We demonstrate an innovative preparation approach of diamond/Cu composites by powder-in-tube technique and rolling. A small copper tube was loaded with Ti- and Cu-coated diamond particles, mad then the diamond particl...We demonstrate an innovative preparation approach of diamond/Cu composites by powder-in-tube technique and rolling. A small copper tube was loaded with Ti- and Cu-coated diamond particles, mad then the diamond particles were combined with Cu matrix by composite rolling. The morphology and element distribution of the interface between diamond and Cu were determined by scanning electron microscopy and energy-dispersive spectrometer. Finite element method (FEM) simulation was used to analyze the rolling process associated with experiment by DEFORM-3D. The final experimental results showed that homogeneous distribution of diamond particles could be observed in the center layer of the composites. According to the contrast experiments, the sample, whose diamond particle size is 0.12-0.15 mm and thickness of pre-rolling is 1.2 mm, showed relatively complete morphologies and homogeneous distribution. Experimental results indicated a poor efficacy of excessive rolling reduction. The thermal conductivity of the composites is about 453 W (m K)-1 by theoretical calculation. For FEM simulation, roiling strain and temperature field of the composites were simulated by DEFORM-3D. Simulation results were interpreted, and numerical results verified the reliability of the model. The simulation predicted that the local area of large strain, indicative of the strain along the thickness direction, could be intensified by adding diamond particles.展开更多
文摘使用自主研发的快热快冷处理设备,对粉末装管Nb/Al前驱线进行快热快冷处理,然后再经过800℃10 h转变退火处理,得到具有Nb3Al超导相的超导短样.通过扫描电镜观察分析超导样品微观结构,发现所有样品均有Nb3Al相存在,但在靠近Ta管内层有少量的Nb2Al相,超导芯内有少量的Nb剩余.在制冷机冷却的环境下使用四引线法测试了样品的超导性能.结果表明,自场下在10.9 K温度时,没有铜稳定体的Nb3Al超导线最高临界电流密度是66.5 A/mm2,超导起始转变温度是15~18 K.
基金supported by the National Nature Science Foundation of China (Nos. 51174028 and 51541406)
文摘We demonstrate an innovative preparation approach of diamond/Cu composites by powder-in-tube technique and rolling. A small copper tube was loaded with Ti- and Cu-coated diamond particles, mad then the diamond particles were combined with Cu matrix by composite rolling. The morphology and element distribution of the interface between diamond and Cu were determined by scanning electron microscopy and energy-dispersive spectrometer. Finite element method (FEM) simulation was used to analyze the rolling process associated with experiment by DEFORM-3D. The final experimental results showed that homogeneous distribution of diamond particles could be observed in the center layer of the composites. According to the contrast experiments, the sample, whose diamond particle size is 0.12-0.15 mm and thickness of pre-rolling is 1.2 mm, showed relatively complete morphologies and homogeneous distribution. Experimental results indicated a poor efficacy of excessive rolling reduction. The thermal conductivity of the composites is about 453 W (m K)-1 by theoretical calculation. For FEM simulation, roiling strain and temperature field of the composites were simulated by DEFORM-3D. Simulation results were interpreted, and numerical results verified the reliability of the model. The simulation predicted that the local area of large strain, indicative of the strain along the thickness direction, could be intensified by adding diamond particles.