The low temperature coal tar(CT)is taken as the raw material,and the extraction and column chromatography are used for detailed and accurate characterization in this paper.The n-heptane soluble fraction(CT-HS)and inso...The low temperature coal tar(CT)is taken as the raw material,and the extraction and column chromatography are used for detailed and accurate characterization in this paper.The n-heptane soluble fraction(CT-HS)and insoluble fraction(CT-HI)were obtained by n-heptane Soxhlet extraction.The extraction rate of CT-HS reached 92.79%(mass),which indicated that there are few heavy compounds in it.Further,different solvents(methylbenzene,benzene,ethyl acetate,methylbenzene-ethanol)were used to elute CT-HS by chromatographic column to obtain five fractions(saturates,aromatics,heteroatoms,phenolics and resins,named CT-SA,CT-AR,CT-HE,CT-PH,CT-RE,respectively).The yields of CTSA,CT-AR,CT-HE,CT-PH,CT-RE are 42.12%,10.43%,2.19%,9.50%and 6.63%(mass),respectively.Gas chromatography-mass spectrometry analysis of eluting components show that alkanes are the main components in CT,followed by polycyclic aromatics,and the corresponding fractions are CT-SA and CT-AR,respectively.The relative content of aliphatics in CT-SA is 76.93%,and the relative content of aromatics in CT-AR is 75.05%.This separation technology effectively separates and enriches different components in CT,and the activation energy required for the pyrolysis process of a single eluting fraction is lower than that of CT,which is expected to provide an important reference for the separation,analysis and conversion of complex oil products such as coal-oil co-processing products,coal tar and other complex heavy carbon oil products.展开更多
This paper focuses on the investigation of a hybrid seismic isolation system with passive variable friction dampers for protection of structures against near fault earthquakes. The seismic isolation can be implemented...This paper focuses on the investigation of a hybrid seismic isolation system with passive variable friction dampers for protection of structures against near fault earthquakes. The seismic isolation can be implemented by replacing the conventional columns fixed to the foundations by seismic isolating ones. These columns allow horizontal displacement between the superstructure and the foundations and decouple the building from the damaging earthquake motion. As a result, the forces in the structural elements decrease and damage that may be caused to the building by the earthquake significantly decreases. However, this positive effect is achieved on account of displacements occurring in the isolating columns. These displacements become very large when the structure is subjected to a strong earthquake. In this case, impact may occur between the parts of the isolating column yielding their damage or collapse. In order to limit the displacements in the isolating columns, it is proposed to add variable friction dampers. A method for selecting the dampers＇ properties is proposed. It is carried out using an artificial ground motion record and optimal active control algorithm. Numerical simulation of a sevenstory structure shows that the proposed method allows efficient reduction in structural response and limits the displacements at the seismic isolating columns.展开更多
Isolation of high quality DNA from multiple samples can be both time-consuming and expensive. We have developed a combined protocol to reduce the time component of the hexadecyltrimethylammonium bromide （CTAB） extra...Isolation of high quality DNA from multiple samples can be both time-consuming and expensive. We have developed a combined protocol to reduce the time component of the hexadecyltrimethylammonium bromide （CTAB） extraction method and reduced costs by regenerating the silica columns used to purify genomic DNA. We present data that shows, by in- creasing the temperature used during the CTAB method, the time required to extract crude genomic DNA can be reduced. We show that silica columns can be regenerated using HCI and still maintain their DNA-binding capacity. Furthermore, we show both spectrophotometrically, and by restriction enzyme cutting, that the quality of the eluted DNA is high. Critically, using both genomic DNA from pea and perennial ryegrass we demonstrate, using species-specific PCR primers, that there is no carry-over of DNA from repeated use of a single column. The main advantages of the method are high yield, high quality, cost effectiveness and time-saving. This method could satisfy demand when large numbers of plant genomic DNA samples are required, for example from targeting induced local lesions in genomes （TILLING） populations.展开更多
A full-scale composite floor plate was tested to investigate the flexural behavior and in-plane effects of the floor slab in a grillage of composite beams that reduces the tendency for longitudinal splitting of the co...A full-scale composite floor plate was tested to investigate the flexural behavior and in-plane effects of the floor slab in a grillage of composite beams that reduces the tendency for longitudinal splitting of the concrete slab along the line of the primary beams. This is important in cases where the steel decking is discontinuous when it is orientated parallel to the beams. In this case, it is important to demonstrate that the amount of transverse reinforcement required to transfer local forces from the shear connectors can be reduced relative to the requirements of Eurocode 4. The mechanism under study involved in-plane compression forces being developed in the slab due to the restraining action of the floor plate, which was held in position by the peripheral composite beams;while the secondary beams acted as transverse ties to resist the forces in the floor plate that would otherwise lead to splitting of the slab along the line of the primary beams. The tendency for cracking along the center line of the primary beam and at the peripheral beams was closely monitored. This is the first large floor plate test that has been carried out under laboratory conditions since the Cardington tests in the early 1990s, although those tests were not carried out to failure. This floor plate test was designed so that the longitudinal force transferred by the primary beams was relatively high (i.e., it was designed for full shear connection), but the transverse reinforcement was taken as the minimum of 0.2% of the concrete area. The test confirmed that the primary beams reached their plastic bending resistance despite the discontinuous decking and transverse reinforcement at the minimum percentage given in Eurocode 4. Based on this test, a reduction factor due to shear connectors at edge beams without U-bars is proposed.展开更多
In the SILER （Seismic-Initiated events risk mitigation in LEad-cooled Reactors） Project, it is interesting to apply seismic isolation technology for the reactor assembly of the fixed base reactor building for ADS （...In the SILER （Seismic-Initiated events risk mitigation in LEad-cooled Reactors） Project, it is interesting to apply seismic isolation technology for the reactor assembly of the fixed base reactor building for ADS （Acceleration Driven System） heavy liquid reactor MYRRHA （Multipurpose Hybrid Research Reactor for High-Tech Application） which contains the most critical safety related components, such as reactor vessel, safe shutdown and control rod mechanisms, primary heat exchangers, primary pumps, spoliation target assembly and fuel assemblies, etc. The purpose of this paper is to investigate the possibility of an application of a partial seismic isolation to the safety critical components only, here, the reactor assembly. This paper presents the preliminary analysis results of the isolated reactor assembly and compares these with those of seismic isolated ADS reactor building. The analysis results show the reduction of the seismic acceleration response but the increase of the relative displacement for the reactor assembly. Some safety issues, especially, coolant＇s incapable covering the reactor core make difficult to apply for the partial seismic isolation of the ADS reactor assembly due to large relative displacement occurring the partial isolation system. Further study on the partial seismic isolation application of the critical safety components are also discussed.展开更多
We statistically validate the 2011-2022 earthquake prediction records of Ada, the sixth finalist of the 2nd China AETA in 2021, who made 147 earthquake predictions (including 60% of magnitude 5.5 earthquakes) with a p...We statistically validate the 2011-2022 earthquake prediction records of Ada, the sixth finalist of the 2nd China AETA in 2021, who made 147 earthquake predictions (including 60% of magnitude 5.5 earthquakes) with a prediction accuracy higher than 70% and a confidence level of 95% over a 12-year period. Since the reliable earthquake precursor signals described by Ada and the characteristics of Alfvén waves match quite well, this paper proposes a hypothesis on how earthquakes are triggered based on the Alfvén (Q G) torsional wave model of Gillette et al. When the plume of the upper mantle column intrudes into the magma and lithosphere of the soft flow layer during the exchange of hot and cold molten material masses deep inside the Earth’s interior during ascent and descent, it is possible to form body and surface plasma sheets under certain conditions to form Alfven nonlinear isolated waves, and Alfven waves often perturb the geomagnetic field, releasing huge heat and kinetic energy thus triggering earthquakes. To explain the complex phenomenon of how Ada senses Alvfen waves and how to locate epicenters, we venture to speculate that special magnetosensory cells in a few human bodies can sense earthquake precursors and attempt to hypothesize an algorithm that analyzes how the human biological nervous system encodes and decodes earthquake precursors and explains how human magnetosensory cells can solve complex problems such as predicting earthquake magnitude and locating epicenters.展开更多
基金financed by the project supported by the National Natural Science Foundation of China(22078266,21908180,22178289,22278338)the Key Research and Development Program of Shaanxi(2020ZDLGY11-02,2021GY-136)the Special Fund for High-level Scholars of China(XJ21B10)。
文摘The low temperature coal tar(CT)is taken as the raw material,and the extraction and column chromatography are used for detailed and accurate characterization in this paper.The n-heptane soluble fraction(CT-HS)and insoluble fraction(CT-HI)were obtained by n-heptane Soxhlet extraction.The extraction rate of CT-HS reached 92.79%(mass),which indicated that there are few heavy compounds in it.Further,different solvents(methylbenzene,benzene,ethyl acetate,methylbenzene-ethanol)were used to elute CT-HS by chromatographic column to obtain five fractions(saturates,aromatics,heteroatoms,phenolics and resins,named CT-SA,CT-AR,CT-HE,CT-PH,CT-RE,respectively).The yields of CTSA,CT-AR,CT-HE,CT-PH,CT-RE are 42.12%,10.43%,2.19%,9.50%and 6.63%(mass),respectively.Gas chromatography-mass spectrometry analysis of eluting components show that alkanes are the main components in CT,followed by polycyclic aromatics,and the corresponding fractions are CT-SA and CT-AR,respectively.The relative content of aliphatics in CT-SA is 76.93%,and the relative content of aromatics in CT-AR is 75.05%.This separation technology effectively separates and enriches different components in CT,and the activation energy required for the pyrolysis process of a single eluting fraction is lower than that of CT,which is expected to provide an important reference for the separation,analysis and conversion of complex oil products such as coal-oil co-processing products,coal tar and other complex heavy carbon oil products.
文摘This paper focuses on the investigation of a hybrid seismic isolation system with passive variable friction dampers for protection of structures against near fault earthquakes. The seismic isolation can be implemented by replacing the conventional columns fixed to the foundations by seismic isolating ones. These columns allow horizontal displacement between the superstructure and the foundations and decouple the building from the damaging earthquake motion. As a result, the forces in the structural elements decrease and damage that may be caused to the building by the earthquake significantly decreases. However, this positive effect is achieved on account of displacements occurring in the isolating columns. These displacements become very large when the structure is subjected to a strong earthquake. In this case, impact may occur between the parts of the isolating column yielding their damage or collapse. In order to limit the displacements in the isolating columns, it is proposed to add variable friction dampers. A method for selecting the dampers＇ properties is proposed. It is carried out using an artificial ground motion record and optimal active control algorithm. Numerical simulation of a sevenstory structure shows that the proposed method allows efficient reduction in structural response and limits the displacements at the seismic isolating columns.
基金funding and the PhD Scholarship for Fu Zeyu from the New Zealand Foundation for Arable Researchfunding for Song Jiancheng from the National Natural Science Foundation of China (31371616)
文摘Isolation of high quality DNA from multiple samples can be both time-consuming and expensive. We have developed a combined protocol to reduce the time component of the hexadecyltrimethylammonium bromide （CTAB） extraction method and reduced costs by regenerating the silica columns used to purify genomic DNA. We present data that shows, by in- creasing the temperature used during the CTAB method, the time required to extract crude genomic DNA can be reduced. We show that silica columns can be regenerated using HCI and still maintain their DNA-binding capacity. Furthermore, we show both spectrophotometrically, and by restriction enzyme cutting, that the quality of the eluted DNA is high. Critically, using both genomic DNA from pea and perennial ryegrass we demonstrate, using species-specific PCR primers, that there is no carry-over of DNA from repeated use of a single column. The main advantages of the method are high yield, high quality, cost effectiveness and time-saving. This method could satisfy demand when large numbers of plant genomic DNA samples are required, for example from targeting induced local lesions in genomes （TILLING） populations.
基金part of a collaborative project between the Steel Construction Institute, the University of Stuttgart, the University of Luxembourg, Arcelor Mittal S.A., and the University of Bradford funded by the European Community’s Research Fund for Coal and Steel (RFSR-CT-2012-00030)
文摘A full-scale composite floor plate was tested to investigate the flexural behavior and in-plane effects of the floor slab in a grillage of composite beams that reduces the tendency for longitudinal splitting of the concrete slab along the line of the primary beams. This is important in cases where the steel decking is discontinuous when it is orientated parallel to the beams. In this case, it is important to demonstrate that the amount of transverse reinforcement required to transfer local forces from the shear connectors can be reduced relative to the requirements of Eurocode 4. The mechanism under study involved in-plane compression forces being developed in the slab due to the restraining action of the floor plate, which was held in position by the peripheral composite beams;while the secondary beams acted as transverse ties to resist the forces in the floor plate that would otherwise lead to splitting of the slab along the line of the primary beams. The tendency for cracking along the center line of the primary beam and at the peripheral beams was closely monitored. This is the first large floor plate test that has been carried out under laboratory conditions since the Cardington tests in the early 1990s, although those tests were not carried out to failure. This floor plate test was designed so that the longitudinal force transferred by the primary beams was relatively high (i.e., it was designed for full shear connection), but the transverse reinforcement was taken as the minimum of 0.2% of the concrete area. The test confirmed that the primary beams reached their plastic bending resistance despite the discontinuous decking and transverse reinforcement at the minimum percentage given in Eurocode 4. Based on this test, a reduction factor due to shear connectors at edge beams without U-bars is proposed.
文摘In the SILER （Seismic-Initiated events risk mitigation in LEad-cooled Reactors） Project, it is interesting to apply seismic isolation technology for the reactor assembly of the fixed base reactor building for ADS （Acceleration Driven System） heavy liquid reactor MYRRHA （Multipurpose Hybrid Research Reactor for High-Tech Application） which contains the most critical safety related components, such as reactor vessel, safe shutdown and control rod mechanisms, primary heat exchangers, primary pumps, spoliation target assembly and fuel assemblies, etc. The purpose of this paper is to investigate the possibility of an application of a partial seismic isolation to the safety critical components only, here, the reactor assembly. This paper presents the preliminary analysis results of the isolated reactor assembly and compares these with those of seismic isolated ADS reactor building. The analysis results show the reduction of the seismic acceleration response but the increase of the relative displacement for the reactor assembly. Some safety issues, especially, coolant＇s incapable covering the reactor core make difficult to apply for the partial seismic isolation of the ADS reactor assembly due to large relative displacement occurring the partial isolation system. Further study on the partial seismic isolation application of the critical safety components are also discussed.
文摘We statistically validate the 2011-2022 earthquake prediction records of Ada, the sixth finalist of the 2nd China AETA in 2021, who made 147 earthquake predictions (including 60% of magnitude 5.5 earthquakes) with a prediction accuracy higher than 70% and a confidence level of 95% over a 12-year period. Since the reliable earthquake precursor signals described by Ada and the characteristics of Alfvén waves match quite well, this paper proposes a hypothesis on how earthquakes are triggered based on the Alfvén (Q G) torsional wave model of Gillette et al. When the plume of the upper mantle column intrudes into the magma and lithosphere of the soft flow layer during the exchange of hot and cold molten material masses deep inside the Earth’s interior during ascent and descent, it is possible to form body and surface plasma sheets under certain conditions to form Alfven nonlinear isolated waves, and Alfven waves often perturb the geomagnetic field, releasing huge heat and kinetic energy thus triggering earthquakes. To explain the complex phenomenon of how Ada senses Alvfen waves and how to locate epicenters, we venture to speculate that special magnetosensory cells in a few human bodies can sense earthquake precursors and attempt to hypothesize an algorithm that analyzes how the human biological nervous system encodes and decodes earthquake precursors and explains how human magnetosensory cells can solve complex problems such as predicting earthquake magnitude and locating epicenters.
