Research progress and application of deep in-situ condition preserved coring and testing

With the depletion of shallow resources,the exploration of deep earth resources has become a global strategy.The study of the different patterns in the physical mechanical properties of rocks at different occurrence depths is the basis for exploring deep into the earth,with the core and premise being the acquisition and testing of deep in-situ core specimens.Based on the original idea of deep in-situ condition preserved coring(ICP-Coring)and testing,combined with theoretical modeling,numerical analysis,test platform development,indoor testing and engineering application,the principles and technologies of deep ICP-Coring are developed.This principle and technology consists of five parts:in-situ pressurepreserved coring(IPP-Coring),in-situ substance-preserved coring(ISP-Coring),in-situ temperaturepreserved coring(ITP-Coring),in-situ light-preserved coring(ILP-Coring),and in-situ moisturepreserved coring(IMP-Coring).The theory and technology of temperature and pressure reconstruction at different occurrence depths and in different environments are proposed,and prototype trial production was completed by following the principle of displacement and tests based on the in-situ reconstructed environment.The notable advances are as follows:(1)Deep in-situ coring system:A pressure-preserved controller with an ultimate bearing capacity greater than 140 MPa,highperformance(temperature-resistant,pressure-resistant,and low thermally conductive)temperaturepreserved materials,an active temperature control system,and high-barrier quality-preserved membrane materials were developed;a deep ICP-Coring capacity calibration platform was independently developed,a deep in-situ coring technology system was developed,and the acquisition of deep in-situ cores was realized.(2)In-situ storage displacement system:Following the dual-circuit hydraulic design idea,a single-drive source push-pull composite grabbing mechanism was designed;the design of the overall structure for the deep in-situ displacement storage system and ultrahigh pressure cabin structure was completed,which could realize docking the coring device and core displacement in the in-situ reconstructed environment.(3)Test analysis system:A noncontact acoustic-electric-magnetic test system was developed under the in-situ reconstructed environment,and the errors between the test results and traditional contact test results were mostly less than 10%;a detachable deep in-situ core true triaxial test system was developed,which could perform loading tests for deep in-situ cores.The relevant technological achievements were successfully applied to the exploration and development of deep resources,such as deep mines,deep-sea natural gas hydrates,and deep oil and gas.The research results provide technical and equipment support for the construction of a theoretical system for deep in-situ rock mechanics,the development of deep earth resources and energy,and the scientific exploration of different layers and occurrence depths(deep and ultradeep)of the Earth.

Thermo-Mechanical Analyses of the High Heat Flux Component for ITER Dual Functional Lithium Lead Test Blanket Module

The finite element code ANSYS is used to calculate the temperature and stress distributions for the first wall of DFLL-TBM （dual functional lithium lead-test blanket module）, for testing in ITER. Preliminary analyses indicate that not only the low temperature design rules, the well-known 3Sin rules, are satisfied for the first wall, but the additional high temperature structural design criteria for the creep damage limits and creep-ratcheting limits are met as well.

Research on in-situ condition preserved coring and testing systems

As shallow resources are increasingly depleted,the mechanics'theory and testing technology of deep insitu rock has become urgent.Traditional coring technologies obtain rock samples without retaining the in-situ environmental conditions,leading to distortion of the measured parameters.Herein,a coring and testing systems retaining in-situ geological conditions is presented:the coring system that obtains in-situ rock samples,and the transfer and testing system that stores and analyzes the rocks under a reconstructed environment.The ICP-Coring system mainly consists of the pressure controller,active insulated core reactor and insulation layer and sealing film.The ultimate bearing strength of 100 MPa for pressurepreservation,temperature control accuracy of 0.97%for temperature-retained are realized.CH_(4)and CO permeability of the optimized sealing film are as low as 3.85 and 0.33 ppm/min.The average tensile elongation of the film is 152.4%and the light transmittance is reduced to 0%.Additionally,the pressure and steady-state temperature accuracy for reconstructing the in-situ environment of transfer and storage system up to 1%and±0.2 is achieved.The error recorded of the noncontact sensor ring made of lowdensity polymer is less than 6%than that of the contact test.The system can provide technical support for the deep in-situ rock mechanics research,improving deep resource acquisition capabilities and further clarifying deep-earth processes.

In-Situ Test on Fatigue Characteristics of Top-Mounted Dividable Pile-Board Subgrade for High-Speed Railway

To simulate the fatigue characteristics of the pile-board structure under long-term dynamic load, using the in-situ dynamic testing system DTS-1, the forced vibration loading was repeated one million times at different cross-sections of the pile-board structure for high-speed railway. The dynamic deformation, permanent deformation and dynamic stress of main reinforcements were measured. The test results show that the dynamic responses of the pile-board structure almost did not vary with the forced vibration times under the simulated trainload. After one million times of forced vibration, the permanent deformations of the midspan section of intermediate span and midspan section of side span were 0.7 mm and 0. 6 mm, respectively, and there was no accumulative plastic deformation at the bearing section of intermediate span.

Effects of temperature and wavelength choice on in-situ dissolution test of Cimetidine tablets

The effects of temperature and wavelength choice on in-situ dissolution test instrument of Cimetidine were studied. Absorbance （A）〈 1.0 is required when using a fiber-optic dissolution test system. The detection wavelength of 2 （218 nm） was replaced by 244 nm to carry out this test. The absorbance of Cimetidine solution at different temperature showed an obvious change. Calibration of Cimetidine solution should be tested at the same temperature （37° C） with the test solution. A suitable wavelength with smaller tangent slope could be chosen for in-situ dissolution test of Cimetidine tablets.

Research of in-situ hydraulic test method by using double packer equipment

Double packer equipment for hydraulic test can be used to measure pressure of test zone directly, and it is frequently used to perform many kinds of hydraulic tests and take groundwater sample from borehole. The test method of this equipment mainly includes the test design, implementation, interpretation and synthetic analysis. By adopting the double packer equipment for hydraulic test, the parameter distribution of rock permeability along borehole can be acquired, as well as the connectivity, water conductivity and water bearing capacity of the disclosed structure and the chemical characteristics of the deep groundwater. It is a necessary method for the research and evaluation of the complex hypotonicity terrace site selection under geological conditions. This method is not only suitable for the geological disposal of high level radioactive waste, but also can be used in the site selection of underground facilities such as storage of petroleum and carbon dioxide. Meanwhile, it has a good application prospect in other hydrogeological investigation fields.

Design and feasibility analysis of a new completion monitoring technical scheme for natural gas hydrate production tests

As a prerequisite and a guarantee for safe and efficient natural gas hydrates(NGHs)exploitation,it is imperative to effectively determine the mechanical properties of NGHs reservoirs and clarify the law of the change in the mechanical properties with the dissociation of NGHs during NGHs production tests by depressurization.Based on the development of Japan’s two offshore NGHs production tests in vertical wells,this study innovatively proposed a new subsea communication technology-accurate directional connection using a wet-mate connector.This helps to overcome the technical barrier to the communication between the upper and lower completion of offshore wells.Using this new communication technology,this study explored and designed a mechanical monitoring scheme for lower completion(sand screens).This scheme can be used to monitor the tensile stress and radial compressive stress of sand screens caused by NGHs reservoirs in real time,thus promoting the technical development for the rapid assessment and real-time feedback of the in-situ mechanical response of NGHs reservoirs during offshore NGHs production tests by depressurization.

In-situ Horizontal Extrusion Test of Herbaceous Root-Soil with Different Root Types

The influence of different types of roots on the soil is complex and still remains unclear.Four in-situ extrusion tests were conducted on two types of root systems,namely fibrous and tap root system,for three plants,Eleusine indica,Potentilla anserine,and Artemisia argyi,according to the classification in Botany,and the thrust-displacement curves and failure patterns of different samples were analysed by comparison to fill the aforementioned gap.Results reveal that the roots can reduce the characteristics of soil brittleness and enhance its capability to resist large deformation,and different root types contribute different effects to the strain-hardening behavior of the root-soil mass.The contribution of the fibrous root system to strength is limited,whilst the tap root system substantially enhances strength and stiffness.Results of failure patterns show that fibrous and tap root systems affect soil solidification and surface cracking reduction.However,the effect of the tap root system depends on the composition of lateral and tap roots:long and rich lateral roots are effective for resisting the creation of cracks,but thick tap roots with few and thin lateral roots may lead to several surface cracks.

In-situ analysis of slip transfer and heterogeneous deformation in tension of Mg-5.4Gd-1.8Y-1.5Zn alloy

Slip transfer is influential in determining damage nucleation of polycrystalline material.The interactions between dislocations and grain boundaries(GBs)was investigated using in-situ tension test in a multi-directionally forged Mg-5.4Gd-1.8Y-1.5Zn(wt%)alloy.It was found that strain accommodation of individual grains by means of slip occurred more easily than slip transfer when several slip systems were operable.The basal-basal slip transfer occurred when the GB misorientation was smaller than 34.2°,whereas basal-pyramidal type took place when the crystallographic misorientation was larger than 48.8°.The product of Luster-Morris m factor and the sum of the Schmid factors of the two correlated slip systems indicated that the threshold for basal-basal slip transfer may exist,however,basal-pyramidal slip transfer shows no such threshold and is more complicated.These results presented here demonstrated that besides the geometrical alignment,the deformation details(such as the number of operable slip systems)and stress state in each individual grain must be considered.

Study on Temperature Distribution of Specimens Tested on the Gleeble 3800 at Hot Forming Conditions

Taking Ti-6Al-4V specimens into consideration, the coupled thermal-electrical finite element model has been developed in Abaqus/Explicit to simulate the heating process in Gleeble 3800 and to study the temperature history and distribution in the specimen. In order to verify the finite element （FE） results, thermal tests are carried out on Gleeble 3800 for a Ti-6Al-4V specimen with a slot to in the centre of the specimen. The effects of the specimen size, heating rate, and air convection on the temperature distribution over the specimen have been investigated. The conclusions can be drawn as： the temperature gradient of the specimen decreases as the specimen size, heating rate, and vacuuming decrease.

In-situ three-dimensional visualization of dynamic tension deformation in ferrite stainless steels

An improved three-dimensional （3-D） experimental visualization methodology is presented tor evaluating the fracture mechanisms of ferritic stainless steels by in-situ tensile testing with an environmental scanning electron microscope （ESEM）. The samples were machined with a radial notched shape and a sloped surface. Both planar surface deformation and sloping surface deformation-induced microvoids were observed during dynamic tension experiments, where a greater amount of information could be obtained from the sloping surface. The results showed that microvoids formed at the grain boundaries of highly elongated large grains. The microvoids nucleated in the severely deformed regions grew nearly parallel to the tensile axis, predominantly along the grain boundaries. The microvoids nucleated at the interface of particles and the matrix did not propagate due to the high plasticity of the matrix. The large microvoids propagated and showed a zigzag shape along the grain boundaries,seemingly a consequence of the fracture of the slip bands caused by dislocation pile-ups. The final failure took place due to the reduction of the load-beating area.

Study on Shear Strength Characteristics of Columnar Jointed Basalt Based on in-situ Direct Shear Test at Baihetan Hydropower Station

Columnar jointed basalt(CJB) widely distributes in the dam site of the Baihetan Hydropower Station.The columnar joint structure and fracture development of CJB have significant influence on the mechanical properties of rock mass,and the mechanical properties of CJB are of great significance to the Baihetan Hydropower Project.Therefore,in-situ direct shear tests were carried out on ten test adit at different locations in the dam site area to study the shear behavior of CJB.In this study,21 sets of in-situ direct shear tests were conducted for rock types of type Ⅱ_(2),type Ⅲ_(1)and type Ⅲ_(2),with horizontal and vertical shear planes and two different specimen sizes of CJB.Shear strength parameters of CJB were obtained by linear fitting of in-situ direct shear test results based on the Mohr-Coulomb strength criterion.The results indicate that the shear strength parameters of CJB with horizontal shear plane increase as the increase of rock type grade.The shear strength parameters of CJB show obvious anisotropy and the friction coefficient of the horizontal shear plane is greater than the vertical shear plane.The friction coefficient in the horizontal direction of the shear plane is 1.27 times that in the vertical direction of the shear plane.With the increase of rock type grade,the difference of friction coefficient becomes larger.However,the cohesion changes little whether the shear plane is horizontal or vertical.In addition,the size effect of CJB in this area is significant.The shear strength parameters of large size(100 cm × 100 cm) specimens are lower than those of regular size(50 cm × 50 cm) specimens.The reduction of cohesion is greater than that of the friction coefficient.For rock type Ⅲ_(2),the cohesion of large-size specimens is 0.637 of the regular-size specimens.The reduction percentage of the friction coefficient for type Ⅲ_(2)is 1.66 times that of type Ⅲ_(1).The reduction percentage of the cohesion for type Ⅲ_(2)is 1.27 times that of type Ⅲ_(1).The size effect decreases with the increase of rock type grade.The research results of this study can provide an important basis for the selection of rock mechanics parameters in the dam site area of Baihetan Hydropower Station and the stability analysis of the dam foundation and rocky slopes.

Stability analysis of gravity anchor foundation of layered argillaceous sandstone under dry-wet cycles

To investigate the stability of gravity anchors of suspension bridges,in-situ tests of the vertical bearing capacity of the bedrock,shear resistance of the anchor-rock interface,shear resistance of the bedrock were conducted in a suspension bridge project.Under dry-wet cycles,the deterioration law of the mechanical properties of argillaceous sandstone was identified in laboratory tests:the elastic modulus,cohesion and friction of the argillaceous sandstone deteriorated significantly at first few dry-wet cycles and then declined slowly after 10 cycles,ultimately these three mechanical parameters were reduced to about 1/3,1/3,2/3 of the initial value respectively.Moreover,numerical simulation was used to restore in-situ shear tests and a good agreement was obtained.Base on the results of in-situ and laboratory tests,the stability of the gravity anchor foundation under natural conditions and drywet cycles was calculated and its failure modes were analyzed.The results demonstrated that the dry-wet cycles caused uneven settlement of the anchor foundation,resulting in more serious stress concentration in the substrate.The dry-wet cycles remarkably reduced the stability coefficient of the anchor foundation,whose failure mode shifted from overturning failure under natural conditions to sliding failure.When there was weak interlayer in the rock layer,the anti-sliding stability of the anchor foundation was affected drastically.

Comparison on crack propagation under tension at 150℃ of Mg-2Zn-1.5Mn alloy sheets with and without crack notch

Generally,edge crack of rolled magnesium alloy sheets initiates in the RD(rolling direction)-ND(normal direction)plane and then propagate in the RD-TD(transverse direction)plane.Hence,the Mg-2Zn-1.5Mn(ZM21)alloy sheets with and without crack notch were designed to carry out in-situ tensile experiments under 150℃(the same temperature of rolling),with the aim to understand their crack propagation mechanism.The scanning electron microscopy(SEM)and electron backscattered diffraction(EBSD)techniques were utilized to reveal microstructural evolution in real time at designated displacements.The results show that the prismatic slip,basal slip,and extension twining play synergistic role in coordinating strain during the tensile process in ZM21 alloy sheet at 150℃.In both tensile samples with and without crack notch,localized strain is mainly concentrated at relatively fine grain area and the grain boundaries or triple junctions of the grains with large basal Schmid factor(SF)difference,which eventually leads to severe surface roughening and subsequent crack initiation.Compared with the sample without crack notch,the pre-cracked sample exhibits severer deformation at the crack tip due to strain concentration.Strain gradient distribution is observed at the crack tip region in the pre-cracked sample.The crack propagation path of the sample with pre-crack is identified and the underlying mechanism is also discussed.

Deformation Mechanism of Bimodal Structured 2205 Duplex Stainless Steel in Two Yield Stages

A kind of micro/nanostructured 2205 duplex stainless steel(DSS)with uniform distribution of nanocrystals was prepared via aluminothermic reaction method.The analysis of stress-strain curve showed that the fracture strength and elongation of the specimen were 946 MPa and 24.7%,respectively.At present,the research on microstructure of bimodal 2205 DSS at room temperature(RT)mainly depended on scanning electron microscope(SEM)observation after loading experiments.The test result indicates that there are two different yield stages in stress-strain curve of specimen during tensile process.The microstructure of duplex bimodal structured stainless steel consists of two pairs of soft hard regions and phases.By studying deformation mechanism of bimodal structured stainless steel,the interaction between soft phase and hard phase are discussed.The principle of composition design and microstructure control of typical duplex stainless steel is obtained,which provides an important research basis for designing of advanced duplex stainless steel.

通信系统原位检测中的信号源设计

文章介绍DDS工作原理和AD9954、 AD9959的特性,论述信号源硬件设计、调频软件设计和性能分析。该信号源具有结构简单、频率分辨率高、功耗低、输出频率信号相位连续、频率转换时间短、调制简单灵活等优点,实现通信系统原位检测的功能需求。

SHAPE MEMORY EFFECT OF PU IONOMERS WITH IONIC GROUPS ON HARD-SEGMENTS

SMPU （shape memory polyurethane） non-ionomers and ionomers, synthesized with poly（c-caprolactone） （PCL）, 4, 4＇-diphenylmethane diisocyanate （MDI）, 1,4-butanediol （BDO）, dimethylolpropionic acid （DMPA） were measured with cyclic tensile test and strain recovery test. The relations between the structure and shape memory effect of these two series were studied with respect to the ionic group content and the effect of neutralization. The resulting data indicate that, with the introduction of asymmetrical extender, the stress at 100% elongation is decreased for PU non-ionomer and ionomer series, especially lowered sharply for non-ionomer series; the fixation ratio of ionomer series is not affected obviously by the ionic group content; the total recovery ratio of ionomer series is decreased greatly. After sufficient relaxation time for samples stretched beforehand, the switching temperature is raised slightly, whereas the recovery ratio measured with strain recovery test method is lowered with increased DMPA content. The characterization with FT-IR, DSC, DMA elucidated that, the ordered hard domain of the two series is disrupted with the introduction of DMPA which causes more hard segments to dissolve in soft phase; ionic groups on hard segment enhance the cohesion between hard segments especially at high ionic group content and significantly facilitate the phase separation compared with the corresponding non-ionomer at moderate ionic group content.

A MEMS Device for in-situ TEM Test of SCS Nanobeam

In-situ tensile testing in TEM (transmission electron microscopy) is a useful tool for studying mechanical properties of nano-structures because it can provide quanti-tative information on sample deformation at atomic scale. To facilitate in-situ TEM tensile tests of SCS (single crystal silicon) nanobeam, a MEMS tensile-testing chip was designed and fabricated. The chip was fabricated by means of bulk micro-machining and wafer bonding techniques. An SCS nanobeam, a comb drive ac-tuator, a force sensor beam and an electron beam window were integrated into the chip. With the on-chip comb-drive-actuator stretching the nanobeam and in-situ TEM observation, tensile test on a 90 nm-thick nanobeam was performed and the strain-stress relationship was obtained. The Young's modulus was fitted to be 161 GPa and did not show the size effect.

A Li-S battery with ultrahigh cycling stability and enhanced rate capability based on novel ZnO yolk-shell sulfur host

Currently,lithium-sulfur(Li-S)batteries still suffer from fast capacity decay,poor coulombic efficiency(CE)and short cycling lifespan,which result from the severe shuttle effect issue caused by high solubility and rapid diffusion of lithium polysulfides(Li PSs)in organic electrolytes.Here,yolk-shell zinc oxide(YSZn O)spheres are synthesized and for the first time,applied as a host for Li-S batteries to tackle this challenge.The polar Zn O exhibits high chemical anchoring ability toward Li PSs while the unique yolk-shell structure not only provides an additional physical barrier to Li PSs but also enables much more uniform sulfur distribution,thus significantly suppressing Li PSs shuttling effect meanwhile promoting sulfur conversion reactions.As a result,the YS-Zn O enables the Li-S battery to display an initial specific capacity of1355 m Ah g^(-1) and an outstanding capacity retention capability(~89.44%retention rate)even after 500 cycles with the average CE of~99.46%at the current of 0.5 C.By contrast,the capacity of conventional-Zn O-nanoparticles based battery severely decays to 472 m Ah g^(-1) after cycling for 500 times.More impressively,the S/YS-Zn O based Li-S battery can maintain a low decay rate of 0.040%every cycle and high average CE of 98.82%over 1000 cycles at 3 C.

Influence of deviatoric stress on rockburst occurrence:An experimental study

As mining delves deeper into the crust, it is necessary to investigate the complex rock responses associated with higher stress gradients. Therefore, it is essential to better understand the mechanisms associated with the rockburst phenomenon. However, due to the large-scale and difficult monitoring of real mining excavations, laboratory scale tests must be utilised to determine the conditions conducive to burst. To this end, this research focuses on the implementation of a new rockburst testing apparatus to replicate the stress conditions of a rock mass excavation at the time of bursting. This apparatus allows the determination of rockburst stresses and a relationship between deviatoric stress and in-situ pressure/depth. Using this relationship it is then possible to estimate the standardised stress levels for a certain rock type which might lead to rockburst occurrence. Furthermore, it is demonstrated that with increasing in-situ pressure, the likelihood(measured as a lower differential stress) and the extent(indicated by the increasing range of deviatoric stress) of rockburst increases. These findings provide valuable information about the conditions necessary for bursting in deep mining.