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Hydrothermal Synthesis and Characterization of a Novel Organic Inorganic Hybrid Compound [Co(dien)_2](dienH_3)(H_3O)_7[P_2Mo_5O_(23)]_2·14H_2O
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作者 赵卫锋 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2007年第1期120-121,共2页
A new compound,[Co(dien)2](dienH3)(H3O)7[P2Mo5O23]2·14H2O, has been hydrothermallly synthesized by using Na2MoO4,CoCl2, H3PO4 and dien, and structurally characterized by elemental analysis, X-ray powder dif... A new compound,[Co(dien)2](dienH3)(H3O)7[P2Mo5O23]2·14H2O, has been hydrothermallly synthesized by using Na2MoO4,CoCl2, H3PO4 and dien, and structurally characterized by elemental analysis, X-ray powder diffraction analysis, SEM, IR and TG analysis. The results show that the compound is composed of a polyanion [P2Mo5O23]2^12, complex [Co(dien)2]^2+ cation, protonated [dienH3]^3+ , and forteen crystallization water molecule. 展开更多
关键词 hydrotherrnal synthesis heteropoly compound organic-inorganic hybrid compound
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