In today’s manufacturing industries,hard competition between rival firms makes it compulsory for researchers to design lighter and cheaper machine components due to the megatrends of cost-effectiveness and anti-pollu...In today’s manufacturing industries,hard competition between rival firms makes it compulsory for researchers to design lighter and cheaper machine components due to the megatrends of cost-effectiveness and anti-pollution.At this point,aluminum syntactic foams(ASFs)are new-generation engineering composites and come into the upfront as a problem-solver.Owing to their features like low density,sufficient elongation,and perfect energy absorption ability,these advanced foams have been considerably seductive for many industrial sectors nowadays.In this study,an industrial-oriented automatic die casting technology was used for the first time to manufacture the combination of AA7075/porous expanded clay(PEC).Micro evaluations(optical and FESEM)reveal that there is a homogenous particle distribution in the foam samples,and inspections are compatible with the other ASF studies.Additionally,T6 aging heat treatment was operated on one half of the produced foams to explore the probable impact of aging on the compressive responses.Attained results show that PEC particles can be an alternative to expensive hollow spheres used in the previous works.Besides,a favorable relationship is ascertained between the aging treatment and mechanical properties such as compression strength and plateau strength.展开更多
The microstructures of ZK60 alloy under conventional direct as-casting (DC),twin roll casting (TRC) and twin roll casting followed by hot compression (TRC-HC) were analyzed by optical morphology (OM),electron backscat...The microstructures of ZK60 alloy under conventional direct as-casting (DC),twin roll casting (TRC) and twin roll casting followed by hot compression (TRC-HC) were analyzed by optical morphology (OM),electron backscatter diffraction (EBSD) and X-ray diffraction (XRD).The deformation condition of hot compression is 350 ℃,0.1 s?1.The microstructural evolution under TRC-HC deformation followed by annealing at different temperatures and time was discussed.The results show that TRC provides more modified microstructure compared with DC.Twins are found in TRC processing;dynamic recrystallization (DRX),shear bands and twins are found in TRC-HC.A short annealing time has little effect on hardness,while during a long time annealing,it is found that low annealing temperatures increase the micro-hardness and high temperature decreases it.展开更多
A dynamic material model of Mg-4.51Al-1.19Zn-0.5Mn-0.5Ca(AZ41,mass fraction,%)magnesium alloy was put forward.The results show that the dynamic material model can characterize the deformation behavior and microstructu...A dynamic material model of Mg-4.51Al-1.19Zn-0.5Mn-0.5Ca(AZ41,mass fraction,%)magnesium alloy was put forward.The results show that the dynamic material model can characterize the deformation behavior and microstructure evolution and describe the relations among flow stress,strain,strain rates and deformation temperatures.Statistical analysis shows the validity of the proposed model.The model predicts that lower deformation temperature and higher strain rate cause the sharp strain hardening. Meanwhile,the flow stress curve turns into a steady state at high temperature and lower strain rate.The moderate temperature of 350 ℃and strain rate of 0.01 s-1 are appropriate to this alloy.展开更多
The relationship of true stress and true strain of AZ41M magnesium alloy under twin-roll-cast (TRC) and hot compression was analyzed us- ing a Gleeble 1500 machine. Microstructural evolutions of the TRC magnesium al...The relationship of true stress and true strain of AZ41M magnesium alloy under twin-roll-cast (TRC) and hot compression was analyzed us- ing a Gleeble 1500 machine. Microstructural evolutions of the TRC magnesium alloy under different deformation conditions (strain, sWain rate and deformation temperature) were examined using optical microscopy and discussed. The relationship of true stress and true sWain pre- dicted that lower deformation temperature and higher sWain rate caused sharp strain hardening. Meanwhile, the flow stress curve turned into a steady state at high temperature and lower strain rate. The intermediate temperature and strain rate (623 K and 0.01 s^-1) is appropriate.展开更多
Fine, equiaxed, non dendritic structure needed by semi solid processing was obtained by liquidus cast, i.e. 7075 wrought aluminum alloy cast from liquidus temperature. The microstructures after heat treatment at diffe...Fine, equiaxed, non dendritic structure needed by semi solid processing was obtained by liquidus cast, i.e. 7075 wrought aluminum alloy cast from liquidus temperature. The microstructures after heat treatment at different temperatures and time in the semi solid range were observed, and the compression deformation behavior at different temperatures (490~600 ℃) and strain rates (5×10 -3 ~5s -1 ) was investigated by means of Gleeble 1500 thermal mechanical simulator. The results show that the deformation resistance of the non dendritic structure attained by liquidus cast in semi solid is remarkably lower than that of conventional dendritic structure. The formability of non dendritic structure is better than that of dendritic structure.展开更多
The flow behavior of a cast Ti-25Al-10Nb-3V-1Mo alloy based onTi3Al, with and without hydrogen content, was investigated under isothermal compression test at strain rates of 0.1s-1 to 0.001s -1 in the temperature rang...The flow behavior of a cast Ti-25Al-10Nb-3V-1Mo alloy based onTi3Al, with and without hydrogen content, was investigated under isothermal compression test at strain rates of 0.1s-1 to 0.001s -1 in the temperature range of 900℃ to1000 ℃. The hot compression peak stress (or the maximum flow stress) of the alloy withand without hydrogen decreases with the increasing temperature and the decreasingstrain rate. Hydrogenation makes the hot compression peak stress decrease by 37%~53%, which corresponds to lowering the deformation temperature by about 50℃.Strain rate does not change the favorable effect of hydrogenation on hot compressionflow behavior at all three deformation temperatures. The microstructure of the alloywith 0.2% H (mass %) deformed at a fixed temperature exhibits the same feature asthat of the alloys without hydrogenation deformed at higher temperatures for bothstrain rates. Hydrogenation has the same effect on microstructure as strain rate andtemperature.展开更多
The NiAl-28Cr-5.85Mo-0.15Hf alloy was prepared by high-pressure die casting (HPDC) and subsequent hot isostatic pressing(HIP), and tested for compressible strength and fracture behavior at 300-1 373 K. The results sho...The NiAl-28Cr-5.85Mo-0.15Hf alloy was prepared by high-pressure die casting (HPDC) and subsequent hot isostatic pressing(HIP), and tested for compressible strength and fracture behavior at 300-1 373 K. The results show that the elevated temperature 0.2% compressible yield strength as well as the room-temperature compressible fracture strain of as-HIP alloy are larger than those of the same alloy prepared by directional solidification (DS). It suggests that the fine structures with a homogeneous distribution of fine Cr (Mo) and Hf-rich phase created by high-pressure die casting lead to these improvements.展开更多
Sea urchin spines were chosen as a model system for biomimetic ceramics obtained using starch-blended slip casting. Porous alumina ceramics with cap-shaped layers with different alternating porosities were found to ha...Sea urchin spines were chosen as a model system for biomimetic ceramics obtained using starch-blended slip casting. Porous alumina ceramics with cap-shaped layers with different alternating porosities were found to have superior fracture behavior under bulk compression compared to ceramics with uniform porosity.They fail in a cascading manner,absorbing high amounts of energy during extended compression paths.The porosity variation in an otherwise single phase material mimicks the architectural microstructure design of sea urchin spines of Heterocentrotus mammillatus,which are promising model materials for impact protection.展开更多
As a new type of lightweight structure,metallic lattice structure has higher stiffness and strength to weight ratio.To freely obtain 316L lattice structures with designed cell structure and adjustable porosity,additiv...As a new type of lightweight structure,metallic lattice structure has higher stiffness and strength to weight ratio.To freely obtain 316L lattice structures with designed cell structure and adjustable porosity,additive manufacturing combined with investment casting was conducted to fabricate the 316L lattice structures with Kelvin cell.The compression simulation of 316L lattice structures with different porosities was carried out by using the finite element method.The numerical simulation results were verified by compression experiment,and the simulated results were consistent with the compression tests.The compressive mechanical properties of 316L lattice structures are directly related to porosity and independent of strut diameters.The 316L lattice structures with Kelvin cell have a smooth stress-strain curve and obvious plastic platform,and the hump stress-strain curves are avoided.展开更多
The effect of Zr on the behavior of compressive creep in as cast ZA27 alloy was investigated in the temperature range of 20160 ℃ and under different compressive stresses in the range of 50137.5 MPa with special appar...The effect of Zr on the behavior of compressive creep in as cast ZA27 alloy was investigated in the temperature range of 20160 ℃ and under different compressive stresses in the range of 50137.5 MPa with special apparatus. The results show that the primary compressive creep strains and steady creep rates of ZA27 Zr alloy and ZA27 alloy increase with increasing temperature and stress. However, the primary compressive creep strain and steady creep rate of the ZA27 Zr alloy are lower than that of the ZA27 alloy below 100 ℃, but higher at 160 ℃. The compressive creep behaviors in both ZA27 Zr alloy and ZA27 alloy obey an empirical equation ln t=C-n ln σ+ Q/RT , and the exponent stress n is 3.63 for ZA27 Zr alloy and 3.46 for ZA27 alloy, respectively, the activation energy Q is 87.32 kJ/mol for ZA27 Zr alloy and 81.09 kJ/mol for ZA27 alloy. Different material structural constants are associated with different compressive creep behaviors in the alloy. The compressive creep rate in the alloy is controlled by the lattice diffusion of zinc and dislocation limb.展开更多
The aim of the present research is to provide a novel technique for preparing gradient Al 2 O 3-ZrO 2 ceramic foams.This technique used epispastic polystyrene spheres to array templates and centrifugal slip casting to...The aim of the present research is to provide a novel technique for preparing gradient Al 2 O 3-ZrO 2 ceramic foams.This technique used epispastic polystyrene spheres to array templates and centrifugal slip casting to obtain cell struts with gradient distribution of Al 2 O 3 and ZrO 2 particles and high packing density.Aqueous Al 2 O 3-20vol.% ZrO 2 slurries with 20vol.% solid contents were prepared and the dispersion and rheological characteristics of the slurries were investigated.The settling velocity and mass segregation of Al 2 O 3 and ZrO 2 particles at different centrifugal accelerations were calculated and studied.The drying behavior,macrostructure,microstructure,compressive property and resistance to thermal shock of the sintered products were also investigated.The results show that the difference of settling velocity of Al 2 O 3 and ZrO 2 particles increases and mass segregation becomes acute with an increase in centrifugal acceleration.The cell struts prepared at a centrifugal acceleration of 1,690 g have high sintered density(99.0% TD) and continuous gradient distribution of Al 2 O 3 and ZrO 2 particles.When sintered at 1,550 o C for 2 h,the cell size of gradient Al 2 O 3-ZrO 2 foam is approximately uniform,about 1.1 mm.With the porosity of gradient Al 2 O 3-ZrO 2 ceramic foams increasing from 75.3% to 83.0%,the compressive strength decreases from 4.4 to 2.4 MPa,and the ceramic foams can resist 8-11 repeated thermal shock from 1,100 o C to room temperature.展开更多
Phosphate-bonded investments have already been widely utilized in dental restoration and micro-casting of artistic products for its outstanding rapid setting and high strength. However, the rapid setting rate of inves...Phosphate-bonded investments have already been widely utilized in dental restoration and micro-casting of artistic products for its outstanding rapid setting and high strength. However, the rapid setting rate of investment slurry has up to now been a barrier to extend the use of such slurry in preparation of medium-sized ceramic moulds. This paper proposes a new process of rapid fabrication of magnesia-phosphate-bonded investment ceramic moulds for medium-sized superalloy castings utilizing bauxite and mullite as refractory aggregates. In order to determine the properties of magnesia-phosphate-bonded bauxite-mullite investments (MPBBMI), a series of experiments were conducted, including modifciation of the workable time of slurry by liquid(mL)/powder(g)(L/P) ratio and addition of boric acid as retard agent and sodium tri-polyphosphate (STP) as strengthening agent, and adjustment of bauxite (g)/mullite(g)(B/M) ratio for mechanical strength. Mechanical vibration was applied to improve initial setting time and fluidity when pouring investment slurry; then an intermediate size ceramic mould for superalloy castings was manufactured by means of this rapid preparing process with MPBBMI material. The results showed that the MPBBMI slurry exhibits proper initial setting time and excellent fluidity when the L/P ratio is 0.64 and the boric acid content is 0.88wt.%. The fired specimens made from the MPBBMI material demonstrated adequate compression strength to withstand impact force of molten metal when the B/M ratio is 0.89 and the STP content is 0.92wt.%. The experimental results confirmed the feasibility of the proposed rapid fabricating process for medium-sized ceramic moulds with MPBBMI material by appropriate measures.展开更多
In this study, boron fiber powder and graphite is reinforced to Al 2024 alloy to develop hybrid metal matrix composite by stir casting process. Hybrid MMCs developed with different weight fraction for 4%, 6%, 8% and 1...In this study, boron fiber powder and graphite is reinforced to Al 2024 alloy to develop hybrid metal matrix composite by stir casting process. Hybrid MMCs developed with different weight fraction for 4%, 6%, 8% and 10% of boron fiber and 2% of graphite. Stirring parameters are optimized to obtain solid casting. Reinforcements are poured into molten aluminium at 15 g/min and stirrer is rotated for 5 minutes at 250 rpm with two stages stirring. 1% of magnesium was added to improve the wettability of Al 2024. Cast samples are machined as per the standards to investigate the microstructure, physical and mechanical properties. Optical and SEM analysis was carried out on machined sample to study the uniform distribution of particles. XRD and EDAX analysis is carried out to confirm the dispersion of particles into the matrix. Uniform distribution of the particles is found in optical and SEM images for these stirring parameters. The peak representation of boron and graphite particles is also observed in XRD and EDAX analysis. Theoretical and experimental density of the cast sample is determined by rule of mixture and Archimedes principle. Result shows the density of the composite decreases by increasing percentage of reinforcements. Micro Vickers hardness was tested on the cast composites and the result showed Al 2024 alloy hardness was increased by 31.25% by reinforcing boron and graphite. Similarly, tensile and compression strength increased by increasing the percentage of reinforcement. Tensile and compression strength of Al 2024 alloy increased by 45.23% and 29.18% respectively. The ductility of the composites decreased by increasing the percentage of reinforcements.展开更多
In present study, BP neural network model was proposed for the prediction of ultimate compressive strength of Al2O3-ZrO2 ceramic foam filter prepared by centrifugal slip casting. The inputs of the BP neural network mo...In present study, BP neural network model was proposed for the prediction of ultimate compressive strength of Al2O3-ZrO2 ceramic foam filter prepared by centrifugal slip casting. The inputs of the BP neural network model were the applied load on the epispastic polystyrene template (F), centrifugal acceleration (v) and sintering temperature (T), while the only output was the ultimate compressive strength ((7). According to the registered BP model, the effects of F, v, T on 0 were analyzed. The predicted results agree with the actual data within reasonable experimental error, indicating that the BP model is practically a very useful tool in property prediction and process parameter design of the Al2O3-ZrO2 ceramic foam filter prepared by centrifugal slip casting.展开更多
文摘In today’s manufacturing industries,hard competition between rival firms makes it compulsory for researchers to design lighter and cheaper machine components due to the megatrends of cost-effectiveness and anti-pollution.At this point,aluminum syntactic foams(ASFs)are new-generation engineering composites and come into the upfront as a problem-solver.Owing to their features like low density,sufficient elongation,and perfect energy absorption ability,these advanced foams have been considerably seductive for many industrial sectors nowadays.In this study,an industrial-oriented automatic die casting technology was used for the first time to manufacture the combination of AA7075/porous expanded clay(PEC).Micro evaluations(optical and FESEM)reveal that there is a homogenous particle distribution in the foam samples,and inspections are compatible with the other ASF studies.Additionally,T6 aging heat treatment was operated on one half of the produced foams to explore the probable impact of aging on the compressive responses.Attained results show that PEC particles can be an alternative to expensive hollow spheres used in the previous works.Besides,a favorable relationship is ascertained between the aging treatment and mechanical properties such as compression strength and plateau strength.
基金Project(10020072) supported by the Korean Ministry of Commerce,Industry and EnergyProject(Y2008F27) supported by the Natural Science Foundation of Shandong Province,China
文摘The microstructures of ZK60 alloy under conventional direct as-casting (DC),twin roll casting (TRC) and twin roll casting followed by hot compression (TRC-HC) were analyzed by optical morphology (OM),electron backscatter diffraction (EBSD) and X-ray diffraction (XRD).The deformation condition of hot compression is 350 ℃,0.1 s?1.The microstructural evolution under TRC-HC deformation followed by annealing at different temperatures and time was discussed.The results show that TRC provides more modified microstructure compared with DC.Twins are found in TRC processing;dynamic recrystallization (DRX),shear bands and twins are found in TRC-HC.A short annealing time has little effect on hardness,while during a long time annealing,it is found that low annealing temperatures increase the micro-hardness and high temperature decreases it.
基金Project(Y2008F27)supported by the Natural Science Foundation of Shandong Province,China
文摘A dynamic material model of Mg-4.51Al-1.19Zn-0.5Mn-0.5Ca(AZ41,mass fraction,%)magnesium alloy was put forward.The results show that the dynamic material model can characterize the deformation behavior and microstructure evolution and describe the relations among flow stress,strain,strain rates and deformation temperatures.Statistical analysis shows the validity of the proposed model.The model predicts that lower deformation temperature and higher strain rate cause the sharp strain hardening. Meanwhile,the flow stress curve turns into a steady state at high temperature and lower strain rate.The moderate temperature of 350 ℃and strain rate of 0.01 s-1 are appropriate to this alloy.
基金supported by the Natural Science Foundation of Shandong Province (Nos Y2008F27 and ZR2009FL003)the S&T Developing Program of Shandong Province, China (2007GG10004013)the Doctoral Foundation of University of Jinan (XBS0830)
文摘The relationship of true stress and true strain of AZ41M magnesium alloy under twin-roll-cast (TRC) and hot compression was analyzed us- ing a Gleeble 1500 machine. Microstructural evolutions of the TRC magnesium alloy under different deformation conditions (strain, sWain rate and deformation temperature) were examined using optical microscopy and discussed. The relationship of true stress and true sWain pre- dicted that lower deformation temperature and higher sWain rate caused sharp strain hardening. Meanwhile, the flow stress curve turned into a steady state at high temperature and lower strain rate. The intermediate temperature and strain rate (623 K and 0.01 s^-1) is appropriate.
文摘Fine, equiaxed, non dendritic structure needed by semi solid processing was obtained by liquidus cast, i.e. 7075 wrought aluminum alloy cast from liquidus temperature. The microstructures after heat treatment at different temperatures and time in the semi solid range were observed, and the compression deformation behavior at different temperatures (490~600 ℃) and strain rates (5×10 -3 ~5s -1 ) was investigated by means of Gleeble 1500 thermal mechanical simulator. The results show that the deformation resistance of the non dendritic structure attained by liquidus cast in semi solid is remarkably lower than that of conventional dendritic structure. The formability of non dendritic structure is better than that of dendritic structure.
文摘The flow behavior of a cast Ti-25Al-10Nb-3V-1Mo alloy based onTi3Al, with and without hydrogen content, was investigated under isothermal compression test at strain rates of 0.1s-1 to 0.001s -1 in the temperature range of 900℃ to1000 ℃. The hot compression peak stress (or the maximum flow stress) of the alloy withand without hydrogen decreases with the increasing temperature and the decreasingstrain rate. Hydrogenation makes the hot compression peak stress decrease by 37%~53%, which corresponds to lowering the deformation temperature by about 50℃.Strain rate does not change the favorable effect of hydrogenation on hot compressionflow behavior at all three deformation temperatures. The microstructure of the alloywith 0.2% H (mass %) deformed at a fixed temperature exhibits the same feature asthat of the alloys without hydrogenation deformed at higher temperatures for bothstrain rates. Hydrogenation has the same effect on microstructure as strain rate andtemperature.
基金Project (05YB31) supported by the Scientific Research Initial Foundation for Doctor of Shenyang Institute of Aeronautical Engineering,China
文摘The NiAl-28Cr-5.85Mo-0.15Hf alloy was prepared by high-pressure die casting (HPDC) and subsequent hot isostatic pressing(HIP), and tested for compressible strength and fracture behavior at 300-1 373 K. The results show that the elevated temperature 0.2% compressible yield strength as well as the room-temperature compressible fracture strain of as-HIP alloy are larger than those of the same alloy prepared by directional solidification (DS). It suggests that the fine structures with a homogeneous distribution of fine Cr (Mo) and Hf-rich phase created by high-pressure die casting lead to these improvements.
基金funded by European sources within the ERASMUS-SOCRATES program
文摘Sea urchin spines were chosen as a model system for biomimetic ceramics obtained using starch-blended slip casting. Porous alumina ceramics with cap-shaped layers with different alternating porosities were found to have superior fracture behavior under bulk compression compared to ceramics with uniform porosity.They fail in a cascading manner,absorbing high amounts of energy during extended compression paths.The porosity variation in an otherwise single phase material mimicks the architectural microstructure design of sea urchin spines of Heterocentrotus mammillatus,which are promising model materials for impact protection.
基金supported by the Technology Development Fund of the China Academy of Machinery Science and Technology(No.170221ZY01).
文摘As a new type of lightweight structure,metallic lattice structure has higher stiffness and strength to weight ratio.To freely obtain 316L lattice structures with designed cell structure and adjustable porosity,additive manufacturing combined with investment casting was conducted to fabricate the 316L lattice structures with Kelvin cell.The compression simulation of 316L lattice structures with different porosities was carried out by using the finite element method.The numerical simulation results were verified by compression experiment,and the simulated results were consistent with the compression tests.The compressive mechanical properties of 316L lattice structures are directly related to porosity and independent of strut diameters.The 316L lattice structures with Kelvin cell have a smooth stress-strain curve and obvious plastic platform,and the hump stress-strain curves are avoided.
文摘The effect of Zr on the behavior of compressive creep in as cast ZA27 alloy was investigated in the temperature range of 20160 ℃ and under different compressive stresses in the range of 50137.5 MPa with special apparatus. The results show that the primary compressive creep strains and steady creep rates of ZA27 Zr alloy and ZA27 alloy increase with increasing temperature and stress. However, the primary compressive creep strain and steady creep rate of the ZA27 Zr alloy are lower than that of the ZA27 alloy below 100 ℃, but higher at 160 ℃. The compressive creep behaviors in both ZA27 Zr alloy and ZA27 alloy obey an empirical equation ln t=C-n ln σ+ Q/RT , and the exponent stress n is 3.63 for ZA27 Zr alloy and 3.46 for ZA27 alloy, respectively, the activation energy Q is 87.32 kJ/mol for ZA27 Zr alloy and 81.09 kJ/mol for ZA27 alloy. Different material structural constants are associated with different compressive creep behaviors in the alloy. The compressive creep rate in the alloy is controlled by the lattice diffusion of zinc and dislocation limb.
基金financially supported by the Natural Science Foundation of Liaoning Province(No.:201102090)the Doctoral Initiating Project of Liaoning Province Foundation for Natural Sciences,China(No.:20111068)+2 种基金the High School Development Plan for Distinguished Young Scholars of Liaoning Province Education Committee(No.:LJQ2012056)the National High-Tech Research and Development Program of China("863"Program,No.:2011AA060102)the International Science and Technology Cooperation Program of China,(No.:2011DFR50270)
文摘The aim of the present research is to provide a novel technique for preparing gradient Al 2 O 3-ZrO 2 ceramic foams.This technique used epispastic polystyrene spheres to array templates and centrifugal slip casting to obtain cell struts with gradient distribution of Al 2 O 3 and ZrO 2 particles and high packing density.Aqueous Al 2 O 3-20vol.% ZrO 2 slurries with 20vol.% solid contents were prepared and the dispersion and rheological characteristics of the slurries were investigated.The settling velocity and mass segregation of Al 2 O 3 and ZrO 2 particles at different centrifugal accelerations were calculated and studied.The drying behavior,macrostructure,microstructure,compressive property and resistance to thermal shock of the sintered products were also investigated.The results show that the difference of settling velocity of Al 2 O 3 and ZrO 2 particles increases and mass segregation becomes acute with an increase in centrifugal acceleration.The cell struts prepared at a centrifugal acceleration of 1,690 g have high sintered density(99.0% TD) and continuous gradient distribution of Al 2 O 3 and ZrO 2 particles.When sintered at 1,550 o C for 2 h,the cell size of gradient Al 2 O 3-ZrO 2 foam is approximately uniform,about 1.1 mm.With the porosity of gradient Al 2 O 3-ZrO 2 ceramic foams increasing from 75.3% to 83.0%,the compressive strength decreases from 4.4 to 2.4 MPa,and the ceramic foams can resist 8-11 repeated thermal shock from 1,100 o C to room temperature.
文摘Phosphate-bonded investments have already been widely utilized in dental restoration and micro-casting of artistic products for its outstanding rapid setting and high strength. However, the rapid setting rate of investment slurry has up to now been a barrier to extend the use of such slurry in preparation of medium-sized ceramic moulds. This paper proposes a new process of rapid fabrication of magnesia-phosphate-bonded investment ceramic moulds for medium-sized superalloy castings utilizing bauxite and mullite as refractory aggregates. In order to determine the properties of magnesia-phosphate-bonded bauxite-mullite investments (MPBBMI), a series of experiments were conducted, including modifciation of the workable time of slurry by liquid(mL)/powder(g)(L/P) ratio and addition of boric acid as retard agent and sodium tri-polyphosphate (STP) as strengthening agent, and adjustment of bauxite (g)/mullite(g)(B/M) ratio for mechanical strength. Mechanical vibration was applied to improve initial setting time and fluidity when pouring investment slurry; then an intermediate size ceramic mould for superalloy castings was manufactured by means of this rapid preparing process with MPBBMI material. The results showed that the MPBBMI slurry exhibits proper initial setting time and excellent fluidity when the L/P ratio is 0.64 and the boric acid content is 0.88wt.%. The fired specimens made from the MPBBMI material demonstrated adequate compression strength to withstand impact force of molten metal when the B/M ratio is 0.89 and the STP content is 0.92wt.%. The experimental results confirmed the feasibility of the proposed rapid fabricating process for medium-sized ceramic moulds with MPBBMI material by appropriate measures.
文摘In this study, boron fiber powder and graphite is reinforced to Al 2024 alloy to develop hybrid metal matrix composite by stir casting process. Hybrid MMCs developed with different weight fraction for 4%, 6%, 8% and 10% of boron fiber and 2% of graphite. Stirring parameters are optimized to obtain solid casting. Reinforcements are poured into molten aluminium at 15 g/min and stirrer is rotated for 5 minutes at 250 rpm with two stages stirring. 1% of magnesium was added to improve the wettability of Al 2024. Cast samples are machined as per the standards to investigate the microstructure, physical and mechanical properties. Optical and SEM analysis was carried out on machined sample to study the uniform distribution of particles. XRD and EDAX analysis is carried out to confirm the dispersion of particles into the matrix. Uniform distribution of the particles is found in optical and SEM images for these stirring parameters. The peak representation of boron and graphite particles is also observed in XRD and EDAX analysis. Theoretical and experimental density of the cast sample is determined by rule of mixture and Archimedes principle. Result shows the density of the composite decreases by increasing percentage of reinforcements. Micro Vickers hardness was tested on the cast composites and the result showed Al 2024 alloy hardness was increased by 31.25% by reinforcing boron and graphite. Similarly, tensile and compression strength increased by increasing the percentage of reinforcement. Tensile and compression strength of Al 2024 alloy increased by 45.23% and 29.18% respectively. The ductility of the composites decreased by increasing the percentage of reinforcements.
基金financially supported by the Innovation Research Team Program of the Ministry of Education(IRT0713)the Key Laboratory of New Materials in Automobile of Liaoning Province(grant No.201016201)Doctoral Initiating Project of Liaoning Province Foundation for Natural Sciences,China
文摘In present study, BP neural network model was proposed for the prediction of ultimate compressive strength of Al2O3-ZrO2 ceramic foam filter prepared by centrifugal slip casting. The inputs of the BP neural network model were the applied load on the epispastic polystyrene template (F), centrifugal acceleration (v) and sintering temperature (T), while the only output was the ultimate compressive strength ((7). According to the registered BP model, the effects of F, v, T on 0 were analyzed. The predicted results agree with the actual data within reasonable experimental error, indicating that the BP model is practically a very useful tool in property prediction and process parameter design of the Al2O3-ZrO2 ceramic foam filter prepared by centrifugal slip casting.
基金the foundation from the National Key Research and Development Program of China (No. 2020YFB1505901)the support by Xiao-qin ZENG Expert Workstation in Yunnan Province, China (No. 202005AF150059)。