Dose inter-comparison studies for Co γ-ray and 10 MeV electron beam irradiation were carried out 60 from July to October in 2002. The purpose of the studies was to check the reliability of the alanine-PE film dosime-...Dose inter-comparison studies for Co γ-ray and 10 MeV electron beam irradiation were carried out 60 from July to October in 2002. The purpose of the studies was to check the reliability of the alanine-PE film dosime- ters made by CIAE, which will be used as transfer standard dosimetry system mainly for electron beam irradiation. The expanded uncertainty of CIAE alanine/EPR dosimetry system was 4.1% for doses not higher than 10 kGy and 5.4% for those above 10 kGy (k=2). CIAE alanine-PE film dosimeters were sent to JAERI, RISO (National Labora- tory in Denmark) and INCT respectively, which were irradiated by Co gamma-rays or electron beams in each labo- 60 ratory. The irradiated dosimeters were then sent back to CIAE for electron paramagnetic resonance (EPR) analysis. The agreements were obtained to be ±1.9% for gamma-ray dose measurement and ±4.3% for electron beam dose measurement, which were all within the combined uncertainty of the reference and CIAE alanine/EPR dosimetry system. Furthermore, the overall mean ratio was found to be 0.995 with 1.8% in the coefficient of variation (CV). The preliminary inter-comparison studies indicated that CIAE film alanine/EPR dosimetry system had the potential to be used as a transfer dosimetry system for high dose measurement.展开更多
An inter-laboratory comparison of the AOAC mouse bioassay for paralytic shellfish poisoning (PSP) toxicity in shellfish was carried out among 25 Chinese laboratories to examine the overall performance for PSP testing ...An inter-laboratory comparison of the AOAC mouse bioassay for paralytic shellfish poisoning (PSP) toxicity in shellfish was carried out among 25 Chinese laboratories to examine the overall performance for PSP testing in China, and to analyze the main factors affecting the performance of this method. The toxic scallop Patinopecten yessoensis collected from coast of Bohai Sea, China, was used as a test sample in the comparison study. The results were reported and evaluated using robust statistical methods. The z scores showed that 80%, 8%, and 12% of laboratories reported satisfactory results, unsatisfactory results, and questionable results, respectively. This evaluation demonstrates that the PSP mouse bioassay is an appropriate method for screening and testing PSP toxicity in shellfish. However, it was found that the experience and skill of technicians, as well as the body weight and health status of mice being used significantly affected the accuracy of the method.展开更多
The successful launch and commissioning of the first geostationary meteorological satellite of Korea has the potential to enhance earth observation capability over the Asia Pacific region. Although the specifications ...The successful launch and commissioning of the first geostationary meteorological satellite of Korea has the potential to enhance earth observation capability over the Asia Pacific region. Although the specifications of the payload, the meteorological imager(MI), have been verified during both ground and in-orbit tests, there is the possibility of variation and/or degradation of data quality due to many different reasons, such as the accumulation of contaminants, the aging of instrument components, and unexpected external disturbance. Thus, for better utilization of MI data, it is imperative to continuously monitor and maintain the data quality. As a part of such activity, this study presents an inter-calibration, based on the Global Space-based Inter-Calibration System(GSICS), between the MI data and the high quality hyperspectral data from the Infrared Atmospheric Sounding Interferometer(IASI) of the Metop-A satellite. Both sets of data, acquired for three years from April 2011 to March 2014, are processed to prepare the matchup dataset, which is spatially collocated, temporally concurrent,angularly coincident, and spectrally comparable. The results show that the MI data are stable within the specifications and show no significant degradation during the study period. However, the water vapor channel shows a rather large bias value of-0.77 K, with a root-mean-square difference(RMSD) of around 1.1 K, which is thought to be due to the shift in the spectral response function. The shortwave channel shows a maximum RMSD of around 1.39 K, mainly due to the coarse digitization at the lower temperature. The inter-comparison results are re-checked through a sensitivity analysis with different sets of threshold values used for the matchup dataset. Based on this, we confirm that the overall quality of the MI data meets the user requirements and maintains the expected performance, although the water vapor channel requires further investigation.展开更多
《能力验证规则》CNAS-RL02:2007中明确规定,申请认可的实验室和已经通过认可的实验室要证明其在该领域具有的检验能力,参加能力验证、测量审核、与权威机构比对以及多家实验室间数据比对等系列质量活动是必经之路。在合成橡胶行业通过...《能力验证规则》CNAS-RL02:2007中明确规定,申请认可的实验室和已经通过认可的实验室要证明其在该领域具有的检验能力,参加能力验证、测量审核、与权威机构比对以及多家实验室间数据比对等系列质量活动是必经之路。在合成橡胶行业通过国家认可实验室较少,组织能力验证活动比较困难,为了满足合成橡胶行业有关生产企业及相关实验室的要求,国家合成橡胶质检中心牵头组织苯乙烯-丁二烯橡胶(SBR)1502产品全项分析实验室间数据比对。数据比对结果采用稳健统计技术进行了统计和分析,所有参加比对的实验室代表了该行业的测试水平。生胶门尼粘度、灰分、混炼胶门尼粘度和50 min 300%定伸应力等测试项目的测定结果较理想;挥发份、25 min 300%定伸应力、35 min 300%定伸应力、35 min拉伸强度和35 min扯断伸长率等测试项目出现的问题相对较多,均有两个以上实验室出现可疑值或离群值;部分实验室尚缺乏化学分析测试能力,应加强相关内容的培训,补充实验仪器的配置,积极参与实验室间比对,不断提高实验室化学分析测试水平。展开更多
The HAZ microstructure and performance of Quenching and Tempering mode temper bead welding and general welded joints which were made on SA508-3 steel of 60 mm thickness were compared in this article. The result shows ...The HAZ microstructure and performance of Quenching and Tempering mode temper bead welding and general welded joints which were made on SA508-3 steel of 60 mm thickness were compared in this article. The result shows that tempering sorbite which has excellent overall performance was obtained in both modes. The microstructure of Quenching and Tempering mode welded joints got more fine grain. Even though the hardness of tempering bead welded joints is higher than the general one,it still meets the standards which is lower than 350 HV. The impact absorbing energy of each district of tempering bead welded joints HAZ reached 170 J,which is equal to general one.展开更多
文摘Dose inter-comparison studies for Co γ-ray and 10 MeV electron beam irradiation were carried out 60 from July to October in 2002. The purpose of the studies was to check the reliability of the alanine-PE film dosime- ters made by CIAE, which will be used as transfer standard dosimetry system mainly for electron beam irradiation. The expanded uncertainty of CIAE alanine/EPR dosimetry system was 4.1% for doses not higher than 10 kGy and 5.4% for those above 10 kGy (k=2). CIAE alanine-PE film dosimeters were sent to JAERI, RISO (National Labora- tory in Denmark) and INCT respectively, which were irradiated by Co gamma-rays or electron beams in each labo- 60 ratory. The irradiated dosimeters were then sent back to CIAE for electron paramagnetic resonance (EPR) analysis. The agreements were obtained to be ±1.9% for gamma-ray dose measurement and ±4.3% for electron beam dose measurement, which were all within the combined uncertainty of the reference and CIAE alanine/EPR dosimetry system. Furthermore, the overall mean ratio was found to be 0.995 with 1.8% in the coefficient of variation (CV). The preliminary inter-comparison studies indicated that CIAE film alanine/EPR dosimetry system had the potential to be used as a transfer dosimetry system for high dose measurement.
基金Supported by a thesis research project of General Administration of Quality Supervision, Inspection and Quarantine of China (No. 2010IK168)
文摘An inter-laboratory comparison of the AOAC mouse bioassay for paralytic shellfish poisoning (PSP) toxicity in shellfish was carried out among 25 Chinese laboratories to examine the overall performance for PSP testing in China, and to analyze the main factors affecting the performance of this method. The toxic scallop Patinopecten yessoensis collected from coast of Bohai Sea, China, was used as a test sample in the comparison study. The results were reported and evaluated using robust statistical methods. The z scores showed that 80%, 8%, and 12% of laboratories reported satisfactory results, unsatisfactory results, and questionable results, respectively. This evaluation demonstrates that the PSP mouse bioassay is an appropriate method for screening and testing PSP toxicity in shellfish. However, it was found that the experience and skill of technicians, as well as the body weight and health status of mice being used significantly affected the accuracy of the method.
基金supported by the project entitled "Development of Meteorological Satellite Operation and Application Technology" of the KMA/NMSC (Korea Meteorological Adminstration/National Meteorological Satellite Center)supported by the Eco Innovation Program of KEITI (Korea Environmental Industry & Technology Institute) (Grant No. 2013000160002)
文摘The successful launch and commissioning of the first geostationary meteorological satellite of Korea has the potential to enhance earth observation capability over the Asia Pacific region. Although the specifications of the payload, the meteorological imager(MI), have been verified during both ground and in-orbit tests, there is the possibility of variation and/or degradation of data quality due to many different reasons, such as the accumulation of contaminants, the aging of instrument components, and unexpected external disturbance. Thus, for better utilization of MI data, it is imperative to continuously monitor and maintain the data quality. As a part of such activity, this study presents an inter-calibration, based on the Global Space-based Inter-Calibration System(GSICS), between the MI data and the high quality hyperspectral data from the Infrared Atmospheric Sounding Interferometer(IASI) of the Metop-A satellite. Both sets of data, acquired for three years from April 2011 to March 2014, are processed to prepare the matchup dataset, which is spatially collocated, temporally concurrent,angularly coincident, and spectrally comparable. The results show that the MI data are stable within the specifications and show no significant degradation during the study period. However, the water vapor channel shows a rather large bias value of-0.77 K, with a root-mean-square difference(RMSD) of around 1.1 K, which is thought to be due to the shift in the spectral response function. The shortwave channel shows a maximum RMSD of around 1.39 K, mainly due to the coarse digitization at the lower temperature. The inter-comparison results are re-checked through a sensitivity analysis with different sets of threshold values used for the matchup dataset. Based on this, we confirm that the overall quality of the MI data meets the user requirements and maintains the expected performance, although the water vapor channel requires further investigation.
文摘《能力验证规则》CNAS-RL02:2007中明确规定,申请认可的实验室和已经通过认可的实验室要证明其在该领域具有的检验能力,参加能力验证、测量审核、与权威机构比对以及多家实验室间数据比对等系列质量活动是必经之路。在合成橡胶行业通过国家认可实验室较少,组织能力验证活动比较困难,为了满足合成橡胶行业有关生产企业及相关实验室的要求,国家合成橡胶质检中心牵头组织苯乙烯-丁二烯橡胶(SBR)1502产品全项分析实验室间数据比对。数据比对结果采用稳健统计技术进行了统计和分析,所有参加比对的实验室代表了该行业的测试水平。生胶门尼粘度、灰分、混炼胶门尼粘度和50 min 300%定伸应力等测试项目的测定结果较理想;挥发份、25 min 300%定伸应力、35 min 300%定伸应力、35 min拉伸强度和35 min扯断伸长率等测试项目出现的问题相对较多,均有两个以上实验室出现可疑值或离群值;部分实验室尚缺乏化学分析测试能力,应加强相关内容的培训,补充实验仪器的配置,积极参与实验室间比对,不断提高实验室化学分析测试水平。
基金supported by the Key State Science and Technology Projects(Grant No.2011ZX04016-061 and No.2012ZX06004-001-001-005)
文摘The HAZ microstructure and performance of Quenching and Tempering mode temper bead welding and general welded joints which were made on SA508-3 steel of 60 mm thickness were compared in this article. The result shows that tempering sorbite which has excellent overall performance was obtained in both modes. The microstructure of Quenching and Tempering mode welded joints got more fine grain. Even though the hardness of tempering bead welded joints is higher than the general one,it still meets the standards which is lower than 350 HV. The impact absorbing energy of each district of tempering bead welded joints HAZ reached 170 J,which is equal to general one.
