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Ultrahigh strength and improved electrical conductivity in an aging strengthened copper alloy processed by combination of equal channel angular pressing and thermomechanical treatment
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作者 WANG Xu LI Zhou +1 位作者 MENG Xiang-peng XIAO Zhu 《Journal of Central South University》 SCIE EI CAS CSCD 2024年第6期1823-1837,共15页
In this paper,equal channel angular pressing and thermomechanical treatment was employed to improve the strength and electrical conductivity of an aging strengthened Cu-Ti-Cr-Mg alloy,and the microstructure and proper... In this paper,equal channel angular pressing and thermomechanical treatment was employed to improve the strength and electrical conductivity of an aging strengthened Cu-Ti-Cr-Mg alloy,and the microstructure and properties of the alloy were investigated in detail.The results showed that the samples deformed by the combination of cryogenic equal channel angular pressing(ECAP)and rolling had good comprehensive properties after aging at 400℃.The tensile strength of the peak-aged and over-aged samples was 1120 MPa and 940 MPa,with their corresponding electrical conductivity of 14.7%IACS and 22.1%IACS,respectively.ECAP and cryogenic rolling introduced high density dislocations,leading to the inhibition of the softening effects and refinement of the grains.After a long time aging at 400℃,the alloy exhibited ultra-high strength with obvious increasing electrical conductivity.The high strength was attributed to the synergistic effect of work hardening,grain refinement strengthening and precipitation strengthening.The precipitation of a large amount of Ti atoms from the matrix led to the high electrical conductivity of the over-aged sample. 展开更多
关键词 Cu-Ti alloy equal channel angular pressing ROLLING aging treatment high strength
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Effect of aging treatment on the precipitation transformation and age hardening of Mg-Gd-Y-Zn-Zr alloy 被引量:2
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作者 Mu Meng Honglei Zhang +2 位作者 Zhi Gao Genxing Lei Jianmin Yu 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2023年第12期4628-4643,共16页
In this study, the precipitation transformation and age hardening of solution-treated Mg-9Gd-4Y-2Zn-0.5Zr(wt.%) alloy were investigated at different aging treatment parameters. The precipitation sequences of the alloy... In this study, the precipitation transformation and age hardening of solution-treated Mg-9Gd-4Y-2Zn-0.5Zr(wt.%) alloy were investigated at different aging treatment parameters. The precipitation sequences of the alloy aged at 200℃, 250℃ and 300℃ are β’’(DO19) → β’(BCO) → β(FCC), β’’(DO19) → β’(BCO) → β_(1)(FCC) → β(FCC) and β(FCC), respectively. The streaks sequences of the alloy aged at 200℃, 250℃ and 300℃ are SF, SF → 14H-LPSO and SF → 14H-LPSO, respectively. For the alloy aged at 200℃ and 250℃, the increase in hardness with increasing aging time is contributed from the increase in precipitate volume fraction and the transformation from β’’ to β’ phase with basal → prismatic and spherical → spindle-like precipitate changes. The decrease in hardness after the peak-aging stage is attributed to the appearance of micro-sized β precipitates. Because of the smaller size of precipitates and the triangular arrangement of β’ precipitate, the hardness of the alloy aged at 200℃ is higher than that aged at 250℃. For the alloy aged at 300℃, the appearance of only micro-sized β precipitate and its coarsening with increasing aging time leads to the lowest hardness and an overall decrease in hardness with the aging time. 展开更多
关键词 Mg-Gd-Y-Zn-Zr alloy aging treatment Precipitation transformation age hardening
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Scaling and clogging treatment of aging tunnel drainage pipes in karst areas using eco-friendly acid agent 被引量:1
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作者 Zhipeng Xu Xuemei Wang +2 位作者 Chunfang Zhang Dejian Zeng Changwu Liu 《Journal of Rock Mechanics and Geotechnical Engineering》 SCIE CSCD 2023年第4期896-910,共15页
In karst areas,the drainage pipes of aging tunnels are prone to be clogged by precipitated carbonates,resulting in lining cracking and tunnel leaking.As a result,not only the driving safety will be deteriorated,but al... In karst areas,the drainage pipes of aging tunnels are prone to be clogged by precipitated carbonates,resulting in lining cracking and tunnel leaking.As a result,not only the driving safety will be deteriorated,but also the water pressure on the lining might also be elevated significantly.For the structural stability and service lifespan of old tunnels,it is of great importance to remove these precipitated carbonates in time.Traditional treatment methods are often destructive to some extent or not efficient enough.This study aims to experimentally develop an eco-friendly acid-based chemical cleaning method to remove carbonate precipitations efficiently.The proposed chemical cleaning agent is an aqueous solution with strong acidity,consisting of sulfamic acid,water,and additives.The factors affecting the cleaning efficiency include the acid solubility,temperature and flow rate of the cleaning agent,as well as additives.Elevating the solution temperature to 50C or a flow rate of no less than 0.2 m/s can improve cleaning efficiency.Although the salt effect cannot work,1 wt%of polymaleic acid as a surfactant could further promote the cleaning rate.The cleaning efficiency will increase with the flow rate in a power function.The relatively low flow rate that improves the cleaning rate considerably can avoid highpressure-induced mechanical damage to tunnel drainpipes.The waste could be easily treated to acceptable levels using commercial sewage treatment products and can also be recycled in agriculture.With the chemical cleaning,the water pressure at the arch springing of the lining will reduce with the increased radius of transverse drainpipes in a power function.The proposed acid-based cleaning method,which is highly efficient,non-or low-destructive to aging tunnels,sufficiently safe for humans,and friendly enough to the environment,will offer a promising alternative to remove the precipitated carbonates in tunnel drainpipes efficiently. 展开更多
关键词 CLOGGING SCALING Carbonate precipitation Acid treatment Water pressure on the lining aging tunnel KARST
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Six Amino Acids among Natural Moisturizing Factors Responsible for Skin Hydration: Improvement and Anti-Aging of Skin by Galactomyces Ferment Filtrate-PiteraTM Containing Skin Moisturizer
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作者 Kukizo Miyamoto Yoko Munakata +4 位作者 Keisuke Fujii Wang Summer Ley Yang Suda Sudarsana Masutaka Furue 《Journal of Cosmetics, Dermatological Sciences and Applications》 2024年第2期113-127,共15页
Background: Natural moisturizing factors (NMFs) are filaggrin-derived components in the cornified layer that are critical for maintaining healthy skin moisturization and barrier function. However, studies have reporte... Background: Natural moisturizing factors (NMFs) are filaggrin-derived components in the cornified layer that are critical for maintaining healthy skin moisturization and barrier function. However, studies have reported conflicting findings on the relationship between NMF levels and aging, while few studies have investigated this relationship clinically. To fill this research gap, we determined the levels of major NMF components such as free amino acids, pyrrolidone carboxylic acid, and urocanic acids, and individually verified their relationships with skin hydration, barrier function, age, and skin aging. Purpose: The objective of this study was to clinically investigate the relationship between NMF components levels and skin aging in facial skin. The main NMF components were obtained from facial skin and quantified. We then selected NMF components showing strong relationships to skin hydration, and analyzed the relationships of the levels of these selected NMF components with signs of skin aging, namely, texture, pores, wrinkles, and dullness (L-value). We also examined the efficacy of treatment with a skin care formula (SK-II Facial Treatment Essence, called SK-II FTE hereafter) including Galactomyces ferment filtrate (GFF, PiteraTM) on the selected NMF component levels associated with skin hydration and barrier function, and the signs of skin aging of texture, pores, wrinkles, and dullness (L-value). Method: We conducted two clinical trials in this research. In Study 1, we measured 23 NMF components using tape-stripped cornified layer to quantify them via an HPLC method in 196 Asian females aged 20 to 59 (mean S.D., 38.6 9.4). Facial visual aging parameters [texture, pores, wrinkles, and dullness (L-value)], as well as elasticity (R7), skin hydration, and TEWL, were quantified using facial skin imaging and skin physical property measurement devices. Study 2 was performed to evaluate whether the facial application of SK-II FTE affects the NMF levels and skin aging parameters in 63 Asian female volunteers aged 20 to 55 (38.4 9.03). During the course of Study 2, 0.6 mL of SK-II FTE was applied to the face twice daily in the morning and afternoon. Skin measurements were performed at the start of the day (baseline) and at week 8. Results: In Study 1, we examined the stratum corneum levels of 23 NMF components comparing to the skin hydration status in 196 female subjects. The subjects were divided into two groups using the median of each measured NMF component. Skin hydration values were compared between the two groups defined for each NMF component. The results showed that subjects with higher levels of six amino acids, alanine, arginine, asparagine, glutamine, glycine, and histidine, exhibited significantly higher skin hydration than those with lower amino acid levels. No significant differences in skin hydration values were found for the other 17 NMF components. We then analyzed whether the sum of these six amino acid NMF components (called 6-AA-NMFs, hereafter) is affected by aging. The 6-AA-NMF level peaked in the subjects aged 25-29, and then gradually and significantly decreased with age. Interestingly, the 6-AA-NMF level was significantly correlated with the skin hydration value, but not with TEWL. In addition, the 6-AA-NMF level demonstrated significant correlations with the signs of skin aging of texture, pores, wrinkles, and dullness (L-value). Then, in Study 2, we examined whether the daily application of SK-II FTE affects the 6-AA-NMF level and visual aging parameters in 63 females. SK-II FTE demonstrated significant increases of the levels of 6-AA-NMFs and each of its components associated with hydration and barrier function, and improvements of skin texture, pores, wrinkles, and dullness (L-value) during the 8 weeks of treatment of facial skin. Conclusion: These clinical studies with large numbers of subjects across a wide age range revealed that six amino acids as NMF components were highly correlated with facial skin hydration in the stratum corneum. The levels of these six NMF components were also found to decrease at ages after the 30 s and were significantly correlated with major signs of skin aging. Notably, these six NMF components (6-AA-NMFs) were increased by SK-II FTE treatment associated with improvements of skin hydration and signs of skin aging, namely, texture, pores, wrinkles, and dullness (L-value). These studies were limited by the lack of investigation of why some NMF components were not associated with skin hydration. More clinical trials examining various NMF components and their relationship with aging are anticipated. 展开更多
关键词 NMF Amino Acid Visual aging Parameter Hydration aging Texture Pore Wrinkle Dullness Galactomyces Ferment Filtrate PiteraTM SK-II Facial treatment Essence
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Effects of aging treatment processes on microstructures and mechanical properties of AZ63 casting magnesium alloy
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作者 Chun-yu Li Hao-bo Wei +3 位作者 Shi-hui Ruan Jie-yi Chen Zong-gang Wu Ming-bo Yang 《China Foundry》 SCIE CAS CSCD 2023年第4期307-314,共8页
The effects of three different aging treatment processes,namely single-stage,double-stage,and reverse double-stage aging treatment processes,on the microstructures and mechanical properties of the AZ63(Mg-6Al-3Zn-0.25... The effects of three different aging treatment processes,namely single-stage,double-stage,and reverse double-stage aging treatment processes,on the microstructures and mechanical properties of the AZ63(Mg-6Al-3Zn-0.25Mn)casting magnesium alloy were investigated and compared.The results indicate that the microstructures of all the aged alloys under the three treatment processes are mainly composed ofα-Mg,Mg17Al12),and Al4Mn phases,indicating that the double-stage and reverse double-stage aging treatments have no obvious effect on the type of alloy phases.However,as compared with the single-stage and double-stage processes,the reverse double-stage process has a great effect on the quantity of the Mg17Al12phases.After the reverse double-stage aging treatment,which results in a stronger drive for decomposition of the supersaturated solid solution,the number of Mg17Al12phases precipitated in the grains significantly increases.In addition,as compared with the single-stage aged alloy,the tensile properties at room temperature for both the double-stage and reverse double-stage aged alloys are significantly improved.Among them,the reverse double-stage aged alloy achieves the highest tensile strength,yield strength,and elongation of 295 MPa,167 MPa,and 8.6%,respectively. 展开更多
关键词 magnesium alloys Mg-Al based alloys AZ63 alloy heat treatment aging treatment
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Effect of solution treatment and aging on microstructural evolution and mechanical behavior of NiTi shape memory alloy 被引量:6
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作者 江树勇 赵亚楠 +2 位作者 张艳秋 胡励 梁玉龙 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2013年第12期3658-3667,共10页
As-received nickel-titanium (NiTi) shape memory alloy with a nominal composition of Ni50.9Ti49.1 (mole fraction,%) was subjected to solution treatment at 1123 K for 2 h and subsequent aging for 2 h at 573 K, 723 K... As-received nickel-titanium (NiTi) shape memory alloy with a nominal composition of Ni50.9Ti49.1 (mole fraction,%) was subjected to solution treatment at 1123 K for 2 h and subsequent aging for 2 h at 573 K, 723 K and 873 K, respectively. The influence of solution treatment and aging on microstructural evolution and mechanical behavior of NiTi alloy was systematically investigated by transmission electron microscopy (TEM), high resolution transmission electron microscopy (HRTEM), scanning electron microscopy (SEM) and compression test. Solution treatment contributes to eliminating the Ti2Ni phase in the as-received NiTi sample, in which the TiC phase is unable to be removed. Solution treatment leads to ordered domain of atomic arrangement in NiTi alloy. In all the aged NiTi samples, the Ni4Ti3 precipitates, the R phase and the B2 austenite coexist in the NiTi matrix at room temperature, while the martensitic twins can be observed in the NiTi samples aged at 873 K. In the NiTi samples aged at 573 and 723 K, the fine and dense Ni4Ti3 precipitates distribute uniformly in the NiTi matrix, and thus they are coherent with the B2 matrix. However, in the NiTi sample aged at 873 K, the Ni4Ti3 precipitates exhibit the very inhomogeneous size, and they are coherent, semi-coherent and incoherent with the B2 matrix. In the case of aging at 723 K, the NiTi sample exhibits the maximum yield strength, where the fine and homogeneous Ni4Ti3 precipitates act as the effective obstacles against the dislocation motion, which results in the maximum critical resolved shear stress for dislocation slip. 展开更多
关键词 NiTi alloy shape memory alloy microstructural evolution mechanical properties solution treatment aging
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Ag元素和时效时间对T6态Al-5Cu-0.8Mg-0.15Zr-0.2Sc合金拉伸性能的影响
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作者 王莹 陈立佳 +2 位作者 车欣 张浩宇 张思倩 《沈阳理工大学学报》 CAS 2024年第4期51-56,共6页
为了明确Ag元素的添加对Al-Cu-Mg系铝合金拉伸性能的影响,针对T6态(固溶+时效处理)的热挤压Al-5Cu-0.8Mg-0.15Zr-0.2Sc(-0.5Ag)合金进行了室温和高温拉伸实验。结果表明,添加0.5%Ag元素可显著提高T6态Al-5Cu-0.8Mg-0.15Zr-0.2Sc合金的... 为了明确Ag元素的添加对Al-Cu-Mg系铝合金拉伸性能的影响,针对T6态(固溶+时效处理)的热挤压Al-5Cu-0.8Mg-0.15Zr-0.2Sc(-0.5Ag)合金进行了室温和高温拉伸实验。结果表明,添加0.5%Ag元素可显著提高T6态Al-5Cu-0.8Mg-0.15Zr-0.2Sc合金的室温抗拉强度、屈服强度、峰时效态及该合金在150~300℃范围的抗拉强度和屈服强度,但会降低该合金的室温和高温塑性。断口形貌的扫描电子显微镜观察与分析结果表明,在室温及高温拉伸加载条件下,T6态Al-5Cu-0.8Mg-0.15Zr-0.2Sc(-0.5Ag)合金的拉伸断口上大部分存在韧窝和撕裂棱,表现出明显的韧性断裂特点。 展开更多
关键词 Al-Cu-Mg系合金 拉伸性能 T6处理 韧性断裂
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T6态热挤压Al-5Cu-0.8Mg-0.15Zr-0.2Sc-0.5Ag合金的低周疲劳行为
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作者 王莹 陈立佳 +2 位作者 周舸 张浩宇 张思倩 《沈阳工业大学学报》 CAS 北大核心 2024年第1期77-81,共5页
为了揭示经过T6处理的热挤压Al-5Cu-0.8Mg-0.15Zr-0.2Sc-0.5Ag合金在不同温度下的低周疲劳变形与断裂行为,对T6态热挤压合金进行了室温和200℃条件下的低周疲劳实验。结果表明:在室温和200℃下合金塑性应变幅与载荷反向周次之间服从Coff... 为了揭示经过T6处理的热挤压Al-5Cu-0.8Mg-0.15Zr-0.2Sc-0.5Ag合金在不同温度下的低周疲劳变形与断裂行为,对T6态热挤压合金进行了室温和200℃条件下的低周疲劳实验。结果表明:在室温和200℃下合金塑性应变幅与载荷反向周次之间服从Coffin-Manson公式,而弹性应变幅与载荷反向周次之间服从Basquin公式;合金在室温和200℃下低周疲劳变形时,在较低外加总应变幅下疲劳变形机制主要为平面滑移,而在较高外加总应变幅下疲劳变形机制主要为波状滑移;室温和200℃下合金的疲劳裂纹均萌生于疲劳试样表面并以穿晶方式扩展。 展开更多
关键词 AL-CU-MG-ag合金 T6处理 低周疲劳 循环硬化 循环稳定 疲劳寿命 变形机制 疲劳断裂
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Effect of solution treatment and artificial aging on microstructure and mechanical properties of Al-Cu alloy 被引量:14
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作者 Jae-Ho JANG Dae-Geun NAM +1 位作者 Yong-Ho PARK Ik-Min PARK 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2013年第3期631-635,共5页
In order to achieve good mechanical properties of Al-Cu alloys such as high strength and good toughness,precipitation hardening and artificial aging treatment were applied.As defined by the T6 heat treatment,the stand... In order to achieve good mechanical properties of Al-Cu alloys such as high strength and good toughness,precipitation hardening and artificial aging treatment were applied.As defined by the T6 heat treatment,the standard artificial aging treatment for Al-Cu alloy followed heat treatments of solution treatment at 510-530 ℃ for 2 h,quenching in water at 60 ℃ and then artificial aging at 160-190 ℃ for 2-8 h.The effects of solution treatment and artificial aging on the microstructure and mechanical properties of Al-Cu alloy were studied by optical microscopy(OM),scanning electron microscopy(SEM),energy dispersive X-ray spectroscopy(EDS),transmission electron microscopy(TEM) and tensile test.The results of solution treatment indicate that the mechanical properties of Al-Cu alloy increase and then decrease with the increase of solution temperature.This is because the residual phases dissolve gradually into the matrix,and the fraction of the precipitation and the size of the re-crystallized grain increased.Compared to the solution temperature,the solution holding time has less effect on the microstructure and the mechanical properties of Al-Cu alloy.The artificial aging treatments were conducted at 160-180 ℃ for 2-8 h.The results show that the ultimate tensile strength can be obtained at 180 ℃ for 8 h.Ultimate tensile strength increased with increasing time or temperature.Yield strength was found as the same as the ultimate tensile strength result. 展开更多
关键词 Al-Cu alloy solid solution treatment artificial aging MICROSTRUCTURE mechanical property
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Transformation behavior and shape memory effect of Ti_(50-x)Ni_(48)Fe_2Nb_x alloys by aging treatment 被引量:5
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作者 Xu, Qing Liu, Fushun 《Rare Metals》 SCIE EI CAS CSCD 2012年第4期311-317,共7页
The influence of aging treatment on transformation behavior and shape memory of the Ti 50_x Ni_(48) Fe_2 Nb_x(x=0,0.6,0.8,1.0,and 1.2) alloys was investigated using differential scanning calorimeter(DSC),mechanical dr... The influence of aging treatment on transformation behavior and shape memory of the Ti 50_x Ni_(48) Fe_2 Nb_x(x=0,0.6,0.8,1.0,and 1.2) alloys was investigated using differential scanning calorimeter(DSC),mechanical drawing machine,and microhardness tester in this paper.It is indicated that the aging treatment has a significant effect on the phase transformation temperatures(M_s,M_f,M_p,A_s,A_f,and A_p) and microhardness of the samples.The phase transformation temperatures are found to decrease initially with the increasing aging temperature from 300 to 500 ℃ and increase with further increase of the aging temperature.The aging treatment at intermediate temperature between 400 and 500 ℃ results in an improved shape memory effect.In addition,the highest microhardness value is also obtained. 展开更多
关键词 Ti-Ni-Fe-Nb shape memory alloys martensitic transformation aging treatment phase transformation temperature
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Effects of Aging Treatment on Intergranular Corrosion and Stress Corrosion Cracking Behavior of AA7003 被引量:6
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作者 ZHANG Xiaoyan SONG Renguo SUN Bin 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2018年第5期1198-1204,共7页
In order to study the effects of aging treatment on the intergranular corrosion(IGC) and stress corrosion cracking(SCC) of 7003 aluminum alloy(AA7003), the intergranular corrosion test, electrochemical test and ... In order to study the effects of aging treatment on the intergranular corrosion(IGC) and stress corrosion cracking(SCC) of 7003 aluminum alloy(AA7003), the intergranular corrosion test, electrochemical test and slow strain rate test(SSRT), combined with optical microscopy(OM) and scanning electron microscopy(SEM) as well as transmission electron microscopy(TEM) observations have been carried out. The IGC and electrochemical test results showed that the IGC resistance of AA7003 for peak aged(PA) temper is the lowest, with double peak aged(DPA) the moderate, and retrogression and re-aging(RRA) the highest among three tempers, which is attributed to the continuous feature of precipitation on grain boundary of PA temper and the interrupted feature of precipitation on grain boundary of DPA and RRA tempers, as well as the wide precipitation free zones(PFZ) of RRA temper. In addition, the SSRT results indicated that all three tempers AA7003 are susceptible to SCC in IGC solution, and the change tendency of SCC susceptibility(ISCC) of AA7003 for three tempers follows the order: ISCC(RRA) 展开更多
关键词 AA7003 aging treatment intergranular corrosion stress corrosion cracking
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Influence of process parameters and aging treatment on the microstructure and mechanical properties of Al Si8Mg3 alloy fabricated by selective laser melting 被引量:9
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作者 Yaoxiang Geng Hao Tang +6 位作者 Junhua Xu Yu Hou Yuxin Wang Zhen He Zhijie Zhang Hongbo Ju Lihua Yu 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2022年第9期1770-1779,共10页
Many studies have investigated the selective laser melting(SLM)of AlSi10Mg and AlSi7Mg alloys,but there are still lack of researches focused on Al-Si-Mg alloys specifically tailored for SLM.In this work,a novel high M... Many studies have investigated the selective laser melting(SLM)of AlSi10Mg and AlSi7Mg alloys,but there are still lack of researches focused on Al-Si-Mg alloys specifically tailored for SLM.In this work,a novel high Mg-content AlSi8Mg3 alloy was specifically designed for SLM.The results showed that this new alloy exhibited excellent SLM processability with a lowest porosity of 0.07%.Massive lattice distortion led to a high Vickers hardness in samples fabricated at a high laser power due to the precipitation of Mg_(2)Si nanoparticles from theα-Al matrix induced by high-intensity intrinsic heat treatment during SLM.The maximum microhardness and compressive yield strength of the alloy reached HV(211±4)and(526±12)MPa,respectively.After aging treatment at 150℃,the maximum microhardness and compressive yield strength of the samples were further improved to HV(221±4)and(577±5)MPa,respectively.These values are higher than those of most known aluminum alloys fabricated by SLM.This paper provides a new idea for optimizing the mechanical properties of Al-Si-Mg alloys fabricated using SLM. 展开更多
关键词 AlSi8Mg3 alloy selective laser melting process parameters MICROSTRUCTURE aging treatment mechanical properties
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Effects of solution treatment and aging process on microstructure refining of semi-solid slurry of wrought aluminum alloy 7A09 被引量:5
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作者 WU Xin HAN Fei WANG Wei-wei 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2009年第S02期331-336,共6页
A new method was exploited using solution treatment and aging process as a pretreatment in preparing semi-solid slurry with fine microstructure before isothermal treatment of wrought aluminum alloy 7A09.Parameters of ... A new method was exploited using solution treatment and aging process as a pretreatment in preparing semi-solid slurry with fine microstructure before isothermal treatment of wrought aluminum alloy 7A09.Parameters of pretreatment were optimized by orthogonal experiment design and proper precursor was prepared.The evolution of microstructure of semi-solid slurry during isothermal treatment was analyzed and the mechanism of microstructure refining was discussed.The result of orthogonal experiment design shows that the optimum parameters are 462 ℃for solution temperature,40min for solution time,132 ℃for aging temperature and 14 h for aging time.Microstructure of isothermal treatment is fine,homogenous,with globular solid grains and a solid fraction between 50%and 70%,which is qualified for later semi-solid forming process.Mechanism of microstructure evolution includes the agglomeration ofα-phase and Ostwald ripening.Precipitations prepared by solution and aging treatment prevent the grains from coarsening and promote the grain ripening to globular shape. 展开更多
关键词 wrought aluminum alloy semi-solid slurry microstructure refining solution treatment aging
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A New Aging Treatment Way for Near α High Temperature Titanium Alloys 被引量:2
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作者 Jun Zhang Na Peng +1 位作者 Qingjiang Wang Xi'nan Wang 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2009年第4期454-458,共5页
Two near α titanium alloys, Ti-5.6Al-4.8Sn-2.0Zr-1Mo-0.35Si (1#) and Ti-6.0AI-4.8Sn-2.0Zr-1Mo-0.35Si (2#), were solution-treated in the upper α+β phase fields, and the duplex mixture microstructures consisting... Two near α titanium alloys, Ti-5.6Al-4.8Sn-2.0Zr-1Mo-0.35Si (1#) and Ti-6.0AI-4.8Sn-2.0Zr-1Mo-0.35Si (2#), were solution-treated in the upper α+β phase fields, and the duplex mixture microstructures consisting of the less volume fraction primary α phase (αp) and the transformed β phase (βt) were obtained. The aging treatments were carried out at 700℃ for 1# alloy and 760℃ for 2# alloy under varied terms, respectively. It guaranteed α2 ordered phase to precipitate only in αp but not in βt for the two alloys. The slower precipitation and growth of the α2 ordered phase and silicide was observed in 1# alloy in comparison with 2# alloy. The mechanical properties including tensile strength and ductility, the creep and lasting properties at 600℃ were investigated. Prolonging aging time did not predominantly change the tensile strength and ductility for the two alloys. The 600℃/100 h thermal exposure caused a notable decrease of tensile ductility in 2# alloy though no distinct decrease could be observed in 1# alloy after the thermal exposure. The lasting property of i# alloy was increased with prolonging aging time and finally was equal to or even better than that of 2# alloy. Nevertheless, no evident increase emerged in 2# alloy with prolonging aging time. Similarly, the creep property of 1# alloy monotonously increased with increasing aging time and finally was equal to or even better than that of 2# alloy. No evident increase could be observed for 2# alloy. It can be deduced that the overgrowth of α2 ordered phase and silicide is unable to enhance hot strength properties but cause an unacceptable damage to tensile ductility. The optimum equilibrium of the comprehensive properties depending on the proper control of α2 ordered phase and silicide can be achieved by properly selecting aging temperature and time. 展开更多
关键词 Titanium alloy Mechanical property aging treatment
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Effect of aging treatment on evolution of S'phase in rapid cold punched Al−Cu−Mg alloy 被引量:6
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作者 Ze-yi HU Cai-he FAN +3 位作者 Tong SHEN Ling OU Nan-shan DAI Lu WANG 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2021年第7期1930-1938,共9页
High-resolution transmission electron microscopy(TEM),X-ray diffractometer(XRD),and hardness test were used to study the evolution of long plate-shaped S'phase in the spray-formed fine-grained Al−Cu−Mg alloy durin... High-resolution transmission electron microscopy(TEM),X-ray diffractometer(XRD),and hardness test were used to study the evolution of long plate-shaped S'phase in the spray-formed fine-grained Al−Cu−Mg alloy during aging after rapid cold punching deformation.Results show that the long plate-shaped S'phase in the extruded Al−Cu−Mg alloy undergoes evident distortion,brittle failure,separation and redissolution,during rapid cold punching deformation,leading to the transformation of long plate-shaped S'phase into short rod or even redissolution and disappearance,causing the matrix to become a supersaturated solid solution.After the aging treatment,the reprecipitation of the phases occurs,and these aging phases are mainly long plate-shaped and granular.The incompletely dissolved S'phase acts as nucleation core,promoting uphill diffusion of the surrounding solute atoms.The S'phase gradually grows with increasing the aging time.The completely dissolved S'phase forms the incoherent equilibrium phase with the matrix to reduce its free energy.After rapid cold punching,the aging response of the deformed Al−Cu−Mg alloy is accelerated,and the hardness of the alloy is substantially increased. 展开更多
关键词 aging treatment Al−Cu−Mg alloy rapid cold punching dissolution REPRECIPITATION
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Effect of solution plus aging heat treatment on microstructural evolution and mechanical properties of near-β titanium alloy 被引量:22
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作者 Chuan WU Mei ZHAN 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2019年第5期997-1006,共10页
The microstructural evolution, mechanical properties and fracture mechanism of a Ti.5Al.5Mo.5V.3Cr.1Zr (Ti-55531) alloy after solution (760.820℃) plus aging (580.640℃) treatments were investigated. The results show ... The microstructural evolution, mechanical properties and fracture mechanism of a Ti.5Al.5Mo.5V.3Cr.1Zr (Ti-55531) alloy after solution (760.820℃) plus aging (580.640℃) treatments were investigated. The results show that the volume fraction of the primary α(αp) phase decreases with the increase of solution temperature, and the length of the secondary α phase (αs) decreases while its width increases with the increase of aging temperature. Yield and tensile strengths decrease with the increase of solution temperature, while increase with the increase of aging temperature. A good balance of tensile strength and ductility of the alloy is obtained under solution of 800℃ for 2 h plus aging of 640℃ for 8 h, in which the tensile strength is 1434 MPa and the elongation is 7.7%. The coarsening αs phase makes crack propagation paths deflected and tortuous, which increases the crack propagation resistance and improves the ductility and fracture toughness. 展开更多
关键词 Ti.5Al.5Mo.5V.3Cr.1Zr titanium alloy hot treatment SOLUTION aging microstructural evolution mechanical properties fracture mechanism
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Influence of aging treatment on corrosion behavior and mechanism of Mg–Y alloys 被引量:2
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作者 徐宏 张新 +2 位作者 蒋三生 任霁萍 高翔宇 《Journal of Central South University》 SCIE EI CAS CSCD 2018年第5期987-1002,共16页
This paper studied the influence of aging treatment on the corrosion behavior and mechanism of Mg-Y alloys with different Y content through corrosion mass loss test, electrochemical test and corrosion morphologies obs... This paper studied the influence of aging treatment on the corrosion behavior and mechanism of Mg-Y alloys with different Y content through corrosion mass loss test, electrochemical test and corrosion morphologies observation. Results show that the peak-aging times of Mg-(0.25, 2.5, 5, 8 and 15) Y alloys at 250 ℃ were 4, 6, 10, 12 and 16 h. The aging treatment reduced the corrosion resistance of Mg-Y alloys, and the corrosion resistance of Mg-Y alloys became worse with increasing of the aging time. The change magnitude of the open circuit potentials for Mg-(0.25, 2.5)Y alloys was greater than that of Mg-(5, 8 and 15)-Y alloys. The polarization curves of Mg (0.25, 2.5, 5, 8 and 15) Y alloys had the similar shape after aging treatment, and the slopes of the anodic branch were greater than those of the cathodic branches. After aging treatment, the corrosion modes of Mg-0.25Y and Mg-(2.5, 5, 8 and 15) Y alloys were uniform corrosion and pitting corrosion with small local deep corrosion. 展开更多
关键词 Mg-Y alloy aging treatment electrochemical corrosion resistance corrosion morphology
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Effect of cryogenic and aging treatments on low-energy impact behaviour of Ti-6Al-4V alloy 被引量:2
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作者 Y. PEKBEY K. ASLANTAS Y. PEKBEY 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2017年第3期514-526,共13页
The objective of this study is to examine the effects of cryogenic and aging treatments on the impact strength andmechanical properties of Ti?6Al?4V alloy.To accomplish that objective,cryogenic treatment(CT),aging tre... The objective of this study is to examine the effects of cryogenic and aging treatments on the impact strength andmechanical properties of Ti?6Al?4V alloy.To accomplish that objective,cryogenic treatment(CT),aging treatment(AT)andcryogenic treatment followed by aging treatment(CAT)were conducted on Ti?6Al?4V alloy.Impact tests were performed onheat-treated and untreated samples using different impactor nose geometries(hemispherical,60°and90°conical)to determine theeffect of impactor nose geometry on the damage characteristic.The findings showed that energy absorption increased and areas ofdamage decreased as a result of heat treatment in all treated samples.The highest energy absorption was observed in the CATsamples,due to the increase in energy absorption,the smallest damaged area occurred in the CAT sample,and the largestdeformation was seen in the untreated samples.Additionally,it was seen that the damaged area and deflection were stronglydependent on impactor nose geometry.The maximum deflection and narrowest deformation area were seen with60o conical nosegeometry.The deformation area increased with increasing impactor nose angle. 展开更多
关键词 Ti.6Al.4V alloy cryogenic treatment aging treatment low-energy impact test impact damage impactor nose geometry
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Effect of Aging Treatment on Microstructural and Mechanical Characteristics of PEO Coatings on Mg-Al Alloy 被引量:1
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作者 Y.L.Kim 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2008年第1期37-40,共4页
Cast Mg-6 wt pct Al alloy solution-treated at 683 K for 16 h and aged at 498 K was coated by plasma electrolytic oxidation (PEO) method.The Mg-6 wt pct Al alloy aged for 16 h exhibited the highest microhardness and ... Cast Mg-6 wt pct Al alloy solution-treated at 683 K for 16 h and aged at 498 K was coated by plasma electrolytic oxidation (PEO) method.The Mg-6 wt pct Al alloy aged for 16 h exhibited the highest microhardness and wear resistance.After PEO coating,however,the microhardness and wear resistance of coatings on Mg- 6 wt pct Al alloy showed a tendency to decrease with increasing aging time,which was in aggrement with the change of thickness with aging time.In addition,the coatings on solution-treated Mg-6 wt pct Al alloy had better microhardness and wear resistance than those on aged Mg-6 wt pct Al alloys.Consequently,it can be understood that the aging treatment has a deleterious influence on the mechanical properties of coatings on Mg-6 wt pct Al alloy. 展开更多
关键词 Cast Mg-6 wt pct Al aging treatment Plasma electrolytic oxidation Thickness MICROHARDNESS Wear resistance
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Optimal Selection and Control for Precipitation of α_2 Phase in Near α High Temperature Ti Alloys during Aging Treatment 被引量:1
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作者 JunZHANG QingjiangWANG +2 位作者 YuyinLIU LiLI GongLI 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2004年第5期574-576,共3页
The characteristic of the precipitation and growth of α2 ordered phase during aging treatment in near α Ti alloys have been investigated in terms of the influences of aging temperature, aging time and aging manner. ... The characteristic of the precipitation and growth of α2 ordered phase during aging treatment in near α Ti alloys have been investigated in terms of the influences of aging temperature, aging time and aging manner. The results exhibit that aging temperatures influence the distribution of α2 phase precipitated and cause the changes in growth speed of α2 phase. For various aging temperatures, the time to finish precipitation of α2 phase is different. The facts that various distribution characteristics and growth speed of α2 ordered phase are caused by changed aging condition imply optimal selection and control for precipitation of α2 ordered phase reachable. Some discussions on adoptable aging steps are presented. 展开更多
关键词 α2 ordered phase Near-α titanium alloy aging treatment
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