A calculation model of stress field in laser additive manufacturing of walnut shell composite powder(walnut shell/Co-PES powder)was established.The DFLUX subroutine was used to implement the moveable application of a ...A calculation model of stress field in laser additive manufacturing of walnut shell composite powder(walnut shell/Co-PES powder)was established.The DFLUX subroutine was used to implement the moveable application of a double ellipsoid heat source by considering the mechanical properties varying with temperature.The stress field was simulated by the sequential coupling method,and the experimental results were in good accordance with the simulation results.In addition,the distribution and variation of stress and strain field were obtained in the process of laser additive manufacturing of walnut shell composite powder.The displacement of laser additive manufacturing walnut shell composite parts gradually decreased with increasing preheating temperature,decreasing laser power and increasing scanning speed.During the cooling process,the displacement of laser additive manufacturing of walnut shell composite parts gradually increased with the increasing preheating temperature,decreasing scanning speed and increasing laser power.展开更多
This paper reports on the ablation process of a pure Ti solid target immersed in a C-enriched acetone solution, leading to the production of titanium carbide (TiC) and Ti-C core-shell nanostructures. The used route of...This paper reports on the ablation process of a pure Ti solid target immersed in a C-enriched acetone solution, leading to the production of titanium carbide (TiC) and Ti-C core-shell nanostructures. The used route of synthesis is generally called pulsed laser ablation in liquid (PLAL). The presence of carbon structures in the solution contributed to the carbon content in the produced Ti-based nanomaterials. The atomic composition of the produced nanostructures was analyzed using SEM-EDS, while TEM micrographs revealed the formation of spherical TiC and core-shell nanostructures ranging from 40 to 100 nm. The identification of atomic planes by HRTEM confirmed a 10 nm diameter C-shell with a graphite structure surrounding the Ti-core. Raman spectroscopy allowed for the identification of D and G peaks for graphite and a Raman signal at 380 and 600 cm<sup>−1</sup>, assigned to TiC. The results contribute to the state-of-the-art production of TiC and Ti-C core-shell nanostructures using the PLAL route.展开更多
With finite-element software ANSYS 7.0 and simple thermal-mechanical coupling constitutive relations,the buckling failure of preloaded cylindrical shell irradiated by high power laser beam was studied by numerical si...With finite-element software ANSYS 7.0 and simple thermal-mechanical coupling constitutive relations,the buckling failure of preloaded cylindrical shell irradiated by high power laser beam was studied by numerical simulations. The buckling mode and buckling critical loading were analysed for different preloading conditions. The influence of laser intensity, beam irradiation time, preloading conditions and geometric parameters of cylindrical shell on the buckling mode were discussed. The numerical results show that: ① the buckling deformation of the cylindrical shell was concentrated in the area of laser spot and the radial buckling was the main buckling mode, ② a linear relationship between the buckling eigenvalue and the maximum temperature at the center of laser spot was approached, ③ the buckling failure of cylindrical shell was attributed to the coupling effect of the material softening and the radial deformation in the laser spot, and hence to raise the stiffness of the material would enhance the ability for anti-irradiation of structure substantially..展开更多
Germanium (Ge)-carbon (C) core-shell nanowires (NWs), 15 - 80 nm thick and <1 μm long, were grown using continuous-wave laser vaporization of Ge-graphite composite targets in high pressure (0.1 - 0.9 MPa) Ar gas. ...Germanium (Ge)-carbon (C) core-shell nanowires (NWs), 15 - 80 nm thick and <1 μm long, were grown using continuous-wave laser vaporization of Ge-graphite composite targets in high pressure (0.1 - 0.9 MPa) Ar gas. The NW core was crystalline Ge and the shell was amorphous C. The fraction of the NWs in deposits was changed significantly by the Ge content in the targets and had a maximum at the Ge content of 40 atomic %. With increasing Ar pressure, thicker NWs were grown. A strong correlation was evident between the two diameters of the NW and nanoparticle (NP) attached with the tip of the NW. The growth of the NWs can be explained by the formation of Ge-C liquid-like molten NPs having a specific range of size and composition and precipitation of Ge and C followed by phase separation.展开更多
Experimental work has been focused on the formation of alloyed Au-Cu nanoparticles under simultaneous laser exposure and mechanical stirring of mixed monometallic colloids, here referred to as dual procedure. As a fee...Experimental work has been focused on the formation of alloyed Au-Cu nanoparticles under simultaneous laser exposure and mechanical stirring of mixed monometallic colloids, here referred to as dual procedure. As a feed for the dual procedure, Au and Cu monometallic nanoparticle colloids have been using a laser ablation technique. To accomplish this, bulk targets were ablated with 1064 nm wavelength Nd: YAG laser in a pure acetone(99.99%) environment. Ultraviolet-visible optical absorption spectrometry, transmission electron microscopy, X-ray diffraction and X-ray fluorescence technique have been used to characterize the nanoparticles. It has been found that experimental conditions such as stirring and laser parameters strongly affect the synthesized particle properties, including the size, shape, composition and stability of the nanoparticles. Alloy nanoparticles containing 39% Au – 61% Cu have also been prepared in the same process, but in two forms of a homogeneous alloy and a core-shell structure.展开更多
基金Supported by the Scientific Research Start-Up Fund Project of Northeast Petroleum University(2019KQ67 and 2021KQ09)the Guiding Innovation Fund Project of Northeast Petroleum University(2021YDL-13)+1 种基金National Natural Science Foundation of China(52075090)Supported by the National Key R&D Program of China(2017YFD0601004).
文摘A calculation model of stress field in laser additive manufacturing of walnut shell composite powder(walnut shell/Co-PES powder)was established.The DFLUX subroutine was used to implement the moveable application of a double ellipsoid heat source by considering the mechanical properties varying with temperature.The stress field was simulated by the sequential coupling method,and the experimental results were in good accordance with the simulation results.In addition,the distribution and variation of stress and strain field were obtained in the process of laser additive manufacturing of walnut shell composite powder.The displacement of laser additive manufacturing walnut shell composite parts gradually decreased with increasing preheating temperature,decreasing laser power and increasing scanning speed.During the cooling process,the displacement of laser additive manufacturing of walnut shell composite parts gradually increased with the increasing preheating temperature,decreasing scanning speed and increasing laser power.
文摘This paper reports on the ablation process of a pure Ti solid target immersed in a C-enriched acetone solution, leading to the production of titanium carbide (TiC) and Ti-C core-shell nanostructures. The used route of synthesis is generally called pulsed laser ablation in liquid (PLAL). The presence of carbon structures in the solution contributed to the carbon content in the produced Ti-based nanomaterials. The atomic composition of the produced nanostructures was analyzed using SEM-EDS, while TEM micrographs revealed the formation of spherical TiC and core-shell nanostructures ranging from 40 to 100 nm. The identification of atomic planes by HRTEM confirmed a 10 nm diameter C-shell with a graphite structure surrounding the Ti-core. Raman spectroscopy allowed for the identification of D and G peaks for graphite and a Raman signal at 380 and 600 cm<sup>−1</sup>, assigned to TiC. The results contribute to the state-of-the-art production of TiC and Ti-C core-shell nanostructures using the PLAL route.
文摘With finite-element software ANSYS 7.0 and simple thermal-mechanical coupling constitutive relations,the buckling failure of preloaded cylindrical shell irradiated by high power laser beam was studied by numerical simulations. The buckling mode and buckling critical loading were analysed for different preloading conditions. The influence of laser intensity, beam irradiation time, preloading conditions and geometric parameters of cylindrical shell on the buckling mode were discussed. The numerical results show that: ① the buckling deformation of the cylindrical shell was concentrated in the area of laser spot and the radial buckling was the main buckling mode, ② a linear relationship between the buckling eigenvalue and the maximum temperature at the center of laser spot was approached, ③ the buckling failure of cylindrical shell was attributed to the coupling effect of the material softening and the radial deformation in the laser spot, and hence to raise the stiffness of the material would enhance the ability for anti-irradiation of structure substantially..
文摘Germanium (Ge)-carbon (C) core-shell nanowires (NWs), 15 - 80 nm thick and <1 μm long, were grown using continuous-wave laser vaporization of Ge-graphite composite targets in high pressure (0.1 - 0.9 MPa) Ar gas. The NW core was crystalline Ge and the shell was amorphous C. The fraction of the NWs in deposits was changed significantly by the Ge content in the targets and had a maximum at the Ge content of 40 atomic %. With increasing Ar pressure, thicker NWs were grown. A strong correlation was evident between the two diameters of the NW and nanoparticle (NP) attached with the tip of the NW. The growth of the NWs can be explained by the formation of Ge-C liquid-like molten NPs having a specific range of size and composition and precipitation of Ge and C followed by phase separation.
基金supported by the Materials and Energy Research Center (MERC),Nanotechnology and Advanced Materials Department in the framework of Project Number 728811
文摘Experimental work has been focused on the formation of alloyed Au-Cu nanoparticles under simultaneous laser exposure and mechanical stirring of mixed monometallic colloids, here referred to as dual procedure. As a feed for the dual procedure, Au and Cu monometallic nanoparticle colloids have been using a laser ablation technique. To accomplish this, bulk targets were ablated with 1064 nm wavelength Nd: YAG laser in a pure acetone(99.99%) environment. Ultraviolet-visible optical absorption spectrometry, transmission electron microscopy, X-ray diffraction and X-ray fluorescence technique have been used to characterize the nanoparticles. It has been found that experimental conditions such as stirring and laser parameters strongly affect the synthesized particle properties, including the size, shape, composition and stability of the nanoparticles. Alloy nanoparticles containing 39% Au – 61% Cu have also been prepared in the same process, but in two forms of a homogeneous alloy and a core-shell structure.
