mg-Al interface primarily depended on Mg/Al atoms diffusion basing point defects movement,while the Ta-Al interface with a micro-interlock pining shape formed by close-packed planes slipping during high temperature strain-induced deformation process.

Influence of Production Sequence of Aluminum Alloy Hot Rolling on Strip Surface Quality

With the intensification of market competition in the aluminum alloy strip processing industry,it is dif-ficult to control the mass production of the same specifications,which is bound to affect the hot rolling production.This paper studied the effect of the hot rolling order of aluminum alloy on the surface quality of strip,such as roll printing,color difference,anodic oxidation,etc.,reasonable discharge sequence and corresponding optimization measures were formulated.

Achieving oxidation protection effect for strips hot rolling via Al_(2)O_(3) nanofluid lubrication

It was discovered the application of Al_(2)O_(3) nanofluid as lubricant for steel hot rolling could synchronously achieve oxidation protection of strips surface.The underlying mechanism was investigated through hot rolling tests and molecular dynamics (MD) simulations.The employment of Al_(2)O_(3) nanoparticles contributed to significant enhancement in the lubrication performance of lubricant.The rolled strip exhibited the best surface topography that the roughness reached lowest with the sparsest surface defects.Besides,the oxide scale generated on steel surface was also thinner,and the ratio of Fe_(2)O_(3) among various iron oxides became lower.It was revealed the above oxidation protection effect of Al_(2)O_(3) nanofluid was attributed to the deposition of nanoparticles on metal surface during hot rolling.A protective layer in the thickness of about 193 nm was formed to prevent the direct contact between steel matrix and atmosphere,which was mainly composed of Al_(2)O_(3) and sintered organic molecules.MD simulations confirmed the diffusion of O_(2) and H_(2)O could be blocked by the Al_(2)O_(3) layer through physical absorption and penetration barrier effect.

FEM modeling of dynamical recrystallization during multi-pass hot rolling of AM50 alloy and experimental verification

The microstructure simulation during the multi-pass hot rolling of AM50 alloy was studied by DEFORM-3D. The excellent agreement with the experiment observations shows that the present modeling and user routine are feasible for the reproduce of the hot rolling process. The multi-pass hot rolling contributes to the achievement of a uniformly recrystallized microstructure with fine grains in the rolled sheet. The sheet temperature before the finish rolling strongly affects the final grain size, but hardly affects the grain size distribution. This modeling and the user routine also have a potential to be applied in the researches of the other multi-pass hot deformation process.

Effects of magnetic field and hot rolling on microstructures and properties of cryo ECAPed 1050 aluminum alloy during annealing

The evolution of hardness and microstructures of 1050 aluminum alloy prepared by hot rolling and subsequent equal- channel angular pressing at cryogenic temperature (cryoECAP) after annealing at 150?400 °C for 1 h without and with magnetic field of 12 T was investigated. The electron back scattering diffraction pattern (EBSD) and transmission electron microscopy (TEM) were utilized to characterize the grain microstructures and dislocations. It is demonstrated that the hot rolling before cryoECAP produces more equiaxed grains with a smaller average size and a higher fraction of high angle boundaries (HABs) in the subsequent cryoECAPed 1050 aluminum alloy, thus accelerating the recovery and recrystallization of cryoECAPed alloy and produces more homogeneous microstructure during annealing. The magnetic field promotes the recovery and recrystallization and leads to much lower hardness at 150?250 °C, while it can suppress the abnormal grain growth and form more homogeneous grain size distributions annealed at 300?400 °C.

Comparison of evolution laws of stress and strain fields in hot rolling of titanium alloy large rings with different sizes

For hot rolling of titanium alloy large rings,evolution laws of stress and strain fields in rings with various sizes were explored and compared based on a reliable coupled thermo-mechanical three-dimensional （3D） finite element （FE） model.The results show that for forming processes of different rings,as γ^-（the equivalent distribution ratio of feed amount per revolution of a process） decreases,the final peak Mises stress may transfer from the biting point at the driver roll side to that at the idle roll side,and the final peak equivalent plastic strain may transfer from the outside surface to the inside surface;as L^- （the equivalent deformation zone length of a process） increases,the final peak Mises stress may appear in the middle layer.The final positions of peak Mises stress and equivalent plastic strain are the combined effects of the above two aspects.In the deformation zone of a deformed ring,the surface layers are in the 3D compressive stress state,while the middle layer is in the 1D compressive and 2D tensile stress state or 2D compressive and 1D tensile stress state;the whole ring is in the 1D compressive and 2D tensile strain state.

Three-Di mensional Model for Strip Hot Rolling

A three-dimensional model for strip hot rolling was developed, in which the plastic deformation of strip, the thermal crown of rolls, roll deflection and flattening were calculated by rigid-plastic finite element method, finite difference method, influential function method and elastic finite element method respectively. The roll wear was taken into consideration. The model can provide detailed information such as rolling pressure distribution, contact pressure distribution between backup rolls and work rolls, deflection and flattening of work rolls, lateral distribution of strip thickness, and lateral distribution of front and back tensions. The finish rolling on a 1 450 mm hot strip mill was simulated.

Backup roll contour in finishing trains of hot rolling based on hybrid genetic algorithm

On the basis of integrating two-dimensional varying thickness finite elementmethod with hybrid genetic algorithm, a precise model was developed to design ideal backup rollcontour (Varying Contact Backup Roll, in short VCR) in finishing rains of hot rolling rapidly andefficaciously. Additionally, a lot of good actual effects of VCR, such as evident improvement ofprofile and flatness of strip, remarkable decrease of roll consume, excellent maneuverability andmaintenance, and so on, were validated by long-term industrial tests in hot rolling strip plant ofWuhan Iron and Steel Group Corporation (WISCO).

MODELING OF FERRITE GRAIN GROWTH OF LOW CARBON STEELS DURING HOT ROLLING

For most commercial steels the prediction of the final properties depends on accurately calculating the room temperature ferrite grain size. A grain growth model is proposed for low carbon steels Q235B during hot rolling. By using this model, the initial ferrite grain size after continuous cooling and ferrite grain growing in coiling procedure can be predicted. In-plant trials were performed in the hot strip mill of Ansteel. The calculated final ferrite grain sizes are in good agreement with the experimental ones. It is helpful both for simulation of microstructure evolution and prediction of mechanical properties.

Mechanical properties and texture evolution during hot rolling of AZ31 magnesium alloy

Mechanical properties and texture evolutions of the as-rolled AZ31 Mg sheets were investigated.The results show that the grains of the sheets are significantly refined after hot rolling.The mechanical properties of the as-rolled samples are enhanced due to the grain size refinement.The intensity of basal texture decreases with the increase of deformation ratio,and double-peak type basal texture is discovered in the intermediate and large strain hot rolling processes.The formation of the texture is ascribed to the activities of prismatic and non-basalslips,which is the same as the 30%rolled and 50%rolled samples.The incline of basal planes exerts an effect on the mechanical anisotropy during tension along rolling direction(RD)and transverse direction(TD)at room temperature.

Test research on sticking mechanism during hot rolling of SUS 430 ferritic stainless steel

The sticking phenomenon during hot rolling of SUS 430 ferritic stainless steel was investigated by means of a two-disc type high-temperature wear tester. The test results indicate that sticking particles on the surfaces of high chromium steel （HiCr） and high-speed steel （HSS） rolls undergo nucleation, growth, and saturation stages. Grooves on the roll surface generated by grinding provide nucleation sites for sticking particles. The number of sticking particles on the HiCr roll surface is greater than that on the HSS roll surface. The average surface roughnesses （Ra） of HiCr and HSS rolls change from 0.502 and 0.493 μm at the initial stage to 0.837 and 0.530 μm at the saturation stage, respectively. The test further proves that the sticking behavior is strongly dependent on roll materials, and the HSS roll is more benefi- cial to prevent particles sticking compared with the HiCr roll under the same hot-rolling conditions.

Comparative study on hot rolling of Cu-Cr and Cu-Cr-CNT nanocomposites

Cu-1%Cr(mass fraction)and Cu-1%Cr-5%carbon nanotube(CNT)(mass fraction)nanocomposite powders were produced by mechanical alloying and consolidated by hot pressing.Then,nanocomposites were hot-rolled by the order of 50%reduction at 650°C.The structure and microstructure were investigated by X-ray diffractometry(XRD)and scanning electron microscopy(SEM).Relative density,microhardness,thermal stability,electrical and wear properties were evaluated.Compared to the Cu-Cr sample,the relative density of Cu-Cr-CNT sample is greatly improved from 75%to near full density of 98%by hot rolling.Although electrical conductivity and microhardness increase in both Cu-Cr and Cu-Cr-CNT nanocomposites after hot rolling,the effect of hot rolling on the enhancement is more prominent in the presence of CNTs.The microhardness and electrical conductivity of hot-rolled Cu-Cr-CNT nanocomposite approach HV 175 and 68%(IACS),respectively.Also,hot rolling is more effective on thermal stability improvement of Cu-Cr-CNT nanocomposite compared to Cu-Cr composite.However,after hot rolling,both the friction coef?cient and wear loss of the Cu-Cr sample display higher reduction than those of Cu-Cr-CNT nanocomposite owing to different wear mechanisms.After hot rolling,friction coefficient and wear loss of Cu-Cr sample display variation of 25%and 62%,respectively.

Microstructure and mechanical properties of Mg-6Al-0.3Mn-xY alloys prepared by casting and hot rolling

Mg-6Al-0.3Mn-xY(x=0,0.3,0.6 and 0.9,mass fraction,%) magnesium alloys were prepared by casting and hot rolling process.The influence of yttrium on microstructure and tensile mechanical properties of the AM60 magnesium alloy was investigated.The results reveal that with increasing the yttrium content,Al2Y precipitates form and the grain size is reduced.The ultimate strength,yield strength and elongation at room temperature are 192 MPa,62 MPa and 12.6%,respectively,for the as-cast Mg-6Al-0.3Mn-0.9Y alloy.All these properties are improved obviously by hot rolling,and the values are up to 303 MPa,255 MPa and 17.1%,respectively,for the rolled Mg-6Al-0.3Mn-0.9Y alloy.The improvement of mechanical properties is attributed to continuous dynamic recrystallization and the existence of highly thermal stable Al2Y precipitate which impedes the movement of dislocation effectively.

Graphitization of Spray-formed Ultrahigh Carbon Steels Containing Si during Hot Rolling

The graphitization behavior of ultrahigh carbon steels containing Si in hot rolling processes was investigated. The graphite stringers went mostly through the small pores and generally paralleled to the rolling direction. The influence of alloy elements on graphitization was estimated based on thermodynamics, which showed that Si content was important for graphitization. Graphite stringers nucleated at small pores and grew with carbon diffusion during hot rolling. Alloy contents, pores and hot deformation at γ+Fe3C phase range were the key factors for the formation of graphite. The probable effect of deformation on graphite formation during hot rolling was discussed in this paper.

Analysis of bending on the front end of sheet during hot rolling

The analysis of bending in finishing rolling was performed. An asymmetrical rolling force model was established, and the upper and lower neutral points were determined. Thc bending which resulted from the asymmetrical rolling force at the roll gap was studied and related flexibility equations were proposed according to elastic mechanics. Moreover, material mechanics was used to analyze the effects of temperature difference and self-weight on the bending out of the roll gap, and the flexibility equations were constructed. The main factors on bending were summed up, and the bending rule in the rolling could be obtained. In addition practical calculation was made with the production data of ribbon steel from Laiwu Iron ＆ Steel Group Co. Ltd.

Thermal Behaviors of Work Roll in Finishing Trains of Hot Rolling

In order to analyze the thermal field and thermal contour of work roll in finishing trains of hot rolling in rolling process, a quasi two-dimension implicit finite difference model is developed. To improve the calculating speed and precision, some special solutions are introduced, including the development of this model, the simplification of boundary conditions and the computation of heat transfer coefficients. The results show that these solutions of thermal behaviors of work roll are very much efficient and the model can be used as an on-line profile and fatness control model of large industrial mills.

Grain refining and property improvement of AZ31 Mg alloy by hot rolling

Hot rolling of AZ31 Mg alloy was performed by using as-cast alloy ingot as the starting material.The microstructures and mechanical properties of the as-rolled alloy subjected to various rolling passes were investigated.The results show that the grain size of the alloy can be refined steadily with increasing rolling passes by dynamic recrystallization.With the steady refining of the grain size,both the mechanical strength and the plasticity of the alloy are improved correspondingly.In particular,when the grain size is reduced to about 5μm after 5 rolling passes,the yield strength,ultimate tensile strength and tensile fracture strain of the alloy are 211 MPa,280 MPa and 0.28 in the transverse direction,they are 200 MPa,268 MPa and 0.32 in the rolling direction,respectively.

Texture evolution in AZ91 alloy after hot rolling and annealing

A commercial AZ91 magnesium alloy with a random initial texture was subjected to homogenization heat treatment （solution annealing） at 450 ℃. This resulted in the appearance of a weak triple （0001）-（10]-0）-（1120） fibber texture. After hot rolling at 400 ℃, the deformation texture was typically （0001） basal with splitting of the basal poles in the rolling direction. After annealing at 450℃ for 36 h, the annealing texture was the retained deformation texture with more homogeneous distribution of poles around the ideal basal orientation. There was no trace of abnormal grain growth.

Effects of hot rolling on microstructure and properties of a 20 vol.% SiC_P/Al composite

A 20 vol. percent SiC_p/Al composite was fabricated by squeeze casting, ofwhich a new process for fabricating the preform was used by blending Al powder and SiC particulateswith average diameters of 10 and 3.5 mu m, respectively. The microstructure of the as-cast and thehot-rolled composite was investigated by using TEM, EDS, and SEM, and their tensile properties weremeasured at room temperature. The results show that the ultimate tensile strength and ultimateelongation of the hot-rolled composite are 80 percent and 140 percent higher than those of theas-cast one. The TEM observation result indicates that there are high density of dislocations anddislocation tangles in the hot-rolled composite. Al_2O_3 layers in the composite resulting from thesurface oxidation of the aluminum powders were damaged to spherical particles during hot rolling.All the results indicate that hot-rolling can improve the mechanical properties of the compositeand, therefore, engineering components of the 20 vol. percent SiC_p/Al composite can be produced bysqueeze casting followed by hot-rolling.