Assessing mixing uniformity in microreactors via in-line spectroscopy

Mixing behavior is critical for enhancing the selectivity of fast chemical reactions in microreactors.A high Reynolds number(Re)improves the mixing rate and selectivity of the reactions,but some exceptions of increasing side product yield with the higher Re have been reported.This study investigated the mixing uniformity in microreactors with in-line UV-vis spectroscopy to clarify the relationship between reaction selectivity and chaotic mixing with the higher Re.A colorization experiment of thymolphthalein in an acidic solution was conducted with an excess acid amount to the base to indicate a non-uniformly mixed region.Non-uniformity significantly increased with Re.At the same time,the degree of mixing,which was measured by a usual decolorization experiment,showed that the mixing rate increased with Re.The in-line analysis of the Villermaux-Dushman reaction during the mixing clarified that side product yield significantly increased with Re at around 300 and then decreased at around 1100.These results suggest the compensation effect between the mixing uniformity and mixing rate on the selectivity of the mixing-sensitive reactions.Faster mixing,characterized by a larger Re,can disturb mixing uniformity and,in some cases,decrease reaction selectivity.

Depth-Guided Vision Transformer With Normalizing Flows for Monocular 3D Object Detection

Monocular 3D object detection is challenging due to the lack of accurate depth information.Some methods estimate the pixel-wise depth maps from off-the-shelf depth estimators and then use them as an additional input to augment the RGB images.Depth-based methods attempt to convert estimated depth maps to pseudo-LiDAR and then use LiDAR-based object detectors or focus on the perspective of image and depth fusion learning.However,they demonstrate limited performance and efficiency as a result of depth inaccuracy and complex fusion mode with convolutions.Different from these approaches,our proposed depth-guided vision transformer with a normalizing flows(NF-DVT)network uses normalizing flows to build priors in depth maps to achieve more accurate depth information.Then we develop a novel Swin-Transformer-based backbone with a fusion module to process RGB image patches and depth map patches with two separate branches and fuse them using cross-attention to exchange information with each other.Furthermore,with the help of pixel-wise relative depth values in depth maps,we develop new relative position embeddings in the cross-attention mechanism to capture more accurate sequence ordering of input tokens.Our method is the first Swin-Transformer-based backbone architecture for monocular 3D object detection.The experimental results on the KITTI and the challenging Waymo Open datasets show the effectiveness of our proposed method and superior performance over previous counterparts.

A Normalizing Flow-Based Bidirectional Mapping Residual Network for Unsupervised Defect Detection

Unsupervised methods based on density representation have shown their abilities in anomaly detection,but detection performance still needs to be improved.Specifically,approaches using normalizing flows can accurately evaluate sample distributions,mapping normal features to the normal distribution and anomalous features outside it.Consequently,this paper proposes a Normalizing Flow-based Bidirectional Mapping Residual Network(NF-BMR).It utilizes pre-trained Convolutional Neural Networks(CNN)and normalizing flows to construct discriminative source and target domain feature spaces.Additionally,to better learn feature information in both domain spaces,we propose the Bidirectional Mapping Residual Network(BMR),which maps sample features to these two spaces for anomaly detection.The two detection spaces effectively complement each other’s deficiencies and provide a comprehensive feature evaluation from two perspectives,which leads to the improvement of detection performance.Comparative experimental results on the MVTec AD and DAGM datasets against the Bidirectional Pre-trained Feature Mapping Network(B-PFM)and other state-of-the-art methods demonstrate that the proposed approach achieves superior performance.On the MVTec AD dataset,NF-BMR achieves an average AUROC of 98.7%for all 15 categories.Especially,it achieves 100%optimal detection performance in five categories.On the DAGM dataset,the average AUROC across ten categories is 98.7%,which is very close to supervised methods.

Effect of normalizing cooling process on microstructure and precipitates in low-temperature silicon steel

Microstructure, precipitate and magnetic characteristic of fmal products with different normalizing cooling processes for Fe-3.2%Si low-temperature hot-rolled grain-oriented silicon steel were analyzed and compared with the hot-rolled plate by optical microscopy （OM）, transmission electron microscopy （TEM）, and energy dispersive spectrometry （EDS）. The results show that, the surface microstructure is uniform, the proportion of recrystallization in matrix increases, and the banding textures are narrowed; the precipitates, whose quantity in normalized plate is more than that in hot-rolled plate greatly, are mainly A1N, MnS, composite precipitates （Cu,Mn）S and so on. Normalizing technology with a temperature of 1120 ℃, holding for 3 min, and a two-stage cooling is a most advantaged method to obtain oriented silicon steel with sharper Goss texture and higher magnetic properties, owing to the uniform surface microstructures and the obvious inhomogeneity of microstructures along the thickness. The normalizing technology with the two-stage cooling is the optimum process, which can generate more fine precipitates dispersed over the matrix, and be beneficial for finished products to get higher magnetic properties.

Experimental Study on Coupled Cross-Flow and in-Line Vortex-Induced Vibration of Flexible Risers

In this work, we study the coupled cross-flow and in-line vortex-induced vibration （VIV） of a fixedly mounted flexible pipe, which is free to move in cross-flow （ Y- ） and in-line （ X- ） direction in a fluid flow where the mass and natural frequencies are precisely the same in both X- and Y-direction. The fluid speed varies from low to high with the corresponding vortex shedding frequency varying from below the first natural frequency to above the second natural frequency of the flexible pipe. Particular emphasis was placed on the investigation of the relationship between in-line and cross-flow vibration. The experimental results analyzed by using these measurements exhibits several valuable features.

The prediction on in-line vortex-induced vibration of slender marine structures

The in-line （IL） vortex-induced vibration （VIV） that occurs frequently in ocean engineering may cause severe fatigue damage in slender marine structures. To the best knowledge of the authors, in existing literatures, there is no efficient analytical model for predicting pure IL VIV. In this paper, a wake oscillator model capable of analyzing the IL VIV of slender marine structures has been developed. Two different kinds of van der Pol equations are used to describe the near wake dynamics related to the fluctuating nature of symmetric vortex shedding in the first excitation region and alternate vortex shedding in the second one. Some comparisons are carried out between the present model results and experimental data. It is found that many phenomena observed in experiments could be reproduced by the present wake oscillator model.

Ultrafiltration with in-line coagulation for the removal of natural humic acid and membrane fouling mechanism

Experimental and theoretical analysis were made on the natural humic acid removal and the membrane fouling of ultrafiltration （UF） with in-line coagulation. The results showed dissolved organic carbon （DOC） and UV254 removals by the UF with in-line coagulation at pH 7 were increased from 28% to 53% and 40% to 78% in comparison with direct UF treatment respectively. At the same time, the analysis of high performance liquid chromatography showed that UF with coagulation had significant improvement of removal of humic acid with molecular weights less than 6000 Da in particular. Compared to direct UF, the in-line coagulation UF also kept more constant permeate flux and very slight increase oftransmembrane pressure during a filtration circle. Two typical membrane fouling models were used by inducing two coefficients Kc and Kp corresponding to cake filtration model and pore narrowing model respectively. It was found that membrane fouling by pore-narrowing effect was effectively alleviated and that by cake-filtration was much decreased by in-line coagulation. Under the condition of coagulation prior to ultrafiltration at pH 7, the cake layer formed on the membrane surface became thicker, but the membrane filtration resistance was lower than that at pH 5 with the extension of operation time.

In-line response of vertical cylinders in regular and random waves

The in-line response of a vertical flexibly mounted cylinder in regular and random waves is reported. Both theoretical analyses and experimental measurements have been performed. The theoretical predictions are based on the Morison equation which is solved by the incremental harmonic balance method. Experiments are then performed in a wave flume to determine the accuracy of the Morison equation in predicting the in-line response of the cylinder in regular and random waves. The interaction between waves and vibrating cylinders are investigated.

Three-axis magnetic flux leakage in-line inspection simulation based on finite-element analysis

With the increase of pipelines, corrosion leakage accidents happen frequently. Therefore, nondestructive testing technology is important for ensuring the safe operation of the pipelines and energy mining. In this paper, the structure and principle of magnetic flux leakage （MFL） in-line inspection system is introduced first. Besides, a mathematic model of the system according to the ampere circuit rule, flux continuity theorem, and column coordinate transform is built, and the magnetic flux density in every point of space is calculated based on the theory of finite element analysis. Then we analyze and design the disposition of measurement section probes and sensors combining both three-axis MFL in-line inspection and multi-sensor fusion technology. Its advantage is that the three-axis changes of magnetic flux leakage field are measured by the multi-probes at the same time, so we can determine various defects accurately. Finally, the theory of finite element analysis is used to build a finite element simulation model, and the relationship between defects and MFL inspection signals is studied. Simulation and experiment results verify that the method not only enhances the detection ability to different types of defects but also improves the precision and reliability of the inspection system.

Nonlinear Coupled in-Line and Cross-Flow Vortex-Induced Vibration Analysis of Top Tensioned Riser

The fluctuating furces of the fluid exerted on the top terrsioned riser （＇FIR） in the in-line and cross-flow directions are both modeled by van del Pol wake oscillator model and the nonlinear coupled dynamics of the in-line and cross-flow vortex-induced vibrations （VIV） of the riser are analyzed in time domain in this papar. The numencal shnulation results of the riser＇s in-line and cross-flow displacements and curvatures are compared with experimental measurements and the comparison shows the validity of this method in modeling some main features of the riser＇s VIV. Finally, the effects of the riser＇s top tensions and internal flow velocities on the coupled vibrations of the riser are investigated.

Anisotropic total variation minimization approach in in-line phase-contrast tomography and its application to correction of ring artifacts

In-line phase-contrast computed tomography（IL-PC-CT） imaging is a new physical and biochemical imaging method.IL-PC-CT has advantages compared to absorption CT when imaging soft tissues. In practical applications, ring artifacts which will reduce the image quality are commonly encountered in IL-PC-CT, and numerous correction methods exist to either pre-process the sinogram or post-process the reconstructed image. In this study, we develop an IL-PC-CT reconstruction method based on anisotropic total variation（TV） minimization. Using this method, the ring artifacts are corrected during the reconstruction process. This method is compared with two methods： a sinogram preprocessing correction technique based on wavelet-FFT filter and a reconstruction method based on isotropic TV. The correction results show that the proposed method can reduce visible ring artifacts while preserving the liver section details for real liver section synchrotron data.

Comparison of up ladder type and terraced type normalizing heat treatments of heavy cylinder

Because of the mixed grain and coarse grain structure, the long heat treatment cycle and large energy conservation in the heavy cylinder heat treatment process, the up ladder type and terraced type normalizing heat treatment of heavy cylinder after rolling were put forward. The microstructure and mechanical properties of 2.25Cr1Mo0.25 V steel after the up ladder type normalizing, terraced type normalizing and isothermal type normalizing were studied. Experimental results show that： 1） For the grain refinement, the twice terraced type normalizing is better than the up ladder type and isothermal type normalizing, and the average grain size is 18 μm; 2） The yield strength, tensile strength and-30℃ charpy impact energy after twice terraced type normalizing are 681 MPa, 768 MPa and 181 J, respectively, and the mechanical properties are better than those of the up ladder type and isothermal type normalizing; 3） Compared with the isothermal type normalizing, the holding time of terraced type normalizing can be shortened by 30%, which greatly reduces the energy consumption.

Effect of Normalizing and Hardening on Mechanical Properties of Spring

This study was carried out to investigate the effect of heat treatment (Normalizing and Hardening) on the mechanical properties of springs. The springs were made from mild steel rod having a diameter of 6 mm, a total of 15 springs were made. The springs were then subjected to various heat treatment processes which included;normalizing, hardening and tempering. The heat treated springs were then subjected to various test in other to determine their mechanical properties, these included;impact toughness test, hardness test and tension test. The normalized spring had more strength, was harder and was much tougher than both the annealed and as received springs. The water quenched springs were the hardest of all the heat treated springs, were very brittle and had the lowest percentage elongation. Their strength was also lower than that of the normalized and as received springs. The water quenched and tempered springs had better mechanical properties required for spring making, they had the optimum combination of hardness, strength and toughness when compared with the other heat treated springs.

Determination of inorganic anions in ethyl acetate by in-line hollow fiber membrane extraction with ion chromatography

In this work, a novel hollow fiber membrane extractor was set up to extract inorganic anions from ethyl acetate using deionized water. Inorganic anions in slightly soluble organic solvents can be determined by the in-line hollow fiber membrane extractor coupled with ion chromatography at first time. Different aspects of the extraction procedure such as magnetic stirring speed, extraction flow rate and extraction time were optimized to achieve high extraction efficiency and good separation results. Satisfactory linear range, limits of detection and good repeatability were obtained. The procedure was applied to analyze inorganic anions in two commercial ethyl acetate samples.

New formulas for normalizing photon-added(-subtracted) two-mode squeezed thermal states

For the first time,we derive the compact forms of normalization factors for photon-added（-subtracted） two-mode squeezed thermal states by using the P-representation and the integration within an ordered product of operators（IWOP） technique.It is found that these two factors are related to the Jacobi polynomials.In addition,some new relationships for Jacobi polynomials are presented.

OpenNAU:An open-source platform for normalizing,analyzing,and visualizing cancer untargeted metabolomics data

Objective:As an important part of metabolomics analysis,untargeted metabolomics has become a powerful tool in the study of tumor mechanisms and the discovery of metabolic markers with high-throughput spectrometric data which also poses great challenges to data analysis,from the extraction of raw data to the identification of differential metabolites.To date,a large number of analytical tools and processes have been developed and constructed to serve untargeted metabolomics research.The different selection of analytical tools and parameter settings lead to varied results of untargeted metabolomics data.Our goal is to establish an easily operated platform and obtain a repeatable analysis result.Methods:We used the R language basic environment to construct the preprocessing system of the original data and the LAMP(Linux+Apache+MySQL+PHP)architecture to build a cloud mass spectrum data analysis system.Results:An open-source analysis software for untargeted metabolomics data(openNAU)was constructed.It includes the extraction of raw mass data and quality control for the identification of differential metabolic ion peaks.A reference metabolomics database based on public databases was also constructed.Conclusions:A complete analysis system platform for untargeted metabolomics was established.This platform provides a complete template interface for the addition and updating of the analysis process,so we can finish complex analyses of untargeted metabolomics with simple human-computer interactions.The source code can be downloaded from https://github.com/zjuRong/openNAU.

Normalizing Book Citations in Google Scholar: A Hybrid Cited-side Citing-side Method

Purpose: To design and test a method for normalizing book citations in Google Scholar.Design/methodology/approach: A hybrid citing-side, cited-side normalization method was developed and this was tested on a sample of 285 research monographs. The results were analyzed and conclusions drawn.Findings: The method was technically feasible but required extensive manual intervention because of the poor quality of the Google Scholar data. Research limitations: The sample of books was limited and also all were from one discipline —business and management. Also, the method has only been tested on Google Scholar, it would be useful to test it on Web of Science or Scopus.Practical limitations: Google Scholar is a poor source of data although it does cover a much wider range citation sources that other databases. Originality/value: This is the first method that has been developed specifically for normalizing books which have so far not been able to be normalized.

STUDY ON AUTOMATIC IN-LINE MEASUREMENT OF FeO CONTENT IN AGGLOMERATE

In this paper, the mechanism of physical method for measuring the FeO content in agglomerate replacing the chemical method is proposed after studying the electromagnetic property of the agglomerate. The microcomputer-measuring system for FeO content is provided. Attention is also paid to introducing the working principle of the H-type compensation sensor and the processing method of the measured data. This system has been successfully applied in practice to in-line measure the FeO content.

Robust adaptive output stabilization using dynamic normalizing signal

For a class of nonlinear systems with dynamic uncertainties, robust adaptive stabilization problem is considered in this paper. Firstly, by introducing an observer, an augmented system is obtained. Based on the system, we construct an exp-ISpS Lyapunov function for the unmodeled dynamics, prove that the unmodeled dynamics is exp-ISpS, and then obtain a dynamic normalizing signal to counteract the dynamic disturbances. By the backstepping technique, an adaptive controller is given, it is proved that all the signals in the adaptive control system are globally uniformly ultimately bounded, and the output can be regulated to the origin with any prescribed accuracy. A simulation example further demonstrates the efficiency of the control scheme.

In-line phase contrast for weakly absorbing materials with a microfocus x-ray source

For weakly absorbing materials, image contrast can be enhanced by phase contrast in formation. The effectiveness of the in-line phase contrast technique relies on its ability to record intensity data which contain information on the x- ray＇s phase shift. Four kinds of approaches to the relationship between intensity distribution and phase shift axe reviewed and discussed. A micro-focal x-ray source with high geometrical magnification is used to acquire phase contrast images. A great improvement on image quality is shown and geometrical parameters axe modified for comparison between different imaging positions.