Accurately measuring magnetic fields is essential for magnetic-field sensitive experiments in areas like atomic,molecular,and optical physics,condensed matter experiments,and other areas.However,since many experiments...Accurately measuring magnetic fields is essential for magnetic-field sensitive experiments in areas like atomic,molecular,and optical physics,condensed matter experiments,and other areas.However,since many experiments are often conducted in an isolated environment that is inaccessible to experimentalists,it can be challenging to accurately determine the magnetic field at the target location.Here,we propose an efficient method for detecting magnetic fields with the assistance of an artificial neural network(NN).Instead of measuring the magnetic field directly at the desired location,we detect fields at several surrounding positions,and a trained NN can accurately predict the magnetic field at the target location.After training,we achieve a below 0.3%relative prediction error of magnetic field magnitude at the center of the vacuum chamber,and successfully apply this method to our erbium quantum gas apparatus for accurate calibration of magnetic field and long-term monitoring of environmental stray magnetic field.The demonstrated approach significantly simplifies the process of determining magnetic fields in isolated environments and can be applied to various research fields across a wide range of magnetic field magnitudes.展开更多
We use nuclear magnetic resonance (NMR) and centrifugation to measure the original water saturation and mobile water saturation of cores from the Xujiahe low permeability sandstone gas reservoir, and compare the NMR...We use nuclear magnetic resonance (NMR) and centrifugation to measure the original water saturation and mobile water saturation of cores from the Xujiahe low permeability sandstone gas reservoir, and compare the NMR results with the corresponding field data. It is shown that the NMR water saturation after 300psi centrifugation effectively represents the original water saturation measured by weighing fresh cores. There is a good correlation between mobile water saturation and the water production performance of the corresponding gas wells. The critical mobile water saturation whether reservoir produces water of the Xujiahe low permeability sandstone gas is 6%. The higher the mobile water saturation, the greater the water production rate of gas well. This indicates that well's water production performance can be forecasted by mobile water saturation of cores.展开更多
Based on analyzing the induced signals from the double-grids of an ionization chamber, the electron-drift time between the two grids is determined and the electron-drift velocity is derived. A waveform digitizer is em...Based on analyzing the induced signals from the double-grids of an ionization chamber, the electron-drift time between the two grids is determined and the electron-drift velocity is derived. A waveform digitizer is employed to record pulses from the two grids of the ionization chamber. The electron-drift velocity is measured as a function of the reduced electric field E/p for eight different ratios of Ar+CH4 mixtures. By analyzing the experimental data of this study, self-consistency of experimental data is achieved, and formulae for calculating electron-drift velocity in any ratio of Ar+CH4 mixtures are obtained.展开更多
A novel method for velocity measurement is presented. In this scheme, a parallel-linear-polarization dual- frequency laser is incident on the target and senses the target velocity with both the frequencies, which can ...A novel method for velocity measurement is presented. In this scheme, a parallel-linear-polarization dual- frequency laser is incident on the target and senses the target velocity with both the frequencies, which can increase the maximum measurable velocity significantly. The theoretical analysis and verification experiment of the novel method are presented, which show that high-velocity measurement can be achieved with high precision using this method.展开更多
Accelerator mass spectrometry (AMS) is one of the most promising methods to detect minute amounts of 182Hf. However, the sensitivity of 5×10^-11 for ^182Hf/180Hf obtained previously by the AMS method at China I...Accelerator mass spectrometry (AMS) is one of the most promising methods to detect minute amounts of 182Hf. However, the sensitivity of 5×10^-11 for ^182Hf/180Hf obtained previously by the AMS method at China Institute of Atomic Energy (CIAE) cannot meet the requirement of some applications. We present some new improvements of measurement method for AMS measurement of 182Hf at the CIAE HI?13 tandem accelerator system. As a result, a sensitivity of 1.0×10^-11 for 182Hf/180Hf is achieved.展开更多
An experimental measurement of radiatively heated iron plasma transmission spectra was performed on Shenguang II laser facility. In the measurement, the self?emission spectrum, the backlighting spectrum, and the abso...An experimental measurement of radiatively heated iron plasma transmission spectra was performed on Shenguang II laser facility. In the measurement, the self?emission spectrum, the backlighting spectrum, and the absorption spectrum were imaged with a flat filed grating and recorded on a gated micro channel plate detector to obtain the time-resolved transmission spectra in the range 10-20 ? (approximately 0.6-1.3 keV). Experimental results are compared with the calculation results of an unsolved transition array (UTA) code. The time-dependent relative shift in the positions of the 2p-3d transmission array is interpreted in terms of the plasma temperature variations.展开更多
A portable microcomputer-controlled inspection system has been developed for detection of magnetic properties of soft magnetic materials. It incorporates custom designed software for control of the magnetic field duri...A portable microcomputer-controlled inspection system has been developed for detection of magnetic properties of soft magnetic materials. It incorporates custom designed software for control of the magnetic field during operation such as demagnetization, field sweeping, and for data logging and analysis. Results are recorded using a 12-bit analog to digital converter and are then stored on disk. The magnetic hysteresis loop and Barkhausen noise data can be converted into important magnetic parameters: coecivity, remanence, and hysteresis loss, Barkhausen amplitude, and Barkhausen noise energy. This system incorporated with the magnetostriction, and magnetoacoustic emission, is then related with the nondestructive detection of material degradation.展开更多
General Administration of Quality Supervision,Inspection and Quarantine of P.R.China has approved the following 8 national measuring verification regulations in 2010 and publicize now.
This paper mainly discusses the development status of solar radiation measurement technology,it expounds the relevant content of the current world radiation measurement datum and its standardization. Article the direc...This paper mainly discusses the development status of solar radiation measurement technology,it expounds the relevant content of the current world radiation measurement datum and its standardization. Article the direct radiation from the sun,the main measuring principle of total radiation and scattering radiation,this paper discusses the different types of radiation survey measuring elements,measuring range,emphasis and the current widespread use of measurement instruments. The development trend of future solar radiation measurement is put forward,and it is emphasized that nanotechnology and spectrum technology will become the focus of solar radiation instrument research and development.展开更多
General Administration of Quality Supervision,Inspection and Quarantine of P.R.China has approved the following 11 national measuring verification regulations in 2008 and publicize now.
General Administration of Quality Supervision,Inspection and Quarantine of P.R.China hasapproved the following 24 national measuring verification regulations in 2008 and publicize now.
General Administration of Quality Supervision,Inspection and Quarantine of P.R.China has approved the following 10 national measuring verification regulations in 2008 and publicize now.
Traditional calibration methods mostly focus on the calibration of detection systems while the calibration from the sampling and pre-condition systems to the detection system is usually ignored.In this regard,a Primar...Traditional calibration methods mostly focus on the calibration of detection systems while the calibration from the sampling and pre-condition systems to the detection system is usually ignored.In this regard,a Primary Standard Aerosol Mass Concentration Calibration System(PAMAS)is developed for the whole-process calibration of time-resolved aerosol measurement instruments.PAMAS is composed of a particle generation chamber,an ultrasonic atomizer,a dilution system,and a syringe pump.It is designed to steadily generate standard aerosol particles of known concentrations(≤250μg/m^(3)),chemical compositions,and stable particle size distributions.Monodispersed aerosol can be generated in the size range of hundreds of nanometers to several micrometers with a narrow size distribution.The generated particles with different compositions generated by PAMAS have been well verified by the filter-based gravimetric method,yielding accuracy and R^(2) of more than 95%and 0.999 in a wide concentration range.The response time by changing the target concentration of reference particles is 1-2 min.PAMAS has been applied to various types of time-resolved aerosol measurement instruments,including particle mass concentration monitors(Beta Attenuation and Tapered Element Oscillating Microbalance),online Ion Chromatograph,and semi-continuous OCEC carbon aerosol analyzer.Very consistent results between PAMAS and calibrated instruments can be obtained if the instruments are functioning well.As for instruments with certain technical issues,PAMAS can serve as a good tool for performance evaluation and quality assurance of the instruments and the accuracy of the measurement data can be adjusted based on the calibration results.展开更多
Methodological quality(risk of bias)assessment is an important step before study initiation usage.Therefore,accurately judging study type is the first priority,and the choosing proper tool is also important.In this re...Methodological quality(risk of bias)assessment is an important step before study initiation usage.Therefore,accurately judging study type is the first priority,and the choosing proper tool is also important.In this review,we introduced methodological quality assessment tools for randomized controlled trial(including individual and cluster),animal study,non-randomized interventional studies(including follow-up study,controlled before-and-after study,before-after/pre-post study,uncontrolled longitudinal study,interrupted time series study),cohort study,case-control study,cross-sectional study(including analytical and descriptive),observational case series and case reports,comparative effectiveness research,diagnostic study,health economic evaluation,prediction study(including predictor finding study,prediction model impact study,prognostic prediction model study),qualitative study,outcome measurement instruments(including patient-reported outcome measure development,content validity,structural validity,internal consistency,cross-cultural validity/measurement invariance,reliability,measurement error,criterion validity,hypotheses testing for construct validity,and responsiveness),systematic review and meta-analysis,and clinical practice guideline.The readers of our review can distinguish the types of medical studies and choose appropriate tools.In one word,comprehensively mastering relevant knowledge and implementing more practices are basic requirements for correctly assessing the methodological quality.展开更多
目的 比较可用于卫生技术评估中的生产率损失测量工具,厘清可用于卫生技术评估中的生产率损失测量工具的应用条件,以期为相关研究者在选择生产率损失的测量工具时提供参考。方法 检索PubMed、Web of Science、中国知网、万方、维普等中...目的 比较可用于卫生技术评估中的生产率损失测量工具,厘清可用于卫生技术评估中的生产率损失测量工具的应用条件,以期为相关研究者在选择生产率损失的测量工具时提供参考。方法 检索PubMed、Web of Science、中国知网、万方、维普等中外数据库,检索时间从数据库建库至2021年11月,由2名研究者按照纳入与排除标准独立筛选文献、识别生产率损失测量工具、提取资料。结果 共识别出5种可用于卫生技术评估领域中的生产率损失测量工具,包括工作能力和活动受损量表(work productivity activity and impairment,WPAI)、工作能力局限调查问卷(work limitations questionnaire,WLQ)、健康与工作绩效问卷(Health and Work Performance Questionnaire,HPQ)、损失产能的估值(Valuation of Lost Productivity Questionnaire,VOLP)和医疗技术评估研究院(Institute for Medical Technology Assessment,IMTA)的生产力成本问卷(IMTA Productivity Questionnaire,IPCQ)。其中WPAI和WLQ是测量属性证据最为充足的工具;VOLP是成本涵盖最全的工具;WLQ是数据敏感性最强的工具;IPCQ是货币转化方法最多的工具;WPAI是获取使用最方便的工具。结论 对于卫生技术评估中的生产率损失测量的标准工具尚未存在统一共识,研究者可根据自身研究选取生产率损失测量工具。展开更多
A new concept called intelligent virtual control (IVC), which can be drivenby measuring functions, is put forward. This small 'intelligent measurement instrument unit (IMIU)',carrying with functions of instrum...A new concept called intelligent virtual control (IVC), which can be drivenby measuring functions, is put forward. This small 'intelligent measurement instrument unit (IMIU)',carrying with functions of instrument, consists of different types of intelligent virtualinstrument (IVI) through individual components together as building blocks and can be displayeddirectly on the computer screen. This is a new concept of measuring instrument, and also animportant breakthrough after virtual instrument (VI). Virtual control makes instrument resourcesobtain further exploitation. It brings about a fundamental change to the design and manufacturingmode. The instrument therefore, can not only be produced directly inside a PC, but the product isinvolved in the 'green product' system. So far, all the present digital instruments will grow to bereplaced by intelligent control with green characteristics.展开更多
The castings defects are affected by the melting volume change rate of material. The change rate has an important effect on running safety of the high temperature thermal storage chamber, too. But the characteristics ...The castings defects are affected by the melting volume change rate of material. The change rate has an important effect on running safety of the high temperature thermal storage chamber, too. But the characteristics of existing measuring installations are complex structure, troublesome operation and low precision. In order to measure the melting volume change rate of material accurately and conveniently, a self-designed measuring instrument, self-heating probe instrument, and measuring method are described. Temperature in heating cavity is controlled by PID temperature controller; melting volume change rate υ and molten density are calculated based on the melt volume which is measured by the instrument. Positive and negative υ represent expansion and shrinkage of the sample volume after melting, respectively. Taking eutectic LiF+CaF2 for example, its melting volume change rate and melting density at 1 123 K are -20.6% and 2 651 kg/m–3 measured by this instrument, which is only 0.71% smaller than literature value. Density and melting volume change rate of industry pure aluminum at 973 K and analysis pure NaCl at 1 123 K are detected by the instrument too. The measure results are agreed with report values. Measuring error sources are analyzed and several improving measures are proposed. In theory, the measuring errors of the change rate and molten density which are measured by the self-designed instrument is nearly 1/20-1/50 of that measured by the refitted mandril thermal expansion instrument. The self-designed instrument and method have the advantages of simple structure, being easy to operate, extensive applicability for material, relatively high accuracy, and most importantly, temperature and sample vapor pressure have little effect on the measurement accuracy. The presented instrument and method solve the problems of complicated structure and procedures, and large measuring errors for the samples with high vapor pressure by existing installations.展开更多
An accurate phase shift extraction method for generalized phase-shifting interferometry is suggested. Based on the nearly random phase distribution of the diffraction field of the object, a singular formula is derived...An accurate phase shift extraction method for generalized phase-shifting interferometry is suggested. Based on the nearly random phase distribution of the diffraction field of the object, a singular formula is derived to calculate the unknown phase shift without the requirements of an iteration process or the selection of the correct value from two or more possible phase shift solutions as needed before. This method can be used in the cases of two or more frames with both smooth and diffusing object surfaces. Computer simulations and optical experiments have satisfactorily verified the efficiency and accuracy of this method.展开更多
基金Project supported by the RGC of China(Grant Nos.16306119,16302420,16302821,16306321,16306922,C6009-20G,N-HKUST636-22,and RFS2122-6S04).
文摘Accurately measuring magnetic fields is essential for magnetic-field sensitive experiments in areas like atomic,molecular,and optical physics,condensed matter experiments,and other areas.However,since many experiments are often conducted in an isolated environment that is inaccessible to experimentalists,it can be challenging to accurately determine the magnetic field at the target location.Here,we propose an efficient method for detecting magnetic fields with the assistance of an artificial neural network(NN).Instead of measuring the magnetic field directly at the desired location,we detect fields at several surrounding positions,and a trained NN can accurately predict the magnetic field at the target location.After training,we achieve a below 0.3%relative prediction error of magnetic field magnitude at the center of the vacuum chamber,and successfully apply this method to our erbium quantum gas apparatus for accurate calibration of magnetic field and long-term monitoring of environmental stray magnetic field.The demonstrated approach significantly simplifies the process of determining magnetic fields in isolated environments and can be applied to various research fields across a wide range of magnetic field magnitudes.
文摘We use nuclear magnetic resonance (NMR) and centrifugation to measure the original water saturation and mobile water saturation of cores from the Xujiahe low permeability sandstone gas reservoir, and compare the NMR results with the corresponding field data. It is shown that the NMR water saturation after 300psi centrifugation effectively represents the original water saturation measured by weighing fresh cores. There is a good correlation between mobile water saturation and the water production performance of the corresponding gas wells. The critical mobile water saturation whether reservoir produces water of the Xujiahe low permeability sandstone gas is 6%. The higher the mobile water saturation, the greater the water production rate of gas well. This indicates that well's water production performance can be forecasted by mobile water saturation of cores.
基金Supported by the National Natural Science Foundation of China under Grant Nos 10875006 and 10811120014, and China Nuclear Data Center.
文摘Based on analyzing the induced signals from the double-grids of an ionization chamber, the electron-drift time between the two grids is determined and the electron-drift velocity is derived. A waveform digitizer is employed to record pulses from the two grids of the ionization chamber. The electron-drift velocity is measured as a function of the reduced electric field E/p for eight different ratios of Ar+CH4 mixtures. By analyzing the experimental data of this study, self-consistency of experimental data is achieved, and formulae for calculating electron-drift velocity in any ratio of Ar+CH4 mixtures are obtained.
文摘A novel method for velocity measurement is presented. In this scheme, a parallel-linear-polarization dual- frequency laser is incident on the target and senses the target velocity with both the frequencies, which can increase the maximum measurable velocity significantly. The theoretical analysis and verification experiment of the novel method are presented, which show that high-velocity measurement can be achieved with high precision using this method.
基金Supported by the Foundation of China Academy of Engineering Physics under Grant No 10576040, and the National Natural Science Foundation of China under Grant No 10705054.
文摘Accelerator mass spectrometry (AMS) is one of the most promising methods to detect minute amounts of 182Hf. However, the sensitivity of 5×10^-11 for ^182Hf/180Hf obtained previously by the AMS method at China Institute of Atomic Energy (CIAE) cannot meet the requirement of some applications. We present some new improvements of measurement method for AMS measurement of 182Hf at the CIAE HI?13 tandem accelerator system. As a result, a sensitivity of 1.0×10^-11 for 182Hf/180Hf is achieved.
基金Supported by the National Natural Science Foundation of China under Grant Nos 10734140, 10874156 and 10875109.
文摘An experimental measurement of radiatively heated iron plasma transmission spectra was performed on Shenguang II laser facility. In the measurement, the self?emission spectrum, the backlighting spectrum, and the absorption spectrum were imaged with a flat filed grating and recorded on a gated micro channel plate detector to obtain the time-resolved transmission spectra in the range 10-20 ? (approximately 0.6-1.3 keV). Experimental results are compared with the calculation results of an unsolved transition array (UTA) code. The time-dependent relative shift in the positions of the 2p-3d transmission array is interpreted in terms of the plasma temperature variations.
基金Reactor Pressure Boundary Materials Project !under the Nuclear R & D Program by MOST in Korea.
文摘A portable microcomputer-controlled inspection system has been developed for detection of magnetic properties of soft magnetic materials. It incorporates custom designed software for control of the magnetic field during operation such as demagnetization, field sweeping, and for data logging and analysis. Results are recorded using a 12-bit analog to digital converter and are then stored on disk. The magnetic hysteresis loop and Barkhausen noise data can be converted into important magnetic parameters: coecivity, remanence, and hysteresis loss, Barkhausen amplitude, and Barkhausen noise energy. This system incorporated with the magnetostriction, and magnetoacoustic emission, is then related with the nondestructive detection of material degradation.
文摘General Administration of Quality Supervision,Inspection and Quarantine of P.R.China has approved the following 8 national measuring verification regulations in 2010 and publicize now.
文摘This paper mainly discusses the development status of solar radiation measurement technology,it expounds the relevant content of the current world radiation measurement datum and its standardization. Article the direct radiation from the sun,the main measuring principle of total radiation and scattering radiation,this paper discusses the different types of radiation survey measuring elements,measuring range,emphasis and the current widespread use of measurement instruments. The development trend of future solar radiation measurement is put forward,and it is emphasized that nanotechnology and spectrum technology will become the focus of solar radiation instrument research and development.
文摘General Administration of Quality Supervision,Inspection and Quarantine of P.R.China has approved the following 11 national measuring verification regulations in 2008 and publicize now.
文摘General Administration of Quality Supervision,Inspection and Quarantine of P.R.China hasapproved the following 24 national measuring verification regulations in 2008 and publicize now.
文摘General Administration of Quality Supervision,Inspection and Quarantine of P.R.China has approved the following 10 national measuring verification regulations in 2008 and publicize now.
基金supported by the National Natural Science Foundation of China (grant No.42175119).
文摘Traditional calibration methods mostly focus on the calibration of detection systems while the calibration from the sampling and pre-condition systems to the detection system is usually ignored.In this regard,a Primary Standard Aerosol Mass Concentration Calibration System(PAMAS)is developed for the whole-process calibration of time-resolved aerosol measurement instruments.PAMAS is composed of a particle generation chamber,an ultrasonic atomizer,a dilution system,and a syringe pump.It is designed to steadily generate standard aerosol particles of known concentrations(≤250μg/m^(3)),chemical compositions,and stable particle size distributions.Monodispersed aerosol can be generated in the size range of hundreds of nanometers to several micrometers with a narrow size distribution.The generated particles with different compositions generated by PAMAS have been well verified by the filter-based gravimetric method,yielding accuracy and R^(2) of more than 95%and 0.999 in a wide concentration range.The response time by changing the target concentration of reference particles is 1-2 min.PAMAS has been applied to various types of time-resolved aerosol measurement instruments,including particle mass concentration monitors(Beta Attenuation and Tapered Element Oscillating Microbalance),online Ion Chromatograph,and semi-continuous OCEC carbon aerosol analyzer.Very consistent results between PAMAS and calibrated instruments can be obtained if the instruments are functioning well.As for instruments with certain technical issues,PAMAS can serve as a good tool for performance evaluation and quality assurance of the instruments and the accuracy of the measurement data can be adjusted based on the calibration results.
基金supported(in part)by the Entrusted Project of National commission on health and health of China(No.2019099)the National Key Research and Development Plan of China(2016YFC0106300)the Nature Science Foundation of Hubei Province(2019FFB03902)。
文摘Methodological quality(risk of bias)assessment is an important step before study initiation usage.Therefore,accurately judging study type is the first priority,and the choosing proper tool is also important.In this review,we introduced methodological quality assessment tools for randomized controlled trial(including individual and cluster),animal study,non-randomized interventional studies(including follow-up study,controlled before-and-after study,before-after/pre-post study,uncontrolled longitudinal study,interrupted time series study),cohort study,case-control study,cross-sectional study(including analytical and descriptive),observational case series and case reports,comparative effectiveness research,diagnostic study,health economic evaluation,prediction study(including predictor finding study,prediction model impact study,prognostic prediction model study),qualitative study,outcome measurement instruments(including patient-reported outcome measure development,content validity,structural validity,internal consistency,cross-cultural validity/measurement invariance,reliability,measurement error,criterion validity,hypotheses testing for construct validity,and responsiveness),systematic review and meta-analysis,and clinical practice guideline.The readers of our review can distinguish the types of medical studies and choose appropriate tools.In one word,comprehensively mastering relevant knowledge and implementing more practices are basic requirements for correctly assessing the methodological quality.
文摘目的 比较可用于卫生技术评估中的生产率损失测量工具,厘清可用于卫生技术评估中的生产率损失测量工具的应用条件,以期为相关研究者在选择生产率损失的测量工具时提供参考。方法 检索PubMed、Web of Science、中国知网、万方、维普等中外数据库,检索时间从数据库建库至2021年11月,由2名研究者按照纳入与排除标准独立筛选文献、识别生产率损失测量工具、提取资料。结果 共识别出5种可用于卫生技术评估领域中的生产率损失测量工具,包括工作能力和活动受损量表(work productivity activity and impairment,WPAI)、工作能力局限调查问卷(work limitations questionnaire,WLQ)、健康与工作绩效问卷(Health and Work Performance Questionnaire,HPQ)、损失产能的估值(Valuation of Lost Productivity Questionnaire,VOLP)和医疗技术评估研究院(Institute for Medical Technology Assessment,IMTA)的生产力成本问卷(IMTA Productivity Questionnaire,IPCQ)。其中WPAI和WLQ是测量属性证据最为充足的工具;VOLP是成本涵盖最全的工具;WLQ是数据敏感性最强的工具;IPCQ是货币转化方法最多的工具;WPAI是获取使用最方便的工具。结论 对于卫生技术评估中的生产率损失测量的标准工具尚未存在统一共识,研究者可根据自身研究选取生产率损失测量工具。
基金This project is supported by National Natural Science Foundation of China(No.50135050).
文摘A new concept called intelligent virtual control (IVC), which can be drivenby measuring functions, is put forward. This small 'intelligent measurement instrument unit (IMIU)',carrying with functions of instrument, consists of different types of intelligent virtualinstrument (IVI) through individual components together as building blocks and can be displayeddirectly on the computer screen. This is a new concept of measuring instrument, and also animportant breakthrough after virtual instrument (VI). Virtual control makes instrument resourcesobtain further exploitation. It brings about a fundamental change to the design and manufacturingmode. The instrument therefore, can not only be produced directly inside a PC, but the product isinvolved in the 'green product' system. So far, all the present digital instruments will grow to bereplaced by intelligent control with green characteristics.
基金supported by Gansu Provincial Critical Patented Projects of China(Grant No. 1101ZSB117)Gansu Provincial Science and Technology Pillar Program of China(Grant No. 1002ZSB018)
文摘The castings defects are affected by the melting volume change rate of material. The change rate has an important effect on running safety of the high temperature thermal storage chamber, too. But the characteristics of existing measuring installations are complex structure, troublesome operation and low precision. In order to measure the melting volume change rate of material accurately and conveniently, a self-designed measuring instrument, self-heating probe instrument, and measuring method are described. Temperature in heating cavity is controlled by PID temperature controller; melting volume change rate υ and molten density are calculated based on the melt volume which is measured by the instrument. Positive and negative υ represent expansion and shrinkage of the sample volume after melting, respectively. Taking eutectic LiF+CaF2 for example, its melting volume change rate and melting density at 1 123 K are -20.6% and 2 651 kg/m–3 measured by this instrument, which is only 0.71% smaller than literature value. Density and melting volume change rate of industry pure aluminum at 973 K and analysis pure NaCl at 1 123 K are detected by the instrument too. The measure results are agreed with report values. Measuring error sources are analyzed and several improving measures are proposed. In theory, the measuring errors of the change rate and molten density which are measured by the self-designed instrument is nearly 1/20-1/50 of that measured by the refitted mandril thermal expansion instrument. The self-designed instrument and method have the advantages of simple structure, being easy to operate, extensive applicability for material, relatively high accuracy, and most importantly, temperature and sample vapor pressure have little effect on the measurement accuracy. The presented instrument and method solve the problems of complicated structure and procedures, and large measuring errors for the samples with high vapor pressure by existing installations.
基金Supported by the National Natural Science Foundation of China under Grant Nos 60977006, 60777008 and 40704021, and the Fund from China University of Petroleum (East China) under Grant No Y081818.
文摘An accurate phase shift extraction method for generalized phase-shifting interferometry is suggested. Based on the nearly random phase distribution of the diffraction field of the object, a singular formula is derived to calculate the unknown phase shift without the requirements of an iteration process or the selection of the correct value from two or more possible phase shift solutions as needed before. This method can be used in the cases of two or more frames with both smooth and diffusing object surfaces. Computer simulations and optical experiments have satisfactorily verified the efficiency and accuracy of this method.